• Title/Summary/Keyword: compressive property

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Preparation of CaO-SiO2-B2O3 Glass-ceramics and Evaluation of Bioactivity Using in-vitro Test (CaO-SiO2-B2O3계 결정화 유리의 제조와 in-vitro법을 이용한 생체활성 평가)

  • Ryu, Hyun-Seung;Seo, Jun-Hyuk;Kim, Hwan;Hong, Kug-Sun;Kim, Deug-Joong;Lee, Jae-Hyup;Lee, Dong-Ho;Chang, Bong-Soon;Lee, Choon-Ki
    • Journal of the Korean Ceramic Society
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    • v.39 no.5
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    • pp.490-497
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    • 2002
  • Sintering property, mechanical property and bioactivity of $CaO-SiO_2-B_2O_3$ glass-ceramics were investigated. This glass-ceramics was sintered at 750-830${\circ}$ and showed nearly pore-free microstructure. The glass-ceramics consisted of three phases, i.e. monclinic-wollastonite, calcium borate and borosilicate glass matrix. The mechanical strength was higher than that of other bioactive ceramics, especially compressive strength(2813 MPa) and fracture toughness($3.12 MPa{\cdot}m^{1/2}$). Bioactivity of the glass-ceramics depends on amount of $CaB_2O_4$ and borosilicate glass matrix. It might be likely that more soluble $CaB_2O_4$ raises supersaturation of Ca ion in SBF solution and borosilicate glass forms Si-OH group that presents nucleation site of hydroxycarbonate apatite(HCA) layer. So, glassceramics of more $CaB_2O_4$ and borosilicate glass showed better bioactivity.

The structural safety diagnosis of Dabo Pagoda of Bulkuk Temple using analyses of ultrasonic wave velocity (초음파 속도 분석을 통한 불국사 다보탑 구조 안전 진단)

  • Suh, Man-Cheol;Song, In-Sun;Choi, Hui-Soo
    • Journal of the Korean Geophysical Society
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    • v.5 no.3
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    • pp.199-209
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    • 2002
  • We have carried out a nondestructive close examination for the purpose of the structural safety diagnosis of the Dabo Pagoda of Bulkuk temple located in Kyungju, Kyungbuk Korea. For estimating the mechanical properties of each rock block of the pagoda, ultrasonic measurements were conducted at 641 points of 255 blocks. The P-wave velocity ranges from 584m/sec through 5,169m/sec, and averages 2,901m/sec Based on this result, the uniaxial compressive strength was estimated to be $93{\sim}1,943kg/cm^2\;with\;396kg/cm^2$ of average, and the index of weathering is $0.07{\sim}0.88$ with 0.43 of average, which means the moderate degree of weathering. The comparison of the rock strength of each block with the overburden acting on the block reveals that the rock blocks related to the structure of the pagoda are relatively sound for uniform stress, but it is highly possible for a concentrated stress to lead to a partial failure. We suggest a monitoring of cracks due to the concentrated stress. The parapets of 1st and 2nd floors composed of small rock pieces are severely weathered. However, this is not directly related to the structural safety of the pagoda.

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Evolution on Microstructure and Mechanical Property of Ti65Fe35 Hypereutectic Alloys by Adding Low Melting Temperature Elements (저융점 원소의 첨가에 따른 Ti65Fe35 과공정 합금의 미세구조와 기계적 특성의 변화)

  • Hwang, Yun Jung;Hong, Sung Hwan;Kim, Jeong Tae;Kim, Young Seok;Park, Hae Jin;Kim, Hee Jin;Jeong, Yeon Beom;Lee, Young Hoon;Kim, Ki Buem
    • Korean Journal of Materials Research
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    • v.27 no.10
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    • pp.557-562
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    • 2017
  • The microstructural evolution and modulation of mechanical properties were investigated for a $Ti_{65}Fe_{35}$ hypereutectic alloy by addition of $Bi_{53}In_{47}$ eutectic alloys. The microstructure of these alloys changed with the additional BiIn elements from a typical dendrite-eutectic composite to a bimodal eutectic structure with primary dendrite phases. In particular, the primary dendrite phase changed from a TiFe intermetallic compound into a ${\beta}$-Ti solid solution despite their higher Fe content. Compressive tests at room temperature demonstrated that the yield strength slightly decreased but the plasticity evidently increased with an increasing Bi-In content, which led to the formation of a bimodal eutectic structure (${\beta}$-Ti/TiFe + ${\beta}$-Ti/BiIn containing phase). Furthermore, the (Ti65Fe35)95(Bi53In47)5 alloy exhibited optimized mechanical properties with high strength (1319MPa) and reasonable plasticity (14.2 %). The results of this study indicate that the transition of the eutectic structure, the type of primary phases and the supersaturation in the ${\beta}$-Ti phase are crucial factors for controlling the mechanical properties of the ultrafine dendrite-eutectic composites.

