• Title/Summary/Keyword: conventional curing

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Flip Chip Assembly Using Anisotropic Conductive Adhesives with Enhanced Thermal Conductivity

  • Yim, Myung-Jin;Kim, Hyoung-Joon;Paik, Kyung-Wook
    • Journal of the Microelectronics and Packaging Society
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    • v.12 no.1 s.34
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    • pp.9-16
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    • 2005
  • This paper presents the development of new anisotropic conductive adhesives with enhanced thermal conductivity for the wide use of adhesive flip chip technology with improved reliability under high current density condition. The continuing downscaling of structural profiles and increase in inter-connection density in flip chip packaging using ACAs has given rise to reliability problem under high current density. In detail, as the bump size is reduced, the current density through bump is also increased. This increased current density also causes new failure mechanism such as interface degradation due to inter-metallic compound formation and adhesive swelling due to high current stressing, especially in high current density interconnection, in which high junction temperature enhances such failure mechanism. Therefore, it is necessary for the ACA to become thermal transfer medium to improve the lifetime of ACA flip chip joint under high current stressing condition. We developed thermally conductive ACA of 0.63 W/m$\cdot$K thermal conductivity using the formulation incorporating $5 {\mu}m$ Ni and $0.2{\mu}m$ SiC-filled epoxy-bated binder system to achieve acceptable viscosity, curing property, and other thermo-mechanical properties such as low CTE and high modulus. The current carrying capability of ACA flip chip joints was improved up to 6.7 A by use of thermally conductive ACA compared to conventional ACA. Electrical reliability of thermally conductive ACA flip chip joint under current stressing condition was also improved showing stable electrical conductivity of flip chip joints. The high current carrying capability and improved electrical reliability of thermally conductive ACA flip chip joint under current stressing test is mainly due to the effective heat dissipation by thermally conductive adhesive around Au stud bumps/ACA/PCB pads structure.

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New Photopolymers Composed of Photoreactive Binder for Holographic Applications (I)

  • Choi, Dong-Hoon;Yoon, Han-Na;Yoon, Hyuk;Lee, Geon-Joon;Feng, De-jun;Kim, Jae-Hong;Paik, Sang-Hyun;Choi, Suk-Ho
    • 한국정보디스플레이학회:학술대회논문집
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    • 2003.07a
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    • pp.230-233
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    • 2003
  • New photopolymers were designed and prepared using the photosensitive polymer binders. The photochemical reaction of the photosensitive polymer binder was studied by virtue of UV absorption and infrared spectroscopy. The holographic gratings were successfully fabricated in these photopolymer film samples by conventional optical interference method. We also investigated the effect of photocrosslink in the polymer binder on the diffraction behavior of the photopolymer. The dynamic behaviors of the grating formation were studied with the change of exposure intensity in terms of the diffraction efficiency. Particularly, we focused our efforts to observe the variation of the diffraction efficiency during post UV curing process.

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Dielectric and Piezoelectric Properties of Alkaline Lead-free Piezoceramic-epoxy Composites (알칼리계 무연 압전 세라믹과 에폭시 복합소재의 유전 및 압전 특성)

  • Yoon, Chang-Ho;Le, Duc Thang;Heo, Dae-Jun;Ahn, Kyoung-Kwan;Lee, Jae-Shin
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.25 no.6
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    • pp.420-425
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    • 2012
  • Lead-free piezoelectric ceramic/epoxy composites with '0-3' connectivity were prepared by cold-pressing with a temperature controlled curing method. A ceramic powder with a composition of $(Na_{0.51}K_{0.47}Li_{0.02})(Nb_{0.8}Ta_{0.2})O_3$ was synthesized by a conventional solid state reaction route. The dielectric and piezoelectric properties of ceramic/epoxy composites were characterized as a function of the volume fraction (${\phi}$) of piezoelectric ceramics, which was varied from 70 to 95 vol%. The results indicated that the piezoelectric properties of composites were significantly affected by the volume fraction of ceramics. In terms of the piezoelectric properties, specimens showed the best performance at ${\phi}$= 85 vol%, resulting in the piezoelectric constant $d_{33}$ of 39 pC/N and the figure of merit as a piezoelectric energy harvester ($d_{33}{\cdot}g_{33}$) of 1.24 $pm^2/N$.

