• Title/Summary/Keyword: contact angle test

Search Result 355, Processing Time 0.024 seconds

Interfacial Adhesion Properties of Surface Treated Polyarylate Fiber with Polyethylene Naphthalate (폴리아릴레이트 섬유의 표면처리에 의한 폴리에틸렌 나프탈레이트 수지와의 계면접착특성)

  • Yong, Da Kyung;Choi, Han Na;Yang, Ji Woo;Lee, Seung Goo
    • Journal of Adhesion and Interface
    • /
    • v.13 no.1
    • /
    • pp.24-30
    • /
    • 2012
  • Morphological changes of polyarylate (PAR) fiber treated with formic acid and ultraviolet (UV) were observed by using a scanning electron microscope (SEM) and an atomic force microscope (AFM). The results were analysed by using root mean square (RMS) roughness. In addition, the chemical changes of surface was investigated using contact angle and the interfacial adhesive strength between PAR fiber and PEN (Polyethylene naphthalate) matrix was calculated using the Pull-out test results. As the acid treatment concentration and UV irradiation time increased, cracks and pores were produced on the PAR fiber surface. Due to the roughness increased, the contact angle was decreased. For this reason, RMS roughness of PAR fiber was increased and the interfacial adhesive strength between the PAR fiber and PEN matrix was improved. The increase of interfacial adhesive strength was responsible for the increase of surface area which have cracks and pores.

Microstructure Analysis of Cement Composite containing PMHS Emulsion to Improve Hydrophobic (소수성 증진을 위한 PMHS 유액 혼입 시멘트 복합체의 미세구조 분석)

  • Kim, Younghwan;Oh, Hongseob
    • Journal of the Korea institute for structural maintenance and inspection
    • /
    • v.25 no.1
    • /
    • pp.25-32
    • /
    • 2021
  • For developing the durable eco-concrete, water-repellent and hydrophobic emulsion were prepared by stirring and mixing polymethyl hydrosiloxane and polyvinyl alcohol. After adding the PMHS emulsion cement paste, the hydration reaction characteristics and the change in chemical composition were analyzed through BSE and EDS analysis, and the micropores were evaluated by MIP test. Cement mixed with PMHS emulsion was analyzed to increase the hydration reactivity and to decrease the capillary porosity, but it was found that the capillary porosity varies depending on the degree of dispersion of the emulsion in the cement paste. In the case of the emulsion containing metakaolin, there was little difference in hydration degree and porosity from the case of using only the PMHS emulsion. However, when the cement surface was coated with PMHS emulsion, the contact angle was found to increase significantly compared to OPC, and it was analyzed that especially when PVA fiber was used together, it changed to a hypohydrophobic surface.

Hydrophobicity and Adhesion Evaluation of MWCNT/Teflon-polyurethane Topcoat for Aircraft with Different MWCNT Coating Times (탄소나노튜브 코팅횟수에 따른 항공기용 탄소나노튜브/테프론-폴리우레탄 탑코트의 표면소수성 및 부착력 평가)

  • Lee, Jae-Hyuk;Kim, Jong-Hyun;Park, Joung-Man
    • Composites Research
    • /
    • v.35 no.2
    • /
    • pp.80-85
    • /
    • 2022
  • This work presents an experiment study to evaluate the nanoparticle adhesion and surface hydrophobicity characteristics of Teflon-polyurethane top coat depending on the number of multi-wall carbon nanotube (MWCNT) coatings, which is a carbon-based hydrophobic particle. In order to measure the adhesion between the nanoparticles and the top coat, adhesion pull-off test was performed with different MWCNT oxidation times. Static contact angle and roughness measurements were carried out to characterize the surface hydrophobic behavior. Through the roughness evaluation, it was confirmed that the carbon nanotubes were wetted in the Teflon-polyurethane top coat, and the degree carbon nanotube wetting was confirmed through a USB-microscope. As a result, it was found that the larger the degree of wetting, the better the adhesion. From the experimental results, as the hydrophobicity of Teflon-polyurethane increased, the adhesive propertydecreased with the number of coatings. It was possible to improve the adhesive force and determine the number of coatings of carbon nanotubes with optimized hydrophobicity.

