• Title/Summary/Keyword: consolidation process

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Dielectric Properties of Al2O3 Thick Films Grown by Aerosol Deposition Method (에어로졸 데포지션법으로 성막된 Al2O3 후막의 유전특성)

  • Park, Jae-Chang;Yoon, Young-Joon;Kim, Hyo-Tae;Koo, Eun-Hae;Nam, Song-Min;Kim, Jong-Hee;Shim, Kwang-Bo
    • Journal of the Korean Ceramic Society
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    • v.45 no.7
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    • pp.411-417
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    • 2008
  • Aerosol Deposition Method (ADM) is a novel technique to grow ceramic thick films with high density and nano-crystal structure at room temperature. $^{1,2)}$ For these unique advantages of ADM, it would be applied to the fabrication process of 3-D integration ceramic modules effectively. However, it is critical to control the properties of starting powders, because a film formation through ADM is achieved by impaction and consolidation of starting powders on the substrates. We fabricated alumina thick films by ADM for the application to integral substrates for RF modules. When the as-received alumina powders were used as a starting material without any treatments, it was observed that the dielectric properties of as-deposited alumina films, such as relative permittivity and loss tangent, showed high dependency on the frequency. In this study, some techniques of powder pre-treatments to improve the dielectric properties of alumina thick films will be shown and the effects of starting powders on the properties of AD films will be discussed.

Micro In-situ Tests on Overconsolidated Clay Prepared in Chambers (토조내에 준비된 과압밀 점토에 대한 모형 원위치 시험)

  • Cho Nam Jun
    • Journal of the Korean Geotechnical Society
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    • v.21 no.2
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    • pp.5-16
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    • 2005
  • Tn this study, model soil deposits are prepared in large test chambers to minimize the scale effects. Also, slurry of mixture containing 50 percent kaolin clay and 50 percent silica has been consolidated to simulate the process of natural soil deposit formation and to reduce the consolidation time. To provide a more detailed description of varying soil properties along the soil profile of model clay deposits and to compare the in-situ test results with those from prototype tests, miniature in-situ tests, including vane shear, piezoprobe, and cone penetration tests were conducted in each of the clay deposits. The current results indicate that consistent soil deposits were prepared for the current and previous test programs. Also, reasonable predicting methods of prototype behavior based on model in-situ test results were suggested in this study by examining differences between the test results from both the model and prototype tests.

Pure inorganic protective silica coating on stainless steel prepared at low heat treatment temperature

  • Hwang, Tae-Jin
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2010.05a
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    • pp.6.2-6.2
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    • 2010
  • Stainless steel is widely known to have superior corrosion properties. However, in some harsh conditions it still suffers various kinds of corrosions such as galvanic corrosion, pitting corrosion, intergranular corrosion, chloride stress corrosion cracking, and etc. For the corrosion protection of stainless steel, the ceramic coatings such as protective silica film can be used. The sol-gel coating technique for the silica film has been extensively studied especially because of the cost effectiveness. It has been proved that silica can improve the oxidation and the acidic corrosion resistance of metal surface in a wide range of temperatures due to its high heat and chemical resistance. However, in the sol-gel coating process there used to engage a heat treatment at an elevated temperature like $500^{\circ}C{\sim}600^{\circ}C$ where cracks in the silica film would be formed because of the thermal expansion mismatch with the metal. The cracks and pores of the film would deteriorate the corrosion resistance. When the heat treatment temperature is reduced while keeping the adhesion and the density of the film, it could possibly give the enhanced corrosion resistance. In this respect, inorganic protective silica film was tried on the surface of stainless steel using a sol-gel chemical route where silica nanoparticles, tetraethoxysilane (TEOS) and methyltriethoxysilane (MTES) were used. Silica nanoparticles with different sizes were mixed and then the film was deposited on the stainless steel substrate. It was intended by mixing the small and the large particles at the same time a sufficient consolidation of the film is possible because of the high surface activity of the small nanoparticles and a modest silica film is obtained with a low temperature heat treatment at as low as $200^{\circ}C$. The prepared film showed enhanced adhesion when compared with a silica film without nanoparticle addition. The films also showed improved protect ability against corrosion.