Polymerization Shrinkage and Stress of Silorane-based Dental Restorative Composite (Silorane-기질 치아 수복용 복합레진의 중합수축과 중합수축응력)

  • Lee, In-Bog;Park, Sung-Hwan;Kweon, Hyun-Jeong;Gu, Ja-Uk;Choi, Nak-Sam
    • Composites Research
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    • v.26 no.3
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    • pp.182-188
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    • 2013
  • The purpose of this study was to measure the volumetric polymerization shrinkage kinetics and stress of a silorane-based dental restorative composite and compare it with those of conventional methacrylate-based dental composites. Two methacrylate-based composites (Z250, Z350 flowable) and one silorane-based composite (P90) were investigated. The volumetric polymerization shrinkage of the composites during light curing was measured using a laboratory-made volume shrinkage measurement instrument based on the Archimedes' principle, and the polymerization stress was also determined with the strain gage method. The shrinkage of silorane-based composites (P90) was the lowest, and that of Z350 flowable was the highest. Peak polymerization shrinkage rate was the lowest in P90 and the highest in Z350 flowable. The time to reach peak shrinkage rate of P90 was longer than those of the methacrylate-based composites. The polymerization shrinkage stress of P90 was lower than those of the methacrylate-based composites.

Effect of accelerators with waste material on the properties of cement paste and mortar

  • Devi, Kiran;Saini, Babita;Aggarwal, Paratibha
    • Computers and Concrete
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    • v.22 no.2
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    • pp.153-159
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    • 2018
  • Accelerators are used to speed up the construction by accelerating the setting time which helps in early removal of formwork thus leading to faster construction rate. Admixtures are used in mortar and concrete during or after mixing to improve certain properties of material which cannot be achieved in conventional cement mortar and concrete. The various industrial by products make nuisance and are hazardous to ecosystem as well. These wastes can be used in the construction industries to reduce the consumption of cement/aggregates, cost; and save the energy and environment by utilising waste and eliminate their disposal problem as well. The effect of calcium nitrate and triethanolamine (TEA) as accelerators and marble powder (MP) as waste material on the various properties of cement paste and mortar has been studied in the present work. The replacement ratio of MP was 0-10% @ 2.5% by weight of cement. The addition of calcium nitrate was 0% and 1%; and variation of addition of TEA was 0-0.1@ 0.025% and 0.1-1.0@ 0.1% by weight of cement. On the basis of setting time, some mix proportions were selected and further investigated. Setting time and soundness of cement paste; compressive strength and microstructure of mortar mix of selected mix proportions were studied experimentally at 3, 7 and 28 days aging. Results showed that use of MP, calcium nitrate, TEA and their combination reduced setting time of cement paste for all the mixes. Addition of calcium nitrate increased the compressive strength at all curing ages while MP and TEA decreased the compressive strength. The mechanism of additives was discussed through scanning electron microscope (SEM) and energy dispersive X-ray spectroscopy (EDS) analysis of the specimens.

Evaluation of fitness according to application of glass fiber reinforcement for lower jaw complete denture (하악 총의치 전용의 유리섬유 보강재 적용에 따른 적합도 비교 분석)