Development of Laser Processing Technology and Life Evaluation Method for Lifespan Improvement of Titanium Superhydrophobic Surface (티타늄 초소수성 표면의 수명 향상을 위한 레이저 처리 기법 개발 및 내수명성 평가법 개발)

  • Kyungeun Jeong;Kyeongryeol Park;Yong Seok Choi;Seongmin Kang;Unseong Kim;Song Yi Jung;Kyungjun Lee
    • Tribology and Lubricants
    • /
    • v.40 no.3
    • /
    • pp.91-96
    • /
    • 2024
  • Recently, extensive studies have been carried out to enhance various performance aspects such as the durability, lifespan, and hardness by combining diverse materials or developing novel materials. The utilization of superhydrophobic surfaces, particularly in the automotive, textile, and medical device industries, has gained momentum to achieve improved performance and efficiency. Superhydrophobicity refers to a surface state where the contact angle when water droplets fall is above 150°, while the contact angle during sliding motion is smaller than 10°. Superhydrophobic surfaces offer the advantage of water droplets not easily sliding off, maintaining a cleaner state as the droplets leave the surface. Surface modification involves two fundamental steps to achieve superhydrophobicity: surface roughness increase and surface energy reduction. However, existing methods, such as time-consuming processes and toxic organic precursors, still face challenges. In this study, we propose a method for superhydrophobic surface modification using lasers, aiming to create roughness in micro/nanostructures, ensuring durability while improving the production time and ease of fabrication. The mechanical durability of superhydrophobic samples treated with lasers is comparatively evaluated against chemical etching samples. The experimental results demonstrate superior mechanical durability through the laser treatment. Therefore, this research provides an effective and practical approach to superhydrophobic surface modification, highlighting the utility of laser treatment.

Effects of McConnell Taping and Kinesio Taping on Pain and Lower Extremity Joint Angles During Stair Ascent in People with Patellofemoral Pain Syndrome (McConnell 테이핑과 Kinesio 테이핑이 무릎넙다리통증증후군 환자의 계단 올라가기 시 통증과 다리관절 각도에 미치는 영향)

  • Yoon, Sam-won;Son, Ho-hee
    • PNF and Movement
    • /
    • v.20 no.2
    • /
    • pp.189-201
    • /
    • 2022
  • Purpose: The purpose of this study was to investigate the effect of McConnell taping and Kinesio taping on pain and lower extremity joint angles when patients with patellofemoral pain syndrome (PFPS) ascend stairs. Methods: Fifty young adults who were experiencing anterior knee pain due to PFPS were selected as participants. Then, 25 patients were randomly assigned to the McConnell taping group and 25 to the Kinesio taping group. Pain and lower extremity joint angle were measured while ascending stairs before and after the intervention. A paired t-test was performed to evaluate the amount of change in the parameter values after the intervention within the groups, and an independent t-test was used to compare the results of the groups. Results: In the within-group comparisons, a statistically significant difference was found in both groups between the anterior knee pain scale scores recorded before and after the intervention (p < 0.05). A statistically significant difference was also found between the groups (p < 0.05). Comparison of the lower extremity joint angles at initial contact, loading response, terminal stance, and pre-swing within the groups showed that there were statistically significant differences in the hip, knee flexion, abduction, lateral rotation, and dorsiflexion angles in both the McConnell and Kinesio taping groups (p < 0.05). There was also a statistically significant difference in all angles between the groups during the following events (p < 0.05): (1) at initial contact, (2) at loading response (except hip flexion angle), (3) at terminal stance (except hip flexion and lateral rotation angles), and (4) at pre-swing (except hip, knee abduction, and inversion angles). Conclusion: McConnell taping and Kinesio taping both effectively improved the occurrence of knee pain and the lower extremity joint angles during stair ascent in patients with PFPS. However, McConnell taping had a significant impact on pain reduction and lower extremity joint angles compared to Kinesio taping.

