• 제목/요약/키워드: conventional curing

검색결과 269건 처리시간 0.029초

도자기 복원에 사용되는 에폭시계 고분자수지의 요구 특성 연구 (Study on the Demand Characteristics of Epoxy Resins Applied to the Restoration of Ceramics)

  • 남병직;정세리;장성윤
    • 접착 및 계면
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    • 제13권4호
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    • pp.171-181
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    • 2012
  • 본 연구는 도자기 복원용 에폭시수지 12종을 대상으로 복원제로서의 요구 특성(내구성, 가공성, 광택특성, 수축 팽창특성)을 조사한 후, 이를 통해 효과적인 재료 선택의 기준을 제시하고자 하였다. 내구성 분석결과 액상형은 비교적 손상 정도가 적고 재질 강도가 높은 도자기 유물에, 페이스트형은 상대적으로 손상 정도가 심하고 재질 강도가 약한 토기 유물에 적용하는 것이 보다 효과적이다. 가공성 분석결과 액상형은 페이스트형보다 높은 표면경도를 보였고, 액상형 중에서는 일반경화형이 속경화형보다 표면경도가 높았다. 따라서 높은 표면경도로 재가공이 어려운 액상형은 향후 첨가제 혼합을 통한 물성 개선이 필요하다. 광택특성 분석결과 외관상 무색투명한 액상형이 페이스트형보다 높은 광택도를 보였고, 액상형 중에서는 일반경화형이 속경화형보다 광택도가 높았다. $700^{\circ}C$ 연질토기는 페이스트형 중 CDK-520A/520B와 Araldite SV 427-2/HV 427-1이, 청자와 백자는 액상형 중 Devcon 5 minute과 EPO-TEK 301-2, 페이스트형 중 Quik Wood가, 분청사기는 페이스트형 중 Quik Wood, 액상형 중 EPO-TEK 301-2와 Devcon 5 minute이 대상 도자기의 광택도에 가장 근접하였다. 수축 팽창특성 분석결과 에폭시수지의 대부분은 경화 중 부피 변화가 발생하였으므로, 수축 팽창률에 따른 복원면의 증감을 사전에 예측하여 형태복원 범위를 설정하여야 한다.

카올린-시멘트 혼합재료의 공학적 특성 (Mechanical Characteristics of Kaolin-cement Mixture)

  • Lee, Kyu-Hwan;Lee, Song;Yi, Chang-Tok
    • 한국지반공학회논문집
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    • 제18권1호
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    • pp.113-125
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    • 2002
  • 연약 지반개량을 위한 심층혼합처리 공법의 사용은 점차로 증가 추세에 있으며 특히, 일본과 해안가에 인접한 동남아 국가는 물론 스칸디나비아지역에서도 보편화된 개량공법으로 각광을 받고 있다. 시멘트는 지반의 강도를 증가시키고 압축성을 감소시키는 역할을 한다. 따라서 심도가 깊은 퇴적지반이나 해안지역에서 지반의 지지력 증가나 압밀침하를 감소시키기 위해 시멘트를 개량재료로 사용할 수가 있다. 연약지반 처리를 위한 고화제로서 시멘트의 사용이 증가하고 있음에도 불구하고 이에 대한 응력-변형특성이나 혼합처리 흙의 구조적인 특성 등의 역학적인 거동특성을 명확하게 파악하지 못하고 있다. 본 연구에서는 시멘트 고화처리 흙의 역학적 성질을 파악하기 위해 카올린을 이용하여 최대 10%의 시멘트를 첨가하여 7일에서 112일가지 양생기간을 변화시켜 삼축압축시험, 일축압축시험, 등방압밀 및 표준압밀시험등을 수행하였으며 이에 따른 시멘트 고화처리 흙의 역학적인 특성을 파악하고자 하였다. 또한 혼합토의 시료 제조 및 양생방법등 일련의 시험과정에 대한 절차 및 방법에 대하여 기술하였다.