  • Kim, Dong-Yeon;Park, Jin-Young;Bae, So-Yeon;Kang, Hoo-Won;Kim, Ji-hwan;Kim, Woong-Chul
    • Journal of Technologic Dentistry
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    • v.40 no.4
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    • pp.201-207
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    • 2018
  • Purpose: The purpose of this study is to evaluate the fitness of lower jaw compete denture with glass fiber. Methods: Lower jaw edentulous model was selected as the master model. Ten study models were produced using Type IV stone(n=10). Lower jaw trial dentures were produced by the wax denture base and artificial teeth. Conventional complete denture (CD) group was fabricated by excluding glass fiber reinforcement (n=5). Glass fiber complete denture (GD) group was fabricated with glass fiber reinforcement (n=5). The lower jaw trial complete denture was invested using a plaster. PMMA resin was injected and curing was performed. The CD and GD groups measured the fit using silicone replica technology. The measured data was verified by t-test. Results: The anterior area of the CD group showed the smallest value. There was a statistically significant difference in the anterior area of the CD group and the GD group (p<0.05), but there was no statistically significant difference in the posterior area (p>0.05). Conclusion : Complete denture with glass fiber showed low fitness and further study is needed to apply it clinically.

A new formulation for strength characteristics of steel slag aggregate concrete using an artificial intelligence-based approach

  • Awoyera, Paul O.;Mansouri, Iman;Abraham, Ajith;Viloria, Amelec
    • Computers and Concrete
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    • v.27 no.4
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    • pp.333-341
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    • 2021
  • Steel slag, an industrial reject from the steel rolling process, has been identified as one of the suitable, environmentally friendly materials for concrete production. Given that the coarse aggregate portion represents about 70% of concrete constituents, other economic approaches have been found in the use of alternative materials such as steel slag in concrete. Unfortunately, a standard framework for its application is still lacking. Therefore, this study proposed functional model equations for the determination of strength properties (compression and splitting tensile) of steel slag aggregate concrete (SSAC), using gene expression programming (GEP). The study, in the experimental phase, utilized steel slag as a partial replacement of crushed rock, in steps 20%, 40%, 60%, 80%, and 100%, respectively. The predictor variables included in the analysis were cement, sand, granite, steel slag, water/cement ratio, and curing regime (age). For the model development, 60-75% of the dataset was used as the training set, while the remaining data was used for testing the model. Empirical results illustrate that steel aggregate could be used up to 100% replacement of conventional aggregate, while also yielding comparable results as the latter. The GEP-based functional relations were tested statistically. The minimum absolute percentage error (MAPE), and root mean square error (RMSE) for compressive strength are 6.9 and 1.4, and 12.52 and 0.91 for the train and test datasets, respectively. With the consistency of both the training and testing datasets, the model has shown a strong capacity to predict the strength properties of SSAC. The results showed that the proposed model equations are reliably suitable for estimating SSAC strength properties. The GEP-based formula is relatively simple and useful for pre-design applications.

A Study on the Seismic Reinforcement of a Low-Rise Building Using Sinusoidal Corrugated Web Members (사인파형 웨브주름 보강재를 이용한 저층건물의 내진보강에 관한 연구)

  • Jung, Dong Jo;Kim, Jin
    • Journal of the Korean Institute of Rural Architecture
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    • v.24 no.2
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    • pp.13-20
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    • 2022
  • In this study, a general low-rise building was selected to compare the new shear wall reinforcement method, which is a general method among the existing reinforcement methods, and the reinforcement method using sinusoidal corrugated web reinforcement. And it was confirmed that the following effects can be expected. Sinusoidal corrugated web members can be carried out in a short period of time as it does not require the removal of the masonry filling wall, the reinforcement of reinforcing bars, and the curing period of the concrete. It is effective in preventing damage that may occur when masonry filling wall is overturned in the out-of-plane direction, and the burden of the foundation is also reduced, and thus the construction period and cost required for reinforcement can greatly be reduced. By adjusting the number of sinusoidal corrugated web member, details of joints, and reinforcement positions, the flow of load can be induced to have an advantageous effect on the building. It can be considered as the most suitable reinforcement plan in terms of life safety. Unlike the shear wall that fills between the columns, the sinusoidal corrugated web members, which has a width of 1.5m, can install openings between two columns depending on the purpose of use, and can be expected to have a great effect in terms of usability due to its free installation location. As mentioned above, the seismic reinforcement using a sinusoidal corrugated web members, can expect great effect compared to conventional reinforcement methods in terms of usability, economic feasibility, and stability.

