• Title/Summary/Keyword: cryostat

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나노다공체 물성 측정을 위한 극저온(20K) 수소 BET 개발 및 응용 (Development of a Cost-Effective 20K Hydrogen BET Measurement for Nanoporous Materials)

  • 박재우;오현철
    • 한국재료학회지
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    • 제27권9호
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    • pp.466-470
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    • 2017
  • With the matters of climate change, energy security and resource depletion, a growing pressure exists to search for replacements for fossil fuels. Among various sustainable energy sources, hydrogen is thought of as a clean energy, and thus efficient hydrogen storage is a major issue. In order to realize efficient and safe hydrogen storage, various porous materials are being explored as solid-states materials for hydrogen storage. For those purposes, it is a prerequisite to characterize a material's textural properties to evaluate its hydrogen storage performance. In general, the textural properties of porous materials are analyzed by the Brunauer-Emmett-Teller (BET) measurement using nitrogen gas as a probe molecule. However, nitrogen BET analysis is sometimes not suitable for materials possessing small pores and surfaces with high curvatures like MOFs because the nitrogen molecule may sometimes be too large to reach the entire porous framework, resulting in an erroneous value. Hence, a smaller probe molecule for BET measurements (such as hydrogen) may be required. In this study, we describe a cost-effective novel cryostat for BET measurement that can reach temperatures below the liquefaction of hydrogen gas. Temperature and cold volume of the cryostat are corrected, and all measurements are validated using a commercial device. In this way, direct observation of the hydrogen adsorption properties is possible, which can translate directly into the determination of textural properties.

Cooling performance test of the superconducting fault current limiter

  • Yeom, H.;Hong, Y.J.;In, S.;Ko, J.;Kim, H.B.;Park, S.J.;Kim, H.;Kim, H.R.
    • 한국초전도ㆍ저온공학회논문지
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    • 제16권4호
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    • pp.66-70
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    • 2014
  • The superconducting fault current limiter (SFCL) is an electrical power system device that detects the fault current automatically and limits the magnitude of the current below a certain safety level. The SFCL module does not have any electrical resistance below the critical temperature, which facilitates lossless power transmission in the electric power system. Once given the fault current, however, the superconducting conductor exhibits extremely high electrical resistance, and the magnitude of the current is accordingly limited to a low value. Therefore, SFCL should be maintained at a temperature below the critical temperature, which justifies the cryogenic cooling system as a mandatory component. This report is a study which reported on the cooling system for the 154 kV-class hybrid SFCL owned by Korea Electric Power Corporation (KEPCO). Using the cryocooler, the temperature of liquid nitrogen (LN2) was lowered to 71 K. The cryostat was pressurized to 5 bars to improve the dielectric strength of nitrogen and suppress nitrogen bubble foaming during operation of SFCL. The SFCL module was immersed in the liquid nitrogen of the cryostat to maintain the superconducting state. The performance test results of the key components such as cryocooler, LN2 circulation pump, cold box, and pressure builder are shown in this paper.

적층단열재의 열침입량 측정 (Measurement of Heat Leak through Multi-Layer Insulation)

  • 김동락;양형석;정원묵;이병섭;신필권;황시돌
    • 한국초전도ㆍ저온공학회논문지
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    • 제7권3호
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    • pp.39-42
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    • 2005
  • In this paper, the thermal characteristics of multilayer insulation (MLI) were experimentally investigated by using boil-off calorimetry method for seeking optimum standards of thermal insulation conditions. It is necessary to design the thermal insulating efficiency for applying to cryogenic instruments such as HTS power cable system. It is well known that the thermal characteristics and heat transfer of MLI are greatly affected by various MLI structures such as the number of layers and layer density, etc. However, it is difficult to know the thermal characteristics of MLI correctly. The heat leak by MLI between room temperature and liquid nitrogen temperature was measured at various conditions using a cylindrical cryostat. The cryostat consists of two guard vessels located at both end sides and a test vessel between them. The guard vessels are also filled with liquid nitrogen to prevent radiation heat leak through the both end side of the cylindrical test vessel to measure the heat leak only through MLI.