Determination of Epoxy/Anhydride Mixing Ratio for the Highly Silica Filled Compounds with Chromium (III) Octoate Catalyst

  • Lee, Noori;Lee, Dong-Hoon;Lee, Jung Hoon;Min, Kyeong-sik;Kang, Sung Yun;Seo, Seungkil;Rho, Byung Lae;Kim, Wonho
    • Elastomers and Composites
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    • 제50권2호
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    • pp.103-109
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    • 2015
  • In this study, epoxy/anhydride mixing ratio for the highly silica filled compounds with chromium (III) octoate catalyst was investigated at a low curing temperature ($71^{\circ}C$ for 40 hr) by evaluating the compressive strength with the weight ratio ranges from 0.3/1.0 to 1.0/1.0 of epoxy part (Part A)/anhydride part (Part B). In case of epoxy/anhydride compounds used surface unmodified silica by coupling agent, these compounds need excess anhydride unlike the weight ratio in the conventional epoxy/anhydride compounds. In curing behavior, the epoxy/anhydride compounds containing chromium (III) octoate showed high conversions at $71^{\circ}C$ for 40 hr, even if a dipropylene glycol (DPG) was not used as a polymerization initiator. Also, DPG leads to a poor epoxy network structure. In conclusion, the appropriate weight ratio of Part A/Part B of highly silica filled epoxy/anhydride compounds with chromium (III) octoate catalyst is 0.5/1.0 and the maximum amounts of silica is 1470 phr of epoxy resin.

LED를 이용한 복합레진의 광조사시, 중합수축의 속도와 양, 미세경도에 관한 연구 (THE AMOUNTS AND SPEED OF POLYMERIZATION SHRINKAGE AND MICROHARDNESS IN LED CURED COMPOSITES)

  • 박성호;김수선;조용식;이순영;김도현;장용주;문현승;서정원;노병덕
    • Restorative Dentistry and Endodontics
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    • 제28권4호
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    • pp.354-359
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    • 2003
  • This study evaluated the effectiveness of the light emitting diode(LED) units for composite curing. To compare its effectiveness with conventional quartz tungsten halogen (QTH) light curing unit. the microhardness of 2mm composite. Z250, which had been light cured by the LEDs (Ultralume LED2, FreeLight, Developing product Dl) or QTH (XL 3000) were compared on the upper and lower surface. One way ANOVA with Tukey and Paired t-test was used at 95% levels of confidence. In addition. the amount of linear polymerization shrinkage was compared between composites which were light cured by QTH or LEDs using a custom-made linometer in 10s and 60s of light curing, and the amount of linear polymerization shrinkage was compared by one way ANOVA with Tukey. The amount of polymerization shrinkage at 10s was XL3000 > Ultralume 2. 40. 60 > FreeLight, D1 (P<0.05) The amount of polymerization shrinkage at 60s was XL3000 > Ultralume 2, 60> Ultralume 2.40 > FreeLight, D1 (P<0.05) The microhardness on the upper and lower surface was as follows ; (equation omitted) It was concluded that the LEDs produced lower polymerization shrinkage in 10s and 60s compared with QTH unit. In addition. the microhardness of samples which had been cured with LEDs was lower on the lower surfaces than the upper surfaces whereas there was no difference in QTH cured samples.

초박형 반도체 패키지의 EMC encapsulation을 위한 경화 공정 개발 (Development of Curing Process for EMC Encapsulation of Ultra-thin Semiconductor Package)

