• Title/Summary/Keyword: complex analysis

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Determination of Methylmercury in Biological Samples Using Dithizone Extraction Method Followed by Purge & Trap GC-MS

  • Lee, Jung-Sub;Ryu, Yoon-Jung;Park, Jae-Sung;Jeon, Sung-Hwan;Kim, Sam-Cwan;Kim, Young-Hee
    • Bulletin of the Korean Chemical Society
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    • v.28 no.12
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    • pp.2293-2298
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    • 2007
  • In this study, a dithizone extraction technique involving purge & trap GC-MS was developed for the determination of methylmercury in biological samples, especially blood and fish. After alkaline digestion, methylmercury in biological samples was extracted into dithizone and back-extracted into aqueous sulfide solution. The extracted methylmercury was converted to the volatile ethyl derivative, purged and trapped onto a solid-phase collection medium, and then introduced into the GC-MS system. The determined MDLs of the established method were 0.9 ng·g?1 for biological samples and its accuracy and precision were found to be 93% and 3.8%, respectively. The method was validated by analysis of CRMs such as SRM 966, BCR 463 and IAEA 407 and all analytical results were within certified ranges with average RSDs of less than 6%. The analytical results of field-sampled fish also showed that the method can be successfully used as an alternative for commonly used distillation method followed by GC-CVAFS detection.

Complex segregation analysis

  • Shin, Han-Poong
    • Journal of the Korean Statistical Society
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    • v.3 no.2
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    • pp.103-115
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    • 1974
  • During the last few years there has been an interest in models for qualitative attributes, where complex signifies that affection may be caused in two or more ways [1-3]. These models have in common the prediction of variable recurrence risks among families with given parental phenotpes. Segregation analysis has covered only a few cases [4,5]. The present paper extends segregation analysis to three complex models under two mode of ascertainment.

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Dynamic analysis for complex structures using the improved component mode method (개선된 콤포넌트 모드법을 이용한 거대구조물의 동적해석)

  • 심재수;박명균
    • Proceedings of the Computational Structural Engineering Institute Conference
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    • 1993.04a
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    • pp.37-44
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    • 1993
  • There are a lot of linear dynamic analysis methods for complex structures. Each method has advantages and shortcomings. Method of dynamic analysis for complex structure is selected considering characteristics of dynamic loading, computer facility available number of degree of freedem and accuracy of results. It is a main point of view to get economical results rather then accurate ones for analysis of general complex structures, Mode superposition method and direct integration method are generally used. However, the characteristics of load is not considered in mode superpositon method, the personal computer cannot be used in direct integration methods. To over-come these shortcomings, the component mode method incorporating Ritz algorithm updated is proposed to solve economically dynamic behavior of the structures. The purpose of study is a formulation of algorithm, and computer programing suitable for dynamic analysis of the complex structure in personal computer environment.

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Soluble Complex Formation of Rifampicin with Arginine (Rifampicin과 Arginine간의 가용성 Complex 형성에 관한 연구)

  • 김종국;신희종
    • YAKHAK HOEJI
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    • v.27 no.1
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    • pp.11-19
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    • 1983
  • Rifampicin-arginine complex was prepared to increase the solubility and dissolution rate of rifampicin. Solvation method was applied to make the complex and its formation was identified by the solubility method, powder x-ray diffractometry, differential thermal analysis and spectroscopic determination. The complex was formed in the molar ratio of 1 : 1 which was proved by the slope ratio method and continuous variation method. The complex was a non-crystalline form determined by the x-ray powder diffractometric analysis. The solubility of complex in water was significantly higher than that of rifampicin itself. The stability constant and thermodynamical properties of the complex were determined to investigate the solubilization phenomena. The thermodynamic data showed that the complexation between rifampicin and arginine was an exothermic and spontaneous reaction. Simulated absorption studies carried out through the artificial lipid barrier in artificial gastric and intestinal juices. The results showed that the complex had an enhanced absorption rate of rifampicin nearly twice compared with that of rifampicin itself.

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A Study on Development Strategy of Industrial Complex using SWOT/AHP Analysis Theory - The Case of the Firms in Seoul Digital Industrial Complex (SWOT/AHP 분석기법을 이용한 산업단지의 발전 전략에 관한 연구: 서울디지털산업단지를 중심으로)

  • Kim, Bo Seok;Lee, Min Jung
    • The Journal of Information Systems
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    • v.24 no.4
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    • pp.61-81
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    • 2015
  • Purpose Seoul Digital Industrial Complex has remarkably grown both quantitatively and qualitatively in short period of time since it started restructuring project in 1997. It's also not few that there were various challenges and difficulties in this industrial complex due to fast growth in short-term, such as the deficient amenities, noncooperation among the related organizations. Now, it's time to overcome these challenges and difficulties to establish new strategy for the sustainable growth and development of this Industrial Complex. Methodology There are some previous researches but almost none of them considered the priority order of the development strategy having reflected the needs of industrial complex in point of customer. In this regard, this study suggests the development strategy of Seoul Digital Industrial Complex by supplementing the limits of proceeding researches and using the combined SWOT/AHP analysis theory. Findings Based on the final analysis result of survey by combined SWOT/AHP method, this study suggests the priority order of 4 development strategies for Seoul Digital Industrial Complex, such as SO strategy, ST strategy, WO strategy and WT strategy.