A Comparative study on Dynamic & Static elastic modulus of cement mortar specimens (시멘트 모르타르 재료의 동탄성계수와 정탄성계수 비교 연구)

  • O, Seon-Hwan;Kim, Hyoung-Soo;Jang, Bo-An;Suh, Man-Cheol
    • Journal of the Korean Geophysical Society
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    • v.3 no.2
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    • pp.127-138
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    • 2000
  • This study was conducted to examine the differences between dynamic and static elastic constants by use of some laboratory tests of cement mortar specimens which have different water/cement mixing ratios. Specific gravity measurement, ultrasonic velocity estimating and uniaxial compression test were adopted to acquire the dynamic and static elastic constants. Digital data acquisition and processing enhanced the accuracy of estimating the velocities of specimens drastically, Also, the method using the gradient of propagation delay time in according to increment of specimen length more enhanced the accuracy than the method using the only one specimen length over total propagation time. The correlation between density and the P and S wave velocity of specimens shows reliable positive relation and the correlation between density and the strength of uniaxial compression has the similar relationship. The dynamic Young's modulus $(E_D)$ is alway greater than the static Young's modulus $(E_S)$ and there is increasing tendency of the ratio $(E_D/E_S)$ according to the increase of density or strength of the specimens. On the other hand, there is no typical relationship between dynamic Poisson's ratio $({\nu}_D)$ and static Poisson's ratio $({\nu}_S)$ and just the ratio of ${\nu}_D/{\nu}_S$ ranges front 69 to 122 %.

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Manufacture and Application of anhydrous calcium sulfate from flue gas desulfurization gypsum (排煙脫黃石膏로부터 無水石膏 製造 및 適用 特性)

  • Hyun, Jong-Yeong;Jeong, Soo-Bok;Chae, Young-Bae;Kim, Byung-Su
    • Resources Recycling
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    • v.14 no.2
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    • pp.10-18
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    • 2005
  • The manufacture property of anhydrous calcium sulfate (anhydrite Ⅱ) from flue gas desulfurization (FGD) gypsum discharged from domestic thermoelectric power plants to apply as an auxiliary material of cement and concrete by high temperature treatment were investigated. The FGD gypsum was completely converted to anhydrite Ⅱ at the temperature of 700$^{\circ}C$ and the retention time of 1 hr. In the phase transformation process, particle size was also changed. The chemical composition, particle size and heat property of anhydrite Ⅱ made from the FGD gypsum were similar to them of natural gypsum. In the leaching test of sulfate ion (SO$_4^{2-}$) at the temperature of 90$^{\circ}C$ and the retention time of 1 hr, the amount of leached SO$_4^{2-}$ for the anhydrite Ⅱ that was sintered at 700$^{\circ}C$ for 1 hr was about 50 wt.% based on that of natural gypsum. In addition, the amount of leached SO$_4^{2-}$ for the anhydrite Ⅱ by adding the slaked lime of 3 wt.% decreased about 70 wt.% comparing with that of natural gypsum. In the application test, the compressive strength of cement and concrete manufactured by using the anhydrite Ⅱ as an auxiliary material were similar or superior compared with them of cement and concrete done by natural gypsum as an auxiliary material.

Study of Tungsten Nitride Diffusion Barrier for Various Nitrogen Gas Flow Rate by Employing Nano-Mechanical Analysis (Nano-Mechanics 분석을 통한 질화 텅스텐 확산방지막의 질소 유량에 따른 연구)

  • Kwon, Ku Eun;Kim, Sung Joon;Kim, Soo In;Lee, Chang Woo
    • Journal of the Korean Vacuum Society
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    • v.22 no.4
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    • pp.188-192
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    • 2013
  • Many studies have been conducted for preventing from diffusion between silicon wafer and metallic thin film due to a decrease of line-width and multi-layer thin film for miniaturization and high integration of semiconductor. This paper has focused on the nano-mechanical property of diffusion barrier which sample is prepared for various gas flow rate of nitrogen with tungsten (W) base from 2.5 to 10 sccm. The deposition rate, resistivity and crystallographic properties were measured by a ${\beta}$-ray back-scattering spectroscopy, 4-point probe and x-ray diffraction (XRD), respectively. We also has investigated the nano-mechanical property using the nano-indenter. As a result, the surface hardness of W-N thin film was increased rapidly from 10.07 to 15.55 GPa when the nitrogen gas flow was increased from 2.5 to 5 sccm. And the surface hardness of W-N thin film had 12.65 and 12.77 GPa at the nitrogen gas flow of 7.5 and 10 sccm respectively. These results were decreased by the comparison with the W-N thin film at nitrogen gas flow of 5 sccm. It was inferred that these severe changes were caused by the stoichiometric difference between the crystalline and amorphous state in W-N thin film. In addition, these results were caused by increased compressive stress.