  • 박성연;온승윤;김성수
    • Composites Research
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    • 제34권1호
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    • pp.47-50
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    • 2021
  • 본 논문은 차량에 사용되는 B필러의 강화재를 기존의 스틸 소재에서 CFRP(Carbon Fiber Reinforced Plastics)와 GFRP(Glass Fiber Reinforced Plastics)로 대체하여 경량화하는 것이 목표다. 이를 위해서는 무게는 감소시키면서 기존 B필러를 대체할 수 있는 구조안정성을 확보해야 한다. 기존 B필러는 스틸 아우터(outer)를 포함하여 다양한 형상의 스틸 강화재로 구성되며, 이와 같은 스틸 강화재 중 2가지의 스틸 강화재를 복합재로 대체하고자 한다. 이와 같은 스틸 강화재는 강화재 각각을 따로 제작하여 용접을 통해 결합되지만, 복합재 강화재는 패치(patch) 형태의 CFRP와 리브(rib) 구조의 GFRP를 활용하여 압축과 사출 공정을 통해 한번에 제작된다. CFRP는 B필러의 고강도부에 부착되어 측면 하중에 저항하도록 하였으며, GFRP 리브는 위상 최적화(Topology optimization) 기법을 통해 비틀림과 측면 하중을 저항하도록 설계하였다. 구조해석을 통해 기존 스틸 강화재와 비교 분석을 수행하였고, 경량화율을 산출하였다.

Technology to reduce water ingress for TBM cutterhead intervention

  • Ham, Soo-Kwon;kim, Beom-Ju;Lee, Seok-Won
    • Geomechanics and Engineering
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    • 제29권3호
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    • pp.321-329
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    • 2022
  • Tunnel site where high water pressure is applied, such as subsea tunnel, generally selects the shield TBM (Tunnel Boring Machine) to maintain the tunnel excavation face. The shield TBM has cutters installed, and the cutters wear out during the process of excavation, so it should be checked and replaced regularly. This is called CHI (Cutterhead Intervention). The conventional CHI under high water pressure is very disadvantageous in terms of safety and economics because humans perform work in response to high water pressure and huge water inflow in the chamber. To overcome this disadvantage, this study proposes a new method to dramatically reduce water pressure and water ingress by injecting an appropriate grout solution into the front of the tunnel face through the shield TBM chamber, called New Face Grouting Method (NFGM). The tunnel model tests were performed to determine the characteristics, injection volume, and curing time of grout solution to be applied to the NFGM. Model test apparatus was composed of a pressure soil tank, a model shield TBM, a grout tank, and an air compressor to measure the amount of water inflow into the chamber. The model tests were conducted by changing the injection amount of the grout solution, the curing time after the grout injection, and the water/cement ratio of grout solution. From an economic point of view, the results showed that the injection volume of 1.0 L, curing time of 6 hours, and water/cement ratio of the grout solution between 1.5 and 2.0 are the most economical. It can be concluded that this study has presented a method to economically perform the CHI under the high water pressure.

Effects of Dongchimi Powder as a Natural Nitrite Source on Quality Properties of Emulsion-Type Sausages

  • Su Min Bae;Da Hun Jeong;Seung Hwa Gwak;Seonyeong Kang;Jong Youn Jeong
    • 한국축산식품학회지
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    • 제43권3호
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    • pp.502-511
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    • 2023
  • The use of nitrite as a conventional curing agent is decreasing because of the negative consumer perception of synthetic compounds in foods. Therefore, this study was conducted to investigate the efficacy of dongchimi as an alternative to synthetic nitrite and its effect on the qualitative properties of emulsion-type sausages. Under all tested fermentation conditions, both nitrite and nitrate contents were the highest when dongchimi was fermented at 0℃ for 1 wk. The fermented dongchimi was powdered and added to the sausages. Emulsion-type sausages were prepared with 0.25% (treatment 1), 0.35% (treatment 2), 0.45% (treatment 3), or 0.55% (treatment 4) dongchimi powder, with 0.01% sodium nitrite-treated (control 1) and 0.40% celery powder-treated (control 2) sausages as controls. There were not different (p>0.05) in the pH, cooking yield, CIE L*, and CIE a* between the control 1 and treatments 2, 3, and 4. CIE b* was significantly higher (p<0.05) in the control 2 and lower (p<0.05) in the control 1 than that in the other groups. Treatment 4 and control 1 had similar contents of residual nitrite, nitrosyl hemochrome, and total pigment. Additionally, treatment 4 exhibited a significantly better (p<0.05) curing efficiency than the control 1. However, naturally cured sausages showed higher (p<0.05) lipid oxidation than the control 1. This study suggests that the use of more than 0.35% dongchimi powder could replace sodium nitrite or celery powder as curing agents for emulsion-type sausages.

