• Korean Journal of Materials Research
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• v.4 no.3
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• pp.329-333
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• 1994

A large number of grain boundaries were seen to crack in near-eutectic solder joints of leadless ceramic chip carriers (LLCC's) during thermal cycling at temperature ranges from -$35^{\circ}C$ to +$125^{\circ}C$ with lhr time period. One potential explanation for this type of cracking might be the presence of embrittling species on the boundary. Although there do not appear to be any instances reported in the literature of solders being embrittled by small amounts of contaminating species, the possibility of such an occurrence exists. The potential presence of impurities located at crack surfaces was inspected using Scanning Auger Microprobe(SAM) and it was found that intergranular cracking could be accomplished by the oxidation of the grain boundary. A physical model for fatigue crack growth was introduced, in which grain boundary separation took place under oxidation facilitated by sliding.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.26 no.4
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• pp.617-624
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• 2002

An equation of J-integral for a penny-shaped crack at the end of the fiber embedded in rubber matrix is proposed. The values of J-integral for the specimens with various crack and specimen radius are obtained by FEA(Finite Element Analysis). The dimensional analysis is applied to derive an equation of J-integral as a nonlinear elastic energy release rate. The geometry and deformation calibration function in an equation of J can be expressed in a separated form. The geometry calibration function characterizing the effects of cord and specimen size is expressed in a polynomial form of fourth order. The deformation calibration function characterizes the effect of the overall level of strain. As approaching the infinitesimal strain, the value of the deformation calibration function approaches the results of LEFM(Linear Elastic Fracture Mechanics).

• Transactions of the Korean Society of Mechanical Engineers A
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• v.29 no.5 s.236
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• pp.663-670
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• 2005

DIN CK35 (JIS S35CK) steels have been used as a material in fuel pump blocks for marine engines. Failures in the inner surface of a drilling hole, due to the initiation of fatigue cracks have been frequently reported. However, the mechanism initiating these cracks and growths has not been clearly diagnosed yet. This study was conducted using a scraped fuel pump block, containing an initiated fatigue crack in the inner surface of a drilling hole. Initially, the cracks and fractured surfaces inside the block were investigated using an optical microscope and a SEM (Scanning Electron Microscope). In addition, microstructure observation, fatigue life test and fatigue crack growth test were performed using a specimen, which was taken from the same block. Results from these tests are summarized as follows; (1) The early crack in the block was supposed to occur inside the inner surface of the drilling hole. (2) The fatigue endurance of this material was about 330 Mpa. (3) The early crack was generated in the cavitations created by the breakdown of a big inclusion, or separation between the big inclusion and the base metal, in which the fundamental ingredients of the inclusion were C, 5, and Mn. (4) In order to prevent these types of failures, the suppression of inclusions inflow by improving the casting process, formation of fine inclusions by applying a heat treatment process, and coating of the surface of the drilling hole were required.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.38 no.4
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• pp.401-407
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• 2014

In this paper, the effect of cohesive laws on the finite element analysis of crack propagation using cohesive elements is investigated through three-point bending and double cantilever beam problems. The cohesive elements are implemented into ABAQUS/Standard user subroutines(UEL), and the shape of cohesive law is varied by changing parameters in polynomial functions of cohesive traction-separation relations. In particular, crack propagation behaviors are studied by comparing load-displacement curves of the analysis models which have different shapes of cohesive laws with the same values of fracture energy and cohesive strength. Furthermore, the influence of the element size on crack propagation is discussed in this study.

• Journal of the Korean Geotechnical Society
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• v.19 no.2
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• pp.171-178
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• 2003

Wing and secondary cracks are unique types of cracks observed in rock masses subjected to uniaxial and biaxial compressive loading conditions. In this study, morphological features of wing and secondary cracks developed in gypsum specimens are investigated in the macro and micro scales. Along the path of wing crack, microtensile cracks are observed. Microtensile cracks coalesce with pores and show branch phenomenon. From the onset of the wing crack, multiple initiations of microtensile cracks are observed. Microtensile cracks show tortuous propagation paths and relatively constant aperture of the cracks during the propagation. It is shown that microtensile cracks propagate by splitting failure. At the micro scale, microfsults are observed in the path of the secondary cracks. Along the path of the secondary cracks, separation of grains and conglomerate grains, oblique microfaults, and irregular aperture of microfault are observed. These features show that the secondary cracks are produced in shear mode. The measured sizes of fracture process zone across the propagation direction near the tip of wing and secondary cracks range from 10$\mu{m}$ to 20$\mu{m}$ far wing cracks and from 100$\mu{m}$ to 200$\mu{m}$ for secondary cracks, respectively.

