• 제목/요약/키워드: changes of grain size

검색결과 267건 처리시간 0.03초

Y2O3가 분산된 Fe-C 및 Fe-CNT 소결체의 미세구조 및 기계적 특성 (The Microstructure and Mechanical Properties of Y2O3-Dispersed Fe-C and Fe-CNT Sintered Steels)

  • 임진영;안중호
    • 한국분말재료학회지
    • /
    • 제24권4호
    • /
    • pp.298-301
    • /
    • 2017
  • In the present work, we use multiwall carbon nanotubes (MWCNT) as the starting material for the fabrication of sintered carbon steel. A comparison is made with conventionally sintered carbon steel, where graphite is used as the starting material. Milling is performed using a horizontal mill sintered in a vacuum furnace. We analyze the grain size, number of pores, X-ray diffraction patterns, and microstructure. Changes in the physical properties are determined by using the Archimedes method and Vickers hardness measurements. The result shows that the use of MWCNTs instead of graphite significantly reduces the size and volume of the pores as well as the grain size after sintering. The addition of $Y_2O_3$.to the Fe-MWCNT samples further inhibits the growth of grains.

전자선 증착기술에 의해 성장된 다결정 CdSe 박막의 광학적 특성 (Optical properties of the polycrystalline CdSe thin films grown by the electron-beam evaporation technique)

  • 김화민
    • 한국진공학회지
    • /
    • 제9권1호
    • /
    • pp.60-68
    • /
    • 2000
  • The optical constants ($E_g^d$, n, K) of the polycrystalline CdSe thin films deposited on the glass substrate by the electron-beam evaporation technique are determined over 400~2,500 nm photon wavelengths. In order to explain the variation of the optical contents with film thickness and substrate temperatures, the surface microstructural parameter are investigated by AFM (atomic forced microscope( images for the films deposited by different growth conditions. It is shown that the variations of optical constants are close related to changes of the surface morphology of the CdSe thin films. The decrease in the band gap with film thickness is connected with quantum size effects due to increase of the grain size. The refractive index of CdSe films decrease with increasing the grain size of the films, and the dispersion of the refractive index followed a single oscillator model according to the Sellmeier formulation.

  • PDF

불포화의 흙-수분 특성곡선 방정식의 개발 (Development of Equation of the Soil-Water Characteristic Curve for an Unsaturated Soil)

  • 송창섭;임성윤;김명환
    • 한국농공학회:학술대회논문집
    • /
    • 한국농공학회 2003년도 학술발표논문집
    • /
    • pp.191-194
    • /
    • 2003
  • The purpose of this paper was to derive soil-water characteristic curve equation for unsaturated soil. To this end, a series of suction measured test was conducted on the selected 4 kinds of soil which is located in Korea, used the modified pressure plate apparatus. From the test results, it was proved that characteristic curve changes according to grain size distribution, size of void and fine grained soil contents. Residual degree of saturation(Sr) was decreased with void ratio and changed with fine grained soil contents, parameter ${\lambda}$ and hr was increased with void ratio. Soil-water characteristic curve equation based on the test result was suggested by void ratio or grain size distribution.

  • PDF

Characteristics of 14K white gold by age-hardening treatment

  • 윤돈규;서진교;신소라;박종완
    • 한국재료학회:학술대회논문집
    • /
    • 한국재료학회 2012년도 춘계학술발표대회
    • /
    • pp.107.1-107.1
    • /
    • 2012
  • Because of beautiful glossy and color, the value of gold leverage is very high in Europe. For improve the quality of white gold, we performed heat treatment on 14K white gold alloys at various age-hardening conditions. Age-hardening behavior and the related phase transformation changes were studied to elucidate the hardening mechanism of 14K white gold alloys. For solid solution treatment [ST], casted 14K white gold alloy specimens were treated at high temperature ($750^{\circ}C$) during 30 minute, and the specimens dropped to water for quenching immediately. For Age-hardening treatment [AT], the specimens were treated at various temperatures ($250^{\circ}C{\sim}300^{\circ}C$). After the heat treatment, we observed increased hardness from 144 Hv to 214 Hv by Vicker's hardness tester. Variation of the grain size measured by optical microscopy (OM) and scanning electron microscopy (SEM) images. By electron probe micro-analysis (EPMA) mapping analysis, we investigated that irregular particles were changed uniformly. After heat treatment, 14K white gold alloys showed improved hardness and became uniformity of grain size by age-hardening treatment.