Methyl Methacrylate(MMA)계 도로보수재의 기초 물성 평가 (Evaluation of Basic Properties of Methyl Methacrylate (MMA) as a Road Repair Material)

  • 최병철;김규용;편수정;지성준;유하민;남정수
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2023년도 가을학술발표대회논문집
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    • pp.109-110
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    • 2023
  • Domestic ultra-hard road repair materials require a lot of time before the road can be opened to traffic. Therefore, in this study, Methyl Methacrylate (MMA) based road repair material was used to improve the above problems. Furthermore, the basic physical properties of MMA-based pavement repair materials are examined to confirm their suitability in concrete pavements. For this study, two types of MMA road repair materials (A type and B type) were selected. Then, the curing of the test specimens prepared for painting was carried out under three conditions. The experimental items were viscosity (drop time) and drying time (set to touch, dry-hard). As a result of the experiment, viscosity (drop time) was faster in type A than in type B. The drying time results were as follows. In the case of set ti touch, both type A and type B dried in about 10 minutes regardless of the curing conditions. In the case of dry-hard, regardless of the curing conditions, A type dried longer than B type, but it dried faster than conventional road repair materials. Therefore, within the scope of this study, it is considered that A type has a high potential for utilization as a road repair material.

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Corrosion Behavior of Cr-bearing Corrosion Resistant Rebar in Concrete with Chloride Ion Content

  • Tae, Sung Ho
    • Architectural research
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    • 제7권1호
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    • pp.49-54
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    • 2005
  • Conventional studies have focused on the reduction in the water-cement ratio, the use of various admixtures, etc., to ensure the durability of reinforced concrete structures against such deterioration factors as carbonation and chloride attack. However, improvement in the concrete quality alone is not considered sufficient or realistic for meeting the recent demand for a service life of over 100 years. This study intends to improve the durability of reinforced concrete structures by improvement in the reinforcing steel, which has remained untouched due to cost problems, through subtle adjustment of the steel components to keep the cost low. As a fundamental study on the performance of Cr-bearing rebars in steel reinforced concrete structures exposed to corrosive environments, The test specimens were made by installing 8 types of rebars in concretes with a chloride ion content of 0.3, 0.6, 1.2, 2.4 and $24kg/m^3$. Corrosion accelerated curing were then conducted with them. The corrosion resistance of Cr-bearing rebars was examined by measuring crack widths, half-cell potential, corrosion area and weight loss after 155 cycles of corrosion-accelerating curing. The results of the study showed that the corrosion resistance increased as the Cr content increased regardless of the content of chloride ions, and that the Cr-bearing rebars with a Cr content of 5% and 9% showed high corrosion resistance in concretes with a chloride ion content of 1.2 and $2.4kg/m^3$, respectively.

가변성형기술을 활용한 항공기 윙렛용 몰드 제작에 관한 수치적 연구 (Numerical Study of Aircraft Winglet Mold Manufacturing using Flexible Forming)

  • 박지우;구태완;김정;강범수
    • 소성∙가공
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    • 제23권8호
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    • pp.482-488
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    • 2014
  • Flexible forming technology has advantages in sheet metal forming, because it can be implemented to produce various shaped molds using a single apparatus. Due to this advantage, it is possible to apply it to the manufacture of an aircraft winglet mold. Presently, most aircraft winglets are manufactured from composite materials. Therefore, the mold for the curing process is an essential element in the fabrication of such composite materials. Compared to conventional mold forming, flexible forming has some advantages such as reduced manufacturing cost and uniformity of mold thickness. If the thickness of the mold is consistent, then the heat transfer will occur uniformly during the curing process leading to improved formability of the composite material. In the current study, numerical simulations were performed to investigate the possibility of flexible forming for manufacturing of the winglet mold. In order to match the size of the actual product, the shape of objective surface was divided to fit the dimensions of the apparatus. The results from the numerical simulations are compared with the objective surface to verify the accuracy. In conclusion, the current study confirms the feasibility and the potential to manufacture winglet molds by flexible forming.