하이브리드 방식을 적용한 배전급 초전도 한류기 개발 (Hybrid Superconducting Fault Current Limiters for Distribution Electric Networks)

  • 이방욱;박권배;심정욱;오일성;임성우;김혜림;현옥배
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2007년도 제38회 하계학술대회
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    • pp.102-103
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    • 2007
  • In order to apply resistive superconducting fault current limiters into electric power systems, the urgent issues to be settled are as follows, such as initial installation price of SFCL, operation and maintenance cost due to ac loss of superconductor and the life of cryostat, and high voltage and high current problems. The ac loss and high cost of superconductor and cryostat system are main bottlenecks for real application. Furthermore in order to increase voltage and current ratings of SFCL, a lot of superconductor components should be connected in series and parallel which resulted in extreme high cost. Thus, in order to make practical SFCL, we designed novel hybrid SFCL which combines superconductor and conventional electric equipment including vacuum interrupter, power fuse and current limiting reactor. The main purpose of hybrid SFCL is to drastically reduce total usage of superconductor by adopting current commutation method by use of superconductor and high fast switch. Consequently, it was possible to get the satisfactory test results using this method, and further works for practical applications are in the process.

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적외선 영상 기법에 의한 화합물 반도체 에너지 갭의 온도 계수 측정 방법 (A Method for evaluating the temperature coefficient of a compound semiconductor energy gap by infrared imaging technique)

  • 강성준
    • 대한전자공학회논문지SD
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    • 제38권5호
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    • pp.26-26
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    • 2001
  • 온도에 따른 반도체 에너지갭의 변화를 디지털 영상처리를 이용해 직접 측정하는 적외선 영상기법을 제안하고 있다. 본 방법은 반도체 에너지갭의 온도계수를 경제적이고 간단하게 평가할 수 있도록 한다. 본 기법의 핵심 구성 부품은 다색광원기(Polychromator), 프레임 그래버가 내장된 컴퓨터 및 가변 온도 저온유지장치(Cryostat)이다. 방법의 타당성을 검증하기 위해 LEC 방법으로 제조한 GaAs에 시험적으로 행한 실험은 온도 계수가 이론 모델에서 구한 값과 전반적으로 잘 일치함을 보여 주었다.

펄스 모드로 작동하는 증기냉각 전류 도입선에 관한 연구 (Investigation on vapor-cooled current leads operating in pulse mode)

  • 인세환;정상권
    • 한국초전도ㆍ저온공학회논문지
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    • 제4권1호
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    • pp.66-72
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    • 2002
  • This paper describes numerical modeling for thermal characteristic of vapor-cooled current leads under pulse operation. The transient thermal analysis considers the temperature difference between a helium gas (low and a copper lead and temperature dependent properties of helium gas, copper and stainless steel. This numerical modeling was compensated and validated by an experiment with commercially available 100 A vapor-cooled current leads. A proper overloading factor was suggested for the current leads under pulse operation through this modeling, which can significantly reduce heat input to a cryostat.

단면적 변화를 가지는 고온초전도체 전류도입선 해석 (Analysis of HTS Current Lead with Variable Area)

  • 문성수;설승윤
    • 한국초전도저온공학회:학술대회논문집
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    • 한국초전도저온공학회 2000년도 KIASC Conference 2000 / 2000년도 학술대회 논문집
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    • pp.22-25
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    • 2000
  • To improve the performance of high temperature superconducting current leads, variable cross-sectional area is considered. The cross-sectional area is varied as a function of current density to fix the safety factor along lead length. New integration method is devised to find optimum cross-sectional area distribution. New design of current lead has low heat leak into cryostat and less material than constant cross-sectional area leads. Conduction cooled lead is considered. The developed method is applied to Bi2223 current leads sheathed Ag-Au alloy.

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