A Comparative Analysis of Complex Disaster Research Trends Using Network Analysis (네트워크 분석을 활용한 국내·외 복합재난 연구 동향 분석)

  • Woosik Kim;Yeonwoo Choi;Youjeong Hong;Dong Keun Yoon
    • Journal of the Society of Disaster Information
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    • v.18 no.4
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    • pp.908-921
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    • 2022
  • Purpose: As the connection between physical and non-physical structures in cities is expanding and becoming more complex, the risk of complex disaster which causes damage in a complex way is increasing. Preparing for these complex disasters, it is important to preemptively identify and manage disasters that can develop into complex disasters. Therefore, this study analyzes the disaster types studied as complex disasters by analyzing the trends of domestic and international studies related to complex disasters, and presents the direction of complex disaster management in the future. Method: We first established co-occurrence networks between disaster types based on 993 articles related to complex disasters published in disaster-related journals for the last 20 years (2002-2021). Then, through network analysis, domestic and international complex disaster research trends were compared and analyzed. Result: Research on complex disasters related to storm and flood damage, infrastructure failure and fire was high in domestic studies, and it was analyzed that research on complex disasters related to earthquakes and landslides has recently increased. However, in international studies, the proportion of studies on infrastructure failure along with storm and flood damage and earthquake was high, and various types of disasters such as tsunami and drought appeared. Conclusion: The results of this study are expected to increase the understanding of the trends in complex disaster research and provide suggestions of domestic complex disaster research in the future.

Free and transient responses of linear complex stiffness system by Hilbert transform and convolution integral

  • Bae, S.H.;Cho, J.R.;Jeong, W.B.
    • Smart Structures and Systems
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    • v.17 no.5
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    • pp.753-771
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    • 2016
  • This paper addresses the free and transient responses of a SDOF linear complex stiffness system by making use of the Hilbert transform and the convolution integral. Because the second-order differential equation of motion having the complex stiffness give rise to the conjugate complex eigen values, its time-domain analysis using the standard time integration scheme suffers from the numerical instability and divergence. In order to overcome this problem, the transient response of the linear complex stiffness system is obtained by the convolution integral of a green function which corresponds to the unit-impulse free vibration response of the complex system. The damped free vibration of the complex system is theoretically derived by making use of the state-space formulation and the Hilbert transform. The convolution integral is implemented by piecewise-linearly interpolating the external force and by superimposing the transient responses of discretized piecewise impulse forces. The numerical experiments are carried out to verify the proposed time-domain analysis method, and the correlation between the real and imaginary parts in the free and transient responses is also investigated.

Chemometric Tool of Chromatographic Pattern Recognition for the Analysis of Complex Mixtures

  • Park, Man-Ki;Park, Jeong-Hill;Cho, Jung-Hwan;Kim, Na-Young;Kang, Jong-Seong
    • Archives of Pharmacal Research
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    • v.15 no.4
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    • pp.376-378
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    • 1992
  • A chemical tool was developed for the analysis of complex mixtures such as crude drugs by the method of pattern recognition. Pattern recognition was accomplished by a multiple reference peak identification method and three kinds of outlier statistics. This tool was tested on the analysis of synthetic mixtures.

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Stability Investigation of Rotor Systems by Complex Modal Analysis (복소 모드해석을 이용한 회전체의 안정성 분석)

  • Han, Dongju
    • Journal of Aerospace System Engineering
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    • v.7 no.4
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    • pp.27-35
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    • 2013
  • Identifying the stability of rotor systems is prerequisite for clear determination of the parameter identification and safety, through which operating conditions may be rationally ascertained. For this purpose, the complex modal analysis of periodically time-varying system has been introduced by transforming the relation between periodic eigen-vectors and the corresponding adjoint vectors into the latent value problem. Stability investigation associated with modal features for rotor systems is performed using numerical simulation based upon the analysis model.

Finding Complex Features by Independent Component Analysis (독립성분 분석에 의한 복합특징 형성)

  • 오상훈
    • The Journal of the Korea Contents Association
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    • v.3 no.2
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    • pp.19-23
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    • 2003
  • Neurons in the mammalian visual cortex can be dassified into the two main categories of simple cells and complex cells based on their response properties. Here, we find the complex features corresponding to the response of complex cells by applying the unsupervised independent component analysis network to input images. This result will be helpful to elucidate the information processing mechanism of neurons in primary visual cortex.

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