• Title/Summary/Keyword: chemical testing

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Green Purification System using Natural Hydrogen Generating Mineral Filter (천연 수소 발생 광물 필터를 이용한 녹조 정화 시스템)

  • Yu-ji Kwon;Dae-gyeom Park
    • Journal of the Korean Society of Industry Convergence
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    • v.27 no.2_2
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    • pp.475-485
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    • 2024
  • In many regions of Korea, including the Four Major Rivers, the seriousness of the problem of algal blooms due to eutrophication of water quality is being raised.In this study, in order to solve these social problems, we manufactured a filter using natural mineral fusion (red illite, zeolite, germanium ceramic, selenium ceramic, carbon ceramic) and independently developed a tank system for green algae experiments to observe and determine the stages of change in water quality. In order to study ways to improve water quality through quantitative analysis, 1 ton of severely polluted green algae water from the Nak dong River region was stored in a water tank and exposed to ultraviolet rays in the same environment as the Nak dong River. Then, the same environment as the Nak dong River was created. The results were derived from a 5-week water quality test. The results of this experiment confirmed that green-colored cyano bacteria were significantly reduced just by the turbidity results. The results were obtained through a request to the Korea Testing & Research Institute located in Changwon-si, Gyeong sang nam-do. CI-(chlorine ion) and NH3-N(ammonia nitrogen) had the effect of saving every week. The device used in this study was made of natural minerals free of heavy metals that are harmless to the human body and nature through long-term consideration and exploration to kill and prevent various strains living in water. Green purification system using natural hydrogen generating mineral filter were effective a non-chemical and physical methods. The results of this study are one way to contribute to the serious problems caused by green algae in many countries, and will contribute to the water quality environment by preventing the waste of environmental resources, improving the health of the people, and increasing the ability to purify environmental water quality at home and abroad.

A Review of Strategies to Improve the Stability of Carbon-supported PtNi Octahedral for Cathode Electrocatalysts in Polymer Electrolyte Membrane Fuel Cells

  • In Gyeom Kim;Sung Jong Yoo;Jin Young Kim;Hyun S. Park;So Young Lee;Bora Seo;Kwan-Young Lee;Jong Hyun Jang;Hee-Young Park
    • Journal of Electrochemical Science and Technology
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    • v.15 no.1
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    • pp.96-110
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    • 2024
  • Polymer electrolyte membrane fuel cells (PEMFCs) are green energy conversion devices, for which commercial markets have been established, owing to their application in fuel cell vehicles (FCVs). Development of cathode electrocatalysts, replacing commercial Pt/C, plays a crucial role in factors such as cost reduction, high performance, and durability in FCVs. PtNi octahedral catalysts are promising for oxygen reduction reactions owing to their significantly higher mass activity (10-15 times) than that of Pt/C; however, their application in membrane electrode assemblies (MEAs) is challenged by their low stability. To overcome this durability issue, various approaches, such as third-metal doping, composition control, halide treatment, formation of a Pt layer, annealing treatment, and size control, have been explored and have shown promising improvements in stability in rotating disk electrode (RDE) testing. In this review, we aimed to compare the features of each strategy in terms of enhancing stability by introducing a stability improvement factor for a direct and reasonable comparison. The limitations of each strategy for enhancing stability of PtNi octahedral are also described. This review can serve as a valuable guide for the development of strategies to enhance the durability of octahedral PtNi.

Mobility and Thermal Comfort Assessment of Personal Protective Equipment for Female Healthcare Workers: Impact of Protective Levels and Body Mass Index (감염병 대응 개인보호복의 동작성 및 열적 쾌적성: 보호 수준 및 여성 착용자 체격의 영향)