Analysis of Occlusal Contacts Using Add-picture Method (Add-picture 방법을 이용한 교합접촉점 분석)

  • Park, Ko-Woon;Cho, Lee-Ra;Kim, Dae-Gon;Park, Chan-Jin
    • Journal of Dental Rehabilitation and Applied Science
    • /
    • v.29 no.1
    • /
    • pp.45-58
    • /
    • 2013
  • The purpose of this study was to analyze the area of occlusal contact points using visual method. One subject was selected who had Angle Class I, normal dentition, without dental caries, periodontal disease and temporomandibular disorders. Forty times PVS impressions were taken and 10 pairs casts were fabricated using dental super hard stone. After mounting the casts with customized loading apparatus, 78.9kg/f force was loaded as a maximum biting force. In T-Scan method, occlusal contact points measurement was repeated twice. Then, using Photoshop program (Adobe photoshop CS3, Adobe. San Jose, USA), the pixels which indicated occlusal contact points by color was recognized, and the distribution of recognized pixels were calculated to area. In Add picture method, polyether bite material applied to the occlusal surface of the casts. Then, the image of the translucent areas was recorded and classified $0{\sim}10{\mu}m$, $0{\sim}30{\mu}m$, $0{\sim}60{\mu}m$ area by the amount of transmitted light. To acquire occlusal surface, the numbers of pixels from the photograph of the contact area indicated cast converted to $mm^2$. The mean occlusal contact area by two methods was statistically analyzed (paired t-test). Part of the red and pink area in T-Scan image were almost equivalent to the $0{\sim}10{\mu}m$, $0{\sim}30{\mu}m$, $0{\sim}60{\mu}m$ area in Add picture image. The distribution of occlusal contact points were similar, but the average area of occlusal contact points was wider in T-scan image (P<.05). Pink and red area in T-scan image was wider than $0{\sim}10{\mu}m$, $0{\sim}30{\mu}m$ area in Add picture image (P<.05), but similar to $0{\sim}60{\mu}m$area in Add picture image (P>.05). Occlusal contact points in T-scan image did not indicate real occlusal contact points. Occlusal contact areas in T-scan method were enlarged results comparing with those in Add picture method.

Evaluation of Dynamic Characteristics of Slipmeters with Force Platform (하중판을 이용한 미끄러짐 측정기의 동력학적 특성 평가)

  • Kim, Jung-Soo
    • Journal of the Korean Society of Safety
    • /
    • v.27 no.5
    • /
    • pp.1-8
    • /
    • 2012
  • The purpose of this study were to evaluate the dynamic characteristics of the portable slipmeters with respect to actual slipping and to compare their output with those of force platform. The selected slipmeters were commonly used devices for slipperiness measurement in situ floors. Their output quantity represented force (BOT-3000), loss of energy(British pendulum striker) and angle of inclination(English XL). The validity of these devices was studied with respect to actual slipping using a force platform. The precision of these devices was also evaluated with force platform. Based on dynamics of human subject behavior when slipping during normal walking, the all devices tested in this study showed poor performances: low built up ratio, low normal pressure, and long contact time prior to slip. Nevertheless, their results reasonably correlated with those calculated from the ground reaction forces generated by the operation of the selected slipmeters on the force platform although the absolute values of COF from these three devices could be quite different. Also the results showed good repeatability under the some test conditions.