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Estimating the Interim Rate of Votes Earned Based on the Exit Poll Results during the Coverage of Ballot Results by Broadcasters (선거 개표방송에서 출구조사 자료를 활용한 중간 득표율 추정에 관한 연구)

  • Lee, Yoon-Dong;Park, Jin-Woo
    • Survey Research
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    • v.12 no.1
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    • pp.141-152
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    • 2011
  • During major elections, three terrestrial broadcasting stations in Korea have covered the progresses of election results by announcing the simple sum of ballot counts of all ballot counting stations. The current approach, however, does not properly reflect the actual ballot count differences by ballot counting location, leading to cause unnecessary but possible confusions. In addition, the current coverage approach restricts the broadcasters from using regional poll data gained through exit polls by letting them to use the significant information on a one-off purpose to announce the initial prediction of the poll results and to fully disregard the exit poll results during the ballot counting process. Based on the understanding, this paper is designed to suggest a Bayesian approach to consolidate the exit poll results with the progressive ballot counting results and announce them as such. The suggested consolidation approach is expected to mitigate or avoid the possible confusions that may arise in connection with the different ballot counting paces by ballot counting station.

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Analysis of the Change in Microstructures of Nano Copper Powders During the Hydrogen Reduction using X-ray Diffraction Patterns and Transmission Electron Microscope, and the Mechanical Property of Compacted Powders (X-선 회절 패턴 측정과 투과 전자 현미경을 이용한 구리 나노분말의 수소 환원 처리 시 발생하는 미세조직 변화 및 치밀화 시편의 물성 분석)

  • Ahn, Dong-Hyun;Lee, Dong Jun;Kim, Wooyeol;Park, Lee Ju;Kim, Hyoung Seop
    • Journal of Powder Materials
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    • v.21 no.3
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    • pp.207-214
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    • 2014
  • In this study, nano-scale copper powders were reduction treated in a hydrogen atmosphere at the relatively high temperature of $350^{\circ}C$ in order to eliminate surface oxide layers, which are the main obstacles for fabricating a nano/ultrafine grained bulk parts from the nano-scale powders. The changes in composition and microstructure before and after the hydrogen reduction treatment were evaluated by analyzing X-ray diffraction (XRD) line profile patterns using the convolutional multiple whole profile (CMWP) procedure. In order to confirm the result from the XRD line profile analysis, transmitted electron microscope observations were performed on the specimen of the hydrogen reduction treated powders fabricated using a focused ion beam process. A quasi-statically compacted specimen from the nano-scale powders was produced and Vickers micro-hardness was measured to verify the potential of the powders as the basis for a bulk nano/ultrafine grained material. Although the bonding between particles and the growth in size of the particles occurred, crystallites retained their nano-scale size evaluated using the XRD results. The hardness results demonstrate the usefulness of the powders for a nano/ultrafine grained material, once a good consolidation of powders is achieved.

Numerical Formulation for Flow Analysis of Dredged Soil (준설토 유동해석을 위한 유한요소 수식화)

  • Shin, Hosung
    • Journal of the Korean GEO-environmental Society
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    • v.15 no.3
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    • pp.41-48
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    • 2014
  • Experimental study of sedimentation and self-weight consolidation has been primary research area in dredged soil. However, good quality of the dredged soil and minimum water pollution caused by the pumping of reclaimed soil require intensive study of the flow characteristics of dredged material due to dumping. In this study, continuity and the equilibrium equations for mass flow assuming single phase was derived to simulate mass flow in dredged containment area. To optimize computation and modeling time for three dimensional geometry and boundary conditions, depth integration is applied to governing equations to consider three dimensional topography of the site. Petrov-Galerkin formulation is applied in spatial discretization of governing equations. Generalized trapezoidal rule is used for time integration, and Newton iteration process approximated the solution. DG and CDG technique were used for weighting matrix in discontinuous test function in dredged flow analysis, and numerical stability was evaluated by performed a square slump simulation. A comparative analysis for numerical methods showed that DG method applied to SU / PG formulation gives minimal pseudo oscillation and reliable numerical results.

Effect of Milling Time on Pore Size and Distribution of Ti-Nb-Zr Biomaterials with Space Holder Consolidated by Spark Plasma Sintering

  • Kim, Dong-Gun;Woo, Kee-Do;Kang, Dong-Soo;Lee, Tack
    • Korean Journal of Materials Research
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    • v.24 no.2
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    • pp.111-115
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    • 2014
  • Titanium and its alloys are useful for implant materials. In this study, porous Ti-Nb-Zr biomaterials were successfully synthesized by powder metallurgy using a $NH_4HCO_3$ as space holder and $TiH_2$ as foaming agent. Consolidation of powder was accomplished by spark plasma sintering process(SPS) at $850^{\circ}C$ under 30 MPa condition. The effect of high energy milling time on pore size and distribution in Ti-Nb-Zr alloys with space holder($NH_4HCO_3$) was investigated by optical microscope(OM), scanning electron microscope(SEM) & energy dispersive spectroscopy(EDS) and X-ray diffraction(XRD). Microstructure observation revealed that, a lot of pores were uniformly distributed in the Ti-Nb-Zr alloys as size of about $30-100{\mu}m$ using mixed powder and milled powders. In addition, the pore ratio was found to be about 5-20% by image analysis, using an image analyzer(Image Pro Plus). Furthermore, the physical properties of specimens were improved with increasing milling time as results of hardness, relative density, compressive strength and Young's modulus. Particularly Young's modulus of the sintered alloy using 4h milled powder reached 52 GPa which is similar to bone elastic modulus.