  • Do-Hee Kim;Youngmin Jun;Ho-Joon Lee;Gyeongri Kang;Cho-Eun Lee;Joo-Young Lee
    • Fashion & Textile Research Journal
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    • v.26 no.1
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    • pp.123-136
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    • 2024
  • This study aimed to assess the mobility and thermal comfort of personal protective equipment (PPE) among female healthcare workers, taking into account wearers' physique and PPE protection levels. A total of 16 participants (age: 26.3 ± 8.3 y, height: 161.5 ± 7.3 cm, body weight: 57.1 ± 11.0 kg, BMI: 21.9 ± 3.6), representing diverse body types, underwent four PPE conditions: L (Low_Plastic gown ensemble), M (Medium_Tyvek 400), H (High_Tyvek 800J with Powered Air Purifying Respirator [PAPR]), and E (Extremely high_Tychem 2000 with PAPR, Bib apron, and Chemical-resistant gloves). The mobility protocol consisted of 10 different tasks in addition to donning and doffing. The 10 tasks were repeated twice at an air temperature of 24.3 ± 0.1℃, 59±4%RH. Findings revealed a disproportionate relationship between PPE protection and wearer discomfort. Significant differences in clothing microclimate and total sweat rate were observed between the lowest (L) and highest (E) protection levels (p < 0.01), while distinctions among medium levels were inconclusive. Subjective evaluations favored conditions H and L over M and E (p < 0.05), indicating reduced heat, and humidity, increased comfort, and lower exertion. Instances of mobility discomfort, specially in the small body type group, underscored the need for a suitable PPE size system for Korean adult female medical workers. Furthermore, enhancements in gloves, shoe cover, and PAPR hood designs are essential for improving ease of movement and preventing hindrance.

Experimental Study on Accelerated Carbonation Characteristics of OPC Paste for CSC-Based Low Carbon Precast Concrete Products (CSC 기반 저탄소 콘크리트 2차제품 제조를 위한 OPC 페이스트의 촉진탄산화 특성에 관한 실험적 연구)

  • Yoon, Jun-Tae;Kim, Young-Jin;Sim, Sang-Rak;Ryu, Dong-Woo
    • Journal of the Korea Institute of Building Construction
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    • v.24 no.3
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    • pp.285-295
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    • 2024
  • This study investigated the impact of accelerated carbonation on Ordinary Portland Cement(OPC) paste that had undergone steam curing at 500℃·hr. Two carbonation environments were examined: atmospheric carbonation(1atm, 20% CO2) and pressurized carbonation(5atm, 99% CO2). Chemical analysis using X-ray diffraction(XRD) and Fourier-Transform Infrared spectroscopy(FT-IR) were conducted, along with physical characterization via scanning electron microscopy(SEM) and compressive strength testing. Results indicated that atmospheric carbonation with 20% CO2 concentration significantly densified the internal microstructure of the OPC paste, leading to enhanced compressive strength. Conversely, pressurized carbonation at 5atm with 99% CO2 concentration resulted in rapid densification of the surface structure, which hindered CO2 diffusion into the sample. This limited the extent of carbonation and prevented the improvement of physical properties.

Evaluating the Protective Effectiveness of Rubber Glove Materials Against Organic Solvents Upon Repeated Exposure and Decontamination

  • Li-Wen Liu;Cheng-Ping Chang;Yu-Wen Lin;Wei-Ming Chu
    • Safety and Health at Work
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    • v.15 no.2
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    • pp.228-235
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    • 2024
  • Background: Glove reuse poses risks, as chemicals can persist even after cleaning. Decontamination methods like thermal aeration, recommended by US OSHA, vary in effectiveness. Some studies show promising results, while others emphasize the importance of considering both permeation and tensile strength changes. This research advocates for informed glove reuse, emphasizing optimal thermal aeration temperatures and providing evidence to guide users in maintaining protection efficiency. Methods: The investigation evaluated Neoprene and Nitrile gloves (22 mils). Permeation tests with toluene and acetone adhered to American Society for Testing Materials (ASTM) F739 standards. Decontamination optimization involved aeration at various temperatures. The experiment proceeded with a maximum of 22 re-exposure cycles. Tensile strength and elongation were assessed following ASTM D 412 protocols. Breakthrough time differences were statistically analyzed using t-test and ANOVA. Results: At room temperature, glove residuals decreased, and standardized breakthrough time (SBT)2 was significantly lower than SBT1, indicating reduced protection. Higher temperature decontamination accelerated residual removal, with ∆SBT (SBT2/SBT1) exceeding 100%, signifying restored protection. Tensile tests showed stable neoprene properties postdecontamination. Results underscore thermal aeration's efficacy for gloves reuse, emphasizing temperature's pivotal role. Findings recommend meticulous management strategies, especially post-breakthrough, to uphold glove-protective performance. Conclusions: Thermal aeration at 100℃ for 1 hour proves effective, restoring protection without compromising glove strength. The study, covering twenty cycles, suggests safe glove reuse with proper decontamination, reducing costs significantly. However, limitations in chemical-glove combinations and exclusive focus on specific gloves caution against broad generalization. The absence of regulatory directives on glove reuse highlight the importance of informed selection and rigorous decontamination validation for workplace safety practices.