Finite element analysis of the effect of novel Lock Screw system preventing abutment screw loosening (지대주 나사 풀림 방지를 위한 새로운 Lock Screw 시스템의 효과에 대한 유한요소해석적 연구)

  • Im, Eun Sub;Kim, Jong Eun;Kim, Jee Hwan;Park, Young Bum
    • Journal of Dental Rehabilitation and Applied Science
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    • v.35 no.3
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    • pp.132-142
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    • 2019
  • Purpose: The purpose of this finite element analysis study is to introduce the novel Lock screw system and analyze its mechanical property to see if it can prevent abutment screw loosening. Materials and Methods: The Lock screw is a component tightened on the inside of the implant abutment which applies compressive force to the abutment screw head. To investigate the effect, modeling was done using CAD program and it was analyzed by finite element analysis under various load conditions. First, the preload was measured according to the tightening torque of the abutment screw then it was compared with the theoretical value to verify the analytical model. The validated analytical model was then divided into those with no external load and those with 178 N, and the tightening torque of the lock screw was changed to 10, 20, 30 Ncm respectively to examine the property of stress distribution on the implant components. Results: Using Lock screw under various loading conditions did not produce equivalent stresses beyond the yield strength of the implant components. In addition, the axial load was increased at the abutment-abutment screw interface. Conclusion: The use of Lock screw does not exert excessive stress on the implant components and may increase the frictional force between the abutment-abutment screw interface, thus it is considered to prevent loosening of the abutment screw.

The Effect of Blast Cleaning for Steel Bridge Painting on Fatigue Behavior of Out-of-Plane Gusset Welded Joints (강교 도장용 블라스트 처리가 면외거셋 용접이음의 피로거동에 미치는 영향)

  • Kim, In Tae;Le, Van Phuoc Nhan;Kim, Kwang Jin;Lee, Dong Uk
    • Journal of Korean Society of Steel Construction
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    • v.20 no.5
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    • pp.583-590
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    • 2008
  • Blasting has been applied in newly-built steel structures for cleaning forged surfaces and increasing the adhesive property of applied painting systems. However, the effect of the blast cleaning on fatigue behavior of welded joints is not clear. In this paper, fatigue tests were carried out on out-of-plane gusset welded joints and the effect of the blast cleaning on the fatigue behavior was studied. The curvature radius at the weld toe of the surface-treated specimens by using the blast method is larger than that of as-welded specimens. By the blast cleaning compressive residual stresses were induced into weld toes. The experimental results showed that the fatigue life of surface-treated specimens is longer than that of as-welded specimens, even though the fatigue life of surface-treated specimens and that of as-welded specimens are not clearly different in the high stress range. About a 160% increase in fatigue limit could be realized by using blast cleaning.

Study of Cure Behavior of the External and Internal of Composite Parts (경화공정에 따른 복합재 부품 외부와 내부의 경화 거동 차이에 대한 연구)

  • Hyun, Dong Keun;Lee, Dong Seung;Shin, Do Hoon;Kim, Ji Hoon
    • Composites Research
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    • v.33 no.5
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    • pp.302-308
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    • 2020
  • We measured the thermal conductivity of composite materials manufactured by the autoclave and vacuum bag only processes and predicted the cure behavior of the external and internal of composite parts with a cure kinetics model. The temperature difference between the external and internal depends on the processes because of the change of thermal conductivity. In the autoclave process, the temperature and cure behavior of the internal were similar to those of the external because of the high thermal conductivity. However, the temperature of the internal of the vacuum bag only process was different from that of the external. The difference can influence the part quality and evacuation of air. Compression tests were performed to find the mechanical property using 0° unidirectional specimens. The composite of the vacuum bag only process was found to have a lower compressive strength than that of the autoclave process.

The Physical Properties of UV-curable Resin for the Restoration of Glass Cultural Properties and Its Application in Conservation Treatment (유리제 문화재 복원용 광경화성 수지의 물성 연구 및 적용)

  • Lee, Hae Soon;Na, Ah Young
    • Conservation Science in Museum
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    • v.21
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    • pp.1-16
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    • 2019
  • This study investigated the material properties of UV-curable Resin in order to identify stable materials for use in the restoration of glass cultural properties. Tested samples were based on acrylic UV-curable Resin (SECURE CP-7321®), to which urethane UV-curable Resin (FLGPCL04 Clear®) was added in 10% increments to produce eleven samples. The results showed that all eleven samples had similar properties in terms of refractive index, density, adhesive strength, and anti-yellowing. But the surface hardness and compressive strength were optimal and effective for maintaining the shape of artifacts after restoration treatment when the proportion of urethane resin was in the range of 10-20%. Based on these findings, the mixing sample [acrylic UV-curable Resin(9) : urethane UV-curable Resin(1)] was applied in the conservation treatment of a glass cultural propertie (Hwangbuk 519) excavated from the North Mound of Hwangnamdaechong, Tomb in Gyeongju.