The Effect of 8 Weeks Athletics Class on Sprint Start Motion (8주 동안의 육상 교양수업 참여가 단거리 스타트 동작에 미치는 영향)

  • Lee, Jin-Taek
    • Korean Journal of Applied Biomechanics
    • /
    • v.24 no.3
    • /
    • pp.209-216
    • /
    • 2014
  • The purpose of this study was to explore the effect of 8 weeks after school classes of track sports on students' start motion through kinematic variables. 30 students in D National university of education participated for this study. These students divided into two groups, 17 students for experimental group and 13 students for control group. The two groups participated in general athletic class as common class, and the experimental group participated in after school class additionally. The general class taught track and jump skill for 3 hours a week, and the after school class taught only athletic running skill for 30 minutes a week. Pre and post test assessed to assess students' kinematic changes. Findings indicated that velocity and step rate were increased, and contact time, step length, displacement of center of mass were decreased in the experimental group. In the control group, early velocity, knee/hip angle velocity were increased, and contact time, step length, displacement of center of mass were decreased. In conclusion, the students who only participated in general class, could not maintain athletic skills obtained from the class. However, students who participated in both general and after school class accomplish athletic start skill. This is because Continuous learning effect helped students keep the skill and did not lose the skill. Thus, in order for students to learn specific sport skills, joining after school class with general class together is recommended.

Amino-Functionalized Alkylsilane SAM-Assisted Patterning of Poly(3-hexylthiophene) Nanofilm Robustly Adhered to SiO2 Substrate

  • Pang, Ilsun;Boo, Jin-Hyo;Sohn, Honglae;Kim, Sung-Soo;Lee, Jae-Gab
    • Bulletin of the Korean Chemical Society
    • /
    • v.29 no.7
    • /
    • pp.1349-1352
    • /
    • 2008
  • We report a novel patterning method for a homo-polymeric poly(3-hexylthiophene) (P3HT) nanofilm particularly capable of strong adhesion to a $SiO_2$ surface. An oxidized silicon wafer substrate was micro-contact printed with n-octadecyltrichlorosilane (OTS) monolayer, and subsequently its negative pattern was selfassembled with three different amino-functionalized alkylsilanes, (3-aminopropyl)trimethoxysilane (APS), N- (2-aminoethyl)-3-aminopropyltrimethoxy silane (EDAS), and (3-trimethoxysilylpropyl) diethylenetriamine (DETAS). Then, P3HT nanofilms were selectively grown on the aminosilane pre-patterned areas via the vapor phase polymerization method. To evaluate the adhesion, patterning, and the film itself, the PEDOT nanofilms and SAMs were investigated with a $Scotch^{(R)}$ tape test, contact angle analyzer, ATR-FT-IR, and optical and atomic force microscopes. The evaluation showed that the newly developed all bottom-up process can offer a simple and inexpensive patterning method for P3HT nanofilms robustly adhered to an oxidized Si wafer surface by the mediation of $FeCl_3$ and amino-functionalized alkylsilane SAMs.

Fabrication of Hydrophilic Poly(dimethylsiloxane)with Periodic Wrinkling Surface and Its Application (일정한 주름을 갖는 친수성 PDMS 제작 및 응용)

  • Lee, Dong-Guk;Oh, Chang-Kyu;Yang, Sung-Ho;Han, Seung-Jin;Jeong, Ok-Chan
    • The Transactions of The Korean Institute of Electrical Engineers
    • /
    • v.63 no.5
    • /
    • pp.671-675
    • /
    • 2014
  • This paper presents a fabrication of hydrophilic Poly(dimethylsiloxane) (PDMS) with periodic wrinkling surface. The proposed periodic wrinkling surface was fabricated using the sequential processes of typical curing process of PDMS, cutting process, platinum deposition process, and wrinkling transfer process. The surface morphology of the fabricated wrinkling surface was observed by using optical and dynamic atomic force microscopy and discussed. The measured period and amplitude of wrinkling was about $2.2{\mu}m$ and $0.31{\mu}m$, respectively. And, the contact angles of water droplets on the wrinkled surface were measured in order to understand effect of the wrinkling surface on surface modification of hydrophobic PDMS. Our new finding was that the proposed wrinkling surface was hydrophilic and the measured contact angle was about $62^{\circ}$. Moreover, it was found out from the simple cell culture test that the fabricated wrinkling surface was more effective for cell spreading and adhesion than the case of native PDMS substrate.