Impact of salt stress on the α-tocopherol, carotenoid derivatives and flocculation efficiency of Euglena sp., Indonesian Strain

  • Ria Amelia;Arief Budiman;Andhika Puspito Nugroho;Eko Agus Suyono
    • Fisheries and Aquatic Sciences
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    • v.27 no.6
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    • pp.379-391
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    • 2024
  • Tocopherol, carotenoids, and chlorophyll are the primary components of the antioxidative response in microalgae. Conditions of stress, such salt stress, can trigger the processes responsible for the accumulation of tocopherol and carotene. It has been found that the most difficult part of culturing microalgae is keeping it affordable. This study investigated the effects of different salt types and concentrations on the amount of α-tocopherol, carotenoid derivatives, and flocculation efficiency of Euglena sp. Cultures of Euglena sp. was developed under salt stress conditions of NaCl 200 mM and KCl 200 mM. UV-VIS spectrophotometry was used to confirm the presence of α-tocopherol and carotenoid derivatives under thirteen days of salt stress testing. Increasing salinity has a significant effect on Euglena sp., causing spherical cell morphologies with aspect ratio 1.385 ± 0.031 for NaCl 200 mM and 1.414 ± 0.040 for KCl 200 mM. Increasing salinity also slowing down development with specific growth rate value of 0.171 ± 0.006 per day and 0.122 ± 0.029 per day for NaCl and KCl 200 mM, respectively. Nevertheless, the amount of α-tocopherol in Euglena sp. increases with a high salt concentration; algal cells flocculated more successfully when increasing the salt concentrations (NaCl 200 mM and KCl 200 mM) was added. Due to the inhibition of photosynthetic activity in salt-stressed cells, the control group exhibited higher levels of carotenoid derivatives (ranging from 0.5-1 ㎍/mL) and pheophytin a and b (0.0062 ± 0.001 ㎍/mL and 0.0064 ± 0.001 ㎍/mL) than the group treated with salt stress. In conclusion, salt stress was an effective way to raises the concentration of α-tocopherol and significantly reduce the expense of harvesting Euglena sp.

Nano-silica in Holcim general use cement mortars: A comparative study with traditional and prefabricated mortars

  • Mohammadfarid Alvansazyazdi;Jorge Figueroa;Alex Paucar;Gilson Robles;Majid Khorami;Pablo M. Bonilla-Valladares;Alexis Debut;Mahdi Feizbahr
    • Advances in concrete construction
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    • v.17 no.3
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    • pp.135-150
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    • 2024
  • Nano-silica's growing use in construction, known for enhancing strength and durability by reducing porosity, drives this research's significance, especially considering Ecuador's reliance on cement in construction. A comprehensive comparative study on mortars made with General Use cement and aggregates from Pifo and San Antonio quarries has been studied. It explores the impact of incorporating nano-silica in varying proportions (0.75%, 1.00%, 1.25%) on mortar properties, contrasting them with conventional and prefabricated mortars. laboratory Testing is conducted according to standards to assess both fresh and hardened state properties, and microscopic analysis reveals the optimal nano-silica proportion's effects on mortar characteristics. Results shows that Incorporating 0.75% nano-silica resulted in a 61% increase in compressive strength at 7 days and. For a nanosilica content of 1.25%, a 14% increase in compressive strength was observed at 28 days in relation to the conventional mortar and the permeability of the mortar decreased by 30% when adding 0.75% nanosilica. It discusses economic viability and provides insights through SEM and EDS analyses. Overall, it underscores nano-silica's potential to enhance mortar properties and its relevance in creating more efficient and durable construction materials.