  • PDF

Mn 및 V 함량이 다른 페라이트-펄라이트 조직강의 강도와 변형능에 미치는 미세조직 인자의 영향 (Effect of Microstructural Factors on the Strength and Deformability of Ferrite-Pearlite Steels with Different Mn and V Contents)

  • 홍태운;이상인;심재혁;이준호;이명규;황병철
    • 한국재료학회지
    • /
    • 제28권10호
    • /
    • pp.570-577
    • /
    • 2018
  • This study examines the effect of microstructural factors on the strength and deformability of ferrite-pearlite steels. Six kinds of ferrite-pearlite steel specimens are fabricated with the addition of different amounst of Mn and V and with varying the isothermal transformation temperature. The Mn steel specimen with a highest Mn content has the highest pearlite volume fraction because Mn addition inhibits the formation of ferrite. The V steel specimen with a highest V content has the finest ferrite grain size and lowest pearlite volume fraction because a large amount of ferrite forms in fine austenite grain boundaries that are generated by the pinning effect of many VC precipitates. On the other hand, the room-temperature tensile test results show that the V steel specimen has a longer yield point elongation than other specimens due to the highest ferrite volume fraction. The V specimen has the highest yield strength because of a larger amount of VC precipitates and grain refinement strengthening, while the Mn specimen has the highest tensile strength because the highest pearlite volume fraction largely enhances work hardening. Furthermore, the tensile strength increases with a higher transformation temperature because increasing the precipitate fraction with a higher transformation temperature improves work hardening. The results reveal that an increasing transformation temperature decreases the yield ratio. Meanwhile, the yield ratio decreases with an increasing ferrite grain size because ferrite grain size refinement largely increases the yield strength. However, the uniform elongation shows no significant changes of the microstructural factors.

Seasonal Variation and Preservation Potential of Tidal-Flat Sediments on the Tidal Flat of Gomso Bay, West Coast of Korea

  • Chang, Jin-Ho
    • 한국제4기학회지
    • /
    • 제18권2호통권23호
    • /
    • pp.19-22
    • /
    • 2004
  • Seasonal changes of topograpy, sediment grain size and accumulation rate on the Gomso-Bay tidal flat(Fig. 1), west coast of Korea, have studied in order to understand the seasonal accumulation pattern and preservation potential of tidal-flat sediments. Seasonal levelings across the tidal flat show that the landward movement of both intertidal sand shoals and cheiers accelerates during the winter and typhoon period, but it almost stops in summer when mud deposition is instead predominant on the middle to upper tidal flat. Seasonal variations of mean grain size were largest on the upper part of middle tidal flat where summer mud layers were eroded during the winter and typhoon periods(Fig. 2). Measurements of accululation depths from sea floor to basal plate reveal that accumulation rates were seasonally controlled according to the elevation of tidal-flat surface(Table 1) : the upper flat, where the accumulation rate of summer was generally higher than that of winter, was characterized by a continuous deposition throughout the entire year, whereas on the middle flat, sediment accumulations were concentrated in winter realtive to summer, and were intermittently eroded by typhoons. The lower tidal flat were deposited mostly in winter and eroded during summer typhoons. Cancores taken across the tidal flat reveal that sand-mud interlaers resulting from such seasonal changes of energy regime are preserved only in the upper part of the deposits and generally replaced by storm layers downcore(Fig. 3). Based on above results, it is suggested that the storm deposits formed by winter stors and typhoons would consist of the major part of the Gomso-Bay deposits(Fig. 4).

  • PDF

경북 내성천과 위천의 하도 형상 및 경관 비교 분석 (A Comparative Analysis on Channel Forms and Landscapes at Naeseongcheon River and Wicheon River in Gyeongpook Province)

