• Title/Summary/Keyword: changes of grain size

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Geomorphological Processes of Yuga Alluvial Fan in Korea (유가 선상지의 지형 형성과정)

  • Lee, Gwang-Ryul;Cho, Young Dong
    • Journal of the Korean Geographical Society
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    • v.48 no.2
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    • pp.204-217
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    • 2013
  • This study shows the geomorphological processes of Yuga alluvial fan at Dalseong-gun, Daegu in Korea, based on characteristics of geomorphological surfaces, analysis of geomorphological deposits and OSL age dating. Alluvial fans of this area are classified into three surfaces(YG-F1, YG-F2, YG-F3) and were formed by the depositional processes resulting from the changes in hydraulic geometry of flowing water which was a stream flowing out of mountains debouched on to a plain, not by a sudden decrease in surface gradient of river bed. YG-F3 surface, about 110,000 yr B.P.(MIS 5.4), was formed as Yongri river deposited a lot of debris. This result was due to the process that the deposition took place actively with the upward of base level as the last interglacial period began. Later, the denudation of the river valley and geomorphological surface constantly occurred and the local and seasonal changes were found in precipitation and stream discharge with the beginning of the interstadial of the last glacial stages(MIS 3), leading to YG-F2 formed by debris flow, earth flow, mud flow and stream flow. Then, short-term climate changes and temporal climate events repeatedly caused aggradation and denudation over time and going through these processes, YG-F1 is believed to have been made by earth flow or mudflow during the last glacial maximum(MIS 2).

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Study of Stress Changes in Nanocrystalline Ni Thin Films Eletrodeposited from Chloride Baths (Chloride Bath로부터 전기도금된 나노결정립 니켈 박막의 잔류응력 변화에 대한 연구)

  • Park, Deok-Yong
    • Journal of the Korean Electrochemical Society
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    • v.14 no.3
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    • pp.163-170
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    • 2011
  • Nanocrystalline Ni thin films were electodeposited from chloride baths to investigate the influences of additive concentration, current density and solution pH on residual (or internal) stress, surface morphology, and microstructure of the films. It was observed that residual stress in Ni thin film was changed from tensile stress mode (about 150 MPa) to compressive stress mode (about -100 MPa) with increasing saccharin concentration as an additive. Microstructure of Ni thin films was changed with/without saccharin in baths. Ni thin films electrodeposited from saccharinfree bath mainly consisted of both FCC(111) and FCC(200) phases. However, Ni thin film electrodeposited from the baths containing saccharin exhibited FCC(111), FCC(200) and FCC (311) phases [sometimes, FCC (220)]. Current density influenced residual stress of Ni thin films. It was measured to be the lowest compressive stress value (about-100 MPa) in range of current density of $2.5\sim10mA{\cdot}cm^{-2}$. Solution pH also influenced residual stress of Ni thin film. Addition of saccharin in baths affected grain size of Ni thin films. Grain sizes of Ni thin films were measured to be about 60 nm without saccharin and 24~38 nm with more than 0.0005M saccharin concentration. Surface of Ni thin films was changed from nodular to smooth surface morphology with addition of saccharin.

Microstructure and dielectric properties in the La2O3-doped BaTiO3 system (La2O3 첨가에 따른 BaTiO3의 미세구조 및 유전특성)

  • Choi, Woo-Jin;Moon, Kyoung-Seok
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.30 no.3
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    • pp.103-109
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    • 2020
  • The effect of La2O3 addition on the crystalline phase, microstructure, and dielectric properties of BaTiO3 has been studied as a function of the amounts of La2O3. 0.3 mol% TiO2-excess BaTiO3 powder was synthesized by solid-state reaction, and then the powder compacts with various amounts of La2O3 were sintered at 1250℃ for 2 hours. Room temperature XRD showed changes in the lattice parameters and a decrease of tetragonality (c/a) as the amounts of La2O3 increased. It can be explained that the phase transition from tetragonal to cubic phase occurred because La3+ replaced Ba2+ site, which increased the instability of the tetragonal phase. As La2O3 was added over 0.1 mol%, the critical driving force for growth (Δgc) increased over maximum driving force (Δgmax). As the result, the grain size decreased with La2O3 addition. Dielectric constant decreased as the amounts of La2O3 increased, which was analyzed with crystal structure and microstructure.

Cryogenic microwave dielectric properties of Mg2TiO4 ceramics added with CeO2 nanoparticles

  • Bhuyan, Ranjan K.;Thatikonda, Santhosh K.;Dobbidi, Pamu;Renehan, J.M.;Jacob, Mohan V.
    • Advances in materials Research
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    • v.3 no.2
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    • pp.105-116
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    • 2014
  • The microwave dielectric properties of $CeO_2$ nanoparticles (0.5, 1.0 & 1.5wt%) doped $Mg_2TiO_4$ (MTO) ceramics have been investigated at cryogenic temperatures. The XRD patterns of the samples were refined using the full proof program reveal the inverse spinel structure without any secondary phases. The addition of $CeO_2$ nanoparticles lowered the sintering temperature with enhancement in density and grain size as compared to pure MTO ceramics. This is attributed to the higher sintering velocity of the fine particles. Further, the microwave dielectric properties of the MTO ceramics were measured at cryogenic temperatures in the temperature range of 6.5-295 K. It is observed that the loss tangent ($tan{\delta}$) of all the samples increased with temperature. However, the $CeO_2$ nanoparticles doped MTO ceramics manifested lower loss tangents as compared to the pure MTO ceramics. The loss tangents of the pure and MTO ceramics doped with 1.5 wt% of $CeO_2$ nanoparticles measured at 6.5K are found to be $6.6{\times}10^{-5}$ and $5.4{\times}10^{-5}$, respectively. The addition of $CeO_2$ nanoparticles did not cause any changes on the temperature stability of the MTO ceramics at cryogenic temperatures. On the other hand, the temperature coefficient of the permittivity increased with rise in temperature and with the wt% of $CeO_2$ nanoparticles. The obtained lower loss tangent values at cryogenic temperatures can be attributed to the decrease in both intrinsic and extrinsic losses in the MTO ceramics.

Microscopic characterization of pretransition oxide formed on Zr-Nb-Sn alloy under various Zn and dissolved hydrogen concentrations

  • Kim, Sungyu;Kim, Taeho;Kim, Ji Hyun;Bahn, Chi Bum
    • Nuclear Engineering and Technology
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    • v.50 no.3
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    • pp.416-424
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    • 2018
  • Microstructure of oxide formed on Zr-Nb-Sn tube sample was intensively examined by scanning transmission electron microscopy after exposure to simulated primary water chemistry conditions of various concentrations