The Method for Classifying Stainless Steel Grades in Products Using Portable NIR Spectrometer and CNN

  • Ju-Hoon Jang;In-Yeop Choi
    • Journal of the Korea Society of Computer and Information
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    • v.29 no.10
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    • pp.97-104
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    • 2024
  • This paper proposes a method for classifying the grade of stainless steel using a portable NIR(Near Infrared Ray) spectrometer and a CNN(Convolutional Neural Network) deep learning model. Traditionally, methods for classifying stainless steel grades have included chemical analysis, magnetic testing, molybdenum spot tests, and portable XRF devices. In addition, a classification method using a machine learning model with element concentration and heat treatment temperature as parameters was presented in the paper. However, these methods are limited in their application to everyday products, such as kitchenware and cookware, due to the need for reagents, specialized equipment, or reliance on professional services. To address these limitations, this paper proposes a simple method for classifying the grade of stainless steel using a NIR spectrometer and a CNN model. If the method presented in this paper is installed on a portable device as an on-device in the future, it will be possible to determine the grade of stainless steel used in the product, and to determine on-site whether a product made of low-cost material has been disguised as a high-cost product.

Fabrication and Evaluation Properties of Micro-Tubular Solid Oxide Fuel Cells (SOFCs) (마이크로 원통형 SOFC 제작 및 특성평가)

  • Kim, Hwan;Kim, Wan-Je;Lee, Jong-Won;Lee, Seung-Bok;Lim, Tak-Hyoung;Park, Seok-Joo;Song, Rak-Hyun;Shin, Dong-Ryul
    • Korean Chemical Engineering Research
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    • v.50 no.4
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    • pp.749-753
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    • 2012
  • In present work, anode support for micro-tubular SOFC was fabricated with outer diameter of 3 mm and characterized with microstructure, mechanical properties and gas permeability. The microstructure of surface and cross section of a porous anode support were analyzed by using SEM (Scanning Electron Microscope) image. The gas permeability and the mechanical strength of anode support was measured and analysed by using differential pressure at the flow rates of 50, 100, 150 cc/min. and using universal testing machine respectively. The unit cell composed of NiO-YSZ, YSZ, YSZ-LSM/LSM/LSCF was fabricated and operated with reaction temperature and fuel flow rate and showed maximum power density of $1095mW/cm^2$ on the condition of $800^{\circ}C$. The performance of single cell for micro-tubular SOFC increased with the increasing the reaction temperature due to the decrement of ohmic resistance of cell by the increment of the ionic conductivity of electrolyte through the evaluation of electrochemical impedance analysis for single cell with reaction temperature.

The Effect of Thatch Decomposing by Application with Composted Liquid Manure and Microorganism Medium in Golf Course Soil (배양미생물과 가축분뇨발효액비의 시비가 골프코스 토양 중 대취분해에 미치는 영향)

  • Ham, Suon Kyu;Lim, Ji Yeon;Lee, Yeong Min
    • Weed & Turfgrass Science
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    • v.3 no.4
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    • pp.342-346
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    • 2014
  • The purpose of this experiment is for investigating how much the amino acid liquid fertilizer and composted liquid manure, culture microorganism effect on the breeding of grasses and knowing the extent of the thatch content through an analysis of the soil. For testing about soil chemical, the quality of grasses, and the extent of the thatch content in the soil, we cultivated 6 kinds of microorganisms having the effect of thatch dissolution and sprayed these 6 microorganisms with composted liquid manure and the amino acid liquid fertilizer on the place Creeping bentgrass have planted. This conduction started from June to October, 2012 and 2013 (The interval: 2 weeks). In the result of the turf growth, there is no big difference between soil chemical and trace element. And we can know Leaf Color Index, Chlorophyll Index and Root Length are almost same as among treatment. In conclusion, the mixing fertilization of culture microorganism and composted liquid manure is better effective than the traditional fertilization. And it can be expected the effect of the quality of grass and Thatch decomposition in soil.