Heavy-impact sound insulation performance according to the changes of dry flooring structure in wall structure

  • Cho, Jongwoo;Lee, Hyun-Soo;Park, Moonseo;Lim, Hohwan;Kim, Jagon
    • International conference on construction engineering and project management
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    • 2017.10a
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    • pp.89-98
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    • 2017
  • The floor heating method generally uses a wet construction method including the installation of resilient material, lightweight foam concrete, heating piping, and finishing mortar. Such a wet construction method not only delays other internal finishing processes during curing period for two mortar pouring process, but also has a disadvantage that it is difficult to replace the floor heating layer when it deteriorated because it is integrated with the frame. Dry floor heating construction method can be a good alternative in that it can solve these defects. Conversely, when it applied to the wall structure that is vulnerable to the interlayer noise compared with the column-beam structure, the question about the heavy-impact sound(HIS) insulation performance is raised. Therefore, conventional dry floor heating method is hard to apply to the wall structure apartments. Therefore, for the purpose to improve the applicability of dry floor heating method in wall structure apartments, this study investigated the change of floor impact sound, especially HIS insulation performance which is one of the required performance for the floor structure. This study tried to examine whether the change of heavy-impact sound pressure level(SPL) shows a tendency at the significant level according to the shape and mass of the floor structure. Through filed experiments on wall structure apartment, this study confirmed that the form of the raised floor shows better HIS insulation performance than the fully-supported form. In addition, it was also confirmed that the HIS insulation performance increases with the mass on the upper part. Moreover, this study found the fact that a mass of about 30 kg/m2 or more should be placed on the upper structure to reduce the heavy-impact SPL according to the bang machine measuring method. Although this study has a limit due to insufficient experiment samples, if the accuracy of this study is increased, it will contribute to the diffusion of dry floor heating by setting the HIS insulation performance target and designing the dry floor heating structure that meets the target.

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Comparison between a bulk-fill resin-based composite and three luting materials on the cementation of fiberglass-reinforced posts

  • Carlos Alberto Kenji Shimokawa ;Paula Mendes Acatauassu Carneiro ;Tamile Rocha da Silva Lobo;Roberto Ruggiero Braga ;Miriam Lacalle Turbino;Adriana Bona Matos
    • Restorative Dentistry and Endodontics
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    • v.48 no.3
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    • pp.30.1-30.11
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    • 2023
  • Objectives: This study verified the possibility of cementing fiberglass-reinforced posts using a flowable bulk-fill composite (BF), comparing its push-out bond strength and microhardness with these properties of 3 luting materials. Materials and Methods: Sixty endodontically treated bovine roots were used. Posts were cemented using conventional dual-cured cement (CC); self-adhesive cement (SA); dual-cured composite (RC); and BF. Push-out bond strength (n = 10) and microhardness (n = 5) tests were performed after 1 week and 4 months of storage. Two-way repeated measures analysis of variance (ANOVA), 1-way ANOVA, t-test, and Tukey post-hoc tests were applied for the push-out bond strength and microhardness results; and Pearson correlation test was applied to verify the correlation between push-out bond strength and microhardness results (α = 0.05). Results: BF presented higher push-out bond strength than CC and SA in the cervical third before aging (p < 0.01). No differences were found between push-out bond strength before and after aging for all the luting materials (p = 0.84). Regarding hardness, only SA presented higher values measured before than after aging (p < 0.01). RC and BF did not present 80% of the maximum hardness at the apical regions. A strong positive correlation was found between the luting materials' push-out bond strength and microhardness (p < 0.01, R2 = 0.7912). Conclusions: The BF presented comparable or higher push-out bond strength and microhardness than the luting materials, which indicates that it could be used for cementing resin posts in situations where adequate light curing is possible.