  • 이광률
    • 한국지형학회지
    • /
    • 제17권4호
    • /
    • pp.1-16
    • /
    • 2010
  • 본 연구는 화강암 유역분지인 내성천과 퇴적암 유역분지인 위천을 대상으로, 하도 지형, 수문, 퇴적물 특성과 하도의 경관 및 지표 피복 특성을 비교·분석하였다. 유역분지의 기반암, 토양, 지표 피복 특성의 차이로 인해, 유속이 느린 위천이 내성천에 비해 하천 수위 변화가 심한 것으로 나타났다. 그리고 입상붕괴된 화강암 퇴적물을 공급 받는 내성천은 상·하류 거의 대부분에서 조립 모래의 입도를 일정하게 나타내고 있지만, 퇴적암 퇴적물이 공급되는 위천은 상류에서 하류로 가면서 평균 입도가 급격히 작아지는 특징을 보인다. 이러한 모래입자 크기의 퇴적물 이동과 준설, 골재 채취 등의 하도 간섭이 활발한 내성천은 위천에 비해 하도 표면의 변화가 심하여 식생 피복이 매우 불량한 것으로 분석되었다.

혼합사로 구성된 하천에서 하상변동 및 유사의 입도분포 계산을 위한 수치모형 개발 (A Numerical Model for Bed Elevation Change and Bed Material Sorting in the Channel of Non-uniform Sediment)

  • 장창래;정관수;김재한
    • 한국수자원학회논문집
    • /
    • 제37권5호
    • /
    • pp.387-395
    • /
    • 2004
  • 본 논문에서는 하상변동 및 유사입자의 시간적 공간적 분포를 동시에 모의할 수 있는 2차원 수치모형을 제시하였다. 사행수로의 하상변동은 만곡부의 외측에서는 하상이 세굴되고 훨씬 더 거친 입경의 재료로 구성되며, 만곡부의 내측에서는 하상이 상승하고, 세립토로 구성되었다. 또한 사행하천에서 흐름의 방향에 대한 입자분포 과정은 상류의 변곡점에서 시작하여, 하류 변곡점에서 마치게 되는 것을 보여주었다. 하천의 경계가 불규칙하고 복잡한 하천에서는 혼합사호 형성된 하천에서보다 균일사로 이루어진 하천에서 하상이 깊게 세굴되는 현상을 보여준다. 혼합사로 이루어진 하천에서의 공간적 입도 분포는 사행하천에서와 마찬가지로 하상이 퇴적되는 사행의 내측에서는 세립토로 구성되고 하상이 세굴되는 외측에서는 굵은 입자로 구성되는 것을 보여주었으며, 하천 폭이 좁은 부분에서는 하상의 세출 및 하상재료가 굵게 변화되는 것을 보여주었다.

기판바이어스 인가에 따른 반응성 마그네트론 스퍼터링에 의한 TiN 코팅 (TiN Coatings by Reactive Magnetron Sputtering Under Various Substrate Bias Voltages)

  • 서평섭;전성용
    • 한국표면공학회지
    • /
    • 제41권6호
    • /
    • pp.287-291
    • /
    • 2008
  • Reactively magnetron sputtered TiN films were deposited on Si wafers under varying bias voltage and characterized by X-ray diffraction, field-emission scanning electron microscopy and Nanoindentation. The films deposited under an Ar + $N_2$ atmosphere exhibited a mixed (200)-(111) orientation with a strong (200) texture, which subsequently changed to a strong (111) texture with increasing bias voltage. The changes in texture and grain size of the TiN thin films are due to one or a combination of factors such as strain energy, surface free energy, surface diffusivity and adatom mobility. The influence of each factor depends on the processing conditions. The average deposition rate and grain size were calculated from FE-SEM images of the films indicating that the deposition rate was lower at the films deposited under bias voltage.

초음파를 이용한 재질열화의 비파괴적 평가 (Nondestructive Evaluation for Material Degradation of 2.25Cr-1Mo steel by Ultrasonic Wave)

  • 김정석;박은수;박인근;김현묵
    • 한국공작기계학회:학술대회논문집
    • /
    • 한국공작기계학회 2000년도 추계학술대회논문집 - 한국공작기계학회
    • /
    • pp.369-374
    • /
    • 2000
  • This study has been achieved on the characteristics of ultrasonic wave in 2.25Cr-1Mo steel to evaluate the feasibility of ultrasonic nondestructive technique on the assessment of aging degradation. The measured values were used find a relationship between the ultrasonic propagation properties and degradation such as coarsening of carbides and precipitates. The ultrasonic attenuation coefficient was mainly affected by the grain size of prior austenitic phase as well as degradation. In this results, degradation and grain size in 2.25Cr-1Mo steel was able to cope with the changes in ultrasonic wave properties by applying the nondestructive evaluation method

  • PDF