A Design of Internet-Based Safety Guarantee Global Integrated Logistics Management System Framework (인터넷 기반의 안전보장 글로벌 통합물류관리시스템 프레임워크 설계)

  • Hong, Ho-Seon;Hong, Ki-Sung;Lee, Chulung
    • Journal of the Korea Society of Computer and Information
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    • v.18 no.5
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    • pp.103-111
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    • 2013
  • This paper provide a framework for an IGILMS(internet-based global integrated logistics management system) which can access and mediate cargo transportations among small- and medium-sized domestic/international logistics corporations as regards cargo, registration and search for space, public tender and negotiation, contract, payment and safety-guarantee, transportation through the internet, wireless communication means, or smart phone etc. In addition, we describe a model to provide customized services in the B2B e-market for IGILMS and the structure and the control of its fulfillment process, and provide technical architecture of the IGILMS for an internet-based global logistics management system. To validate an efficiency of the proposed system, we develop a simulation model and analyze the performance of the proposed system.

Synthesis and Microstructure of Fe-Base Superalloy Powders with Y-Oxide Dispersion by High Energy Ball Milling (고에너지 볼 밀링을 이용한 Y-산화물 분산 Fe-기초내열합금 분말의 합성 및 미세조직 특성)

  • Yim, Da-Mi;Park, Jong Kwan;Oh, Sung-Tag
    • Korean Journal of Materials Research
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    • v.25 no.8
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    • pp.386-390
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    • 2015
  • Fe-base superalloy powders with $Y_2O_3$ dispersion were prepared by high energy ball milling, followed by spark plasma sintering for consolidation. High-purity elemental powders with different Fe powder sizes of 24 and 50 mm were used for the preparation of $Fe-20Cr-4.5Al-0.5Ti-O.5Y_2O_3$ powder mixtures (wt%). The milling process of the powders was carried out in a horizontal rotary ball mill using a stainless steel vial and balls. The milling times of 1 to 5 h by constant operation (350 rpm, ball-to-powder ratio of 30:1 in weight) or cycle operation (1300 rpm for 4 min and 900 rpm for 1 min, 15:1) were applied. Microstructural observation revealed that the crystalline size of Fe decreased with an increase in milling time by cyclic operation and was about 15 nm after 3 h, forming a FeCr alloy phase. The cyclic operation had an advantage over constant milling in that a smaller-agglomerated structure was obtained. The milled powders were sintered at $1100^{\circ}C$ for 30 min in vacuum. With an increase in milling time, the sintered specimen showed a more homogeneous microstructure. In addition, a homogenous distribution of Y-compound particles in the grain boundary was confirmed by EDX analysis.

A Case of Septic Pulmonary Embolism Associated with MRSA Infective Endocarditis (메치실린 내성 황색포도상구균 세균성 심내막염에 의한 패혈성 폐색전증 1예)

  • Lee, Ki-Jong;Kim, Nha-Young;Kim, Ja-Seon;Yun, Han-Kyeol;Oh, Mi-Jung;Kim, Do-Hoon;Cho, Sang-Kyun;Ryu, Han-Young;Bae, Young-A;Kim, Dae-Bong;Shin, Mi-Kyung;Chin, Jae-Yong
    • Tuberculosis and Respiratory Diseases
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    • v.69 no.2
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    • pp.124-128
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    • 2010
  • Septic pulmonary embolism is the process in which an infected thrombus becomes detached from its site of origin and lodges in a pulmonary artery, and is usually associated with infective endocarditis, especially right-sided, or infection-associated with indwelling catheters, peripheral septic thrombophlebitis, and periodontal diseases, etc. Here, we report a case of septic pulmonary embolism associated with tricuspid valve infective endocarditis. A 23-year-old female was admitted to our hospital, due to fever, sore throat, and myalgia. In her past medical history, she had undergone a surgical operation for closure of a ventricular septal defect, but was informed that the operation resulted in an incomplete closure. The initial chest radiograph demonstrated multiple rounded, parenchymal nodules in various sizes; several nodules had central lucency suggesting cavitations. Echocardiography demonstrated a large vegetation attached to the septal tricuspid valve leaflet, extending from right ventricular inflow tract to outflow tract. Computed tomography of thorax revealed bilateral peripheral nodules and wedge-shaped consolidation at various sizes, mostly accompanied by cavitations.