• Journal of the Korean Ceramic Society
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• v.29 no.6
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• pp.496-504
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• 1992

Alumina tubes suitable for the support of gas separation membranes have been prepared by the slipcasting technique. These supports have the average pore size of 0.1 ${\mu}{\textrm}{m}$ within the narrow distribution. The sol-gel dipcoating process of nanoparticulate sols is very sensitive to microstructure of the support, and the coating on the inside surface of the tube is found to be more successful than on the outside surface. Nanoparticulate silica sols (0.82 mol/ι) have been synthesized by an interfacial hydrolysis reaction between TEOS and high alkaline water. When coating an alumina tube with these sols, the minimum limits of the particle size and the aging time required for forming the coated gel layer at the given pH are provided. It is optimum to coat the support with less concentrated sols stabilized through aging for the appropriate time (more than 22 days) at the lower pH (pH 2.0) for producing a reproducible crack free thin film coating in composite membranes.

• Journal of the Korean Ceramic Society
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• v.25 no.1
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• pp.59-65
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• 1988

To develop porous glass membranes used for a effective membrane-separation process, porous glasses and glass membranes were prepared from the sodium borosilicate parent glass by the phaseseparation technique and effects of heat-treatment and leaching conditions on their characteristics were investigated. The crack-free glass membranes could be fabricated from the 9.4 Na2-O-30.7 B2O3-59.2 SiO2-0.7 Al2O3(wt%) parent glass by heat-treatment at the lower temperature(550-570$^{\circ}C$) and for longer than 45 hrs for the phase separation, followed by leaching with 3N-HCl＋60% ethylene glycol solution at 90$^{\circ}C$ over 25 hrs. Porous glasses prepared in this work showed large specific surface areas(400㎡/g) and narrow pore size distribution with the mean pore radius of 14${\AA}$ enough for the application as reverse osmosis membranes. The salt-rejection efficiency and product-flux of the glass membranes heat-treated at 570$^{\circ}C$ for 80 hrs were found to be 51.8% and 270cc/㎡. hr, respectively. This result suggests that the porous glass membranes fabricated in this study could be applied for the reverse osmosis process.

• Membrane Journal
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• v.20 no.1
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• pp.62-68
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• 2010

The powder mixture for fabricating the cermet membranes was prepared by mechanically mixing 60 vol.% vanadium with $Y_2O_3$-stabilized $ZrO_2$ (YSZ). The powder mixture was pressed into disks, which were then sintered in vacuum at $1600^{\circ}C$ for 2 h. As-sintered membrane was dense and mounted to a stainless steel ring with brazing filler. Hydrogen fluxes of V/YSZ membrane have been measured in the range of $200{\sim}350^{\circ}C$ with 100% $H_2$. The crack was formed in the both sides of membrane at $350^{\circ}C$ and pressure of 0.5 bar. During permeation experiment, vanadium of V/YSZ membrane reacted with hydrogen to form $V_2H$ which was the origin of crack formation.

• Fire Science and Engineering
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• v.25 no.4
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• pp.48-55
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• 2011

This paper presents the failure analysis of the rate of rise spot type heat detectors on artificially accelerated aging. The failures of heat detector turned out by two reasons. The first one is the separation of binder from plastic moulding, resulting in the leakage of air from heat chamber. The second reason is the crack of plastic. The large cracks were maybe created by these reasons, thermal expansion difference, mechanical stress, or growth of microcrack. In the sound detector, the separation and the crack were not occurred or not developed to the critical size. The glass fibers which increase the mechanical strength were added in the binder of detector 2010G. The densities of binder or plastic of each detector were similar. However, the TGA result shows that the thermal characteristics of 2005A and 2005B were not similar.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.24 no.6 s.177
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• pp.1547-1556
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• 2000

In this paper, an evaluation method of fracture toughness to apply interfacial fracture mechanics was investigated in adhesively bonded double-cantilever beam (DCB) joints. Four types of adhesively bonded DCB joints with an interface crack were prepared for analyses of the stress intensity factors using boundary element method(BEM) and the fracture toughness test. From the results of BEM analysis and fracture toughness experiments, it is found that the stress intensity factor, K1 is a parameter driving the fracture of adhesively bonded joints. Also, the evaluation method of fracture toughness by separated stress intensity factors of mixed mode cracks was proposed and the influences of mode components for its fracture toughness are investigated in adhesively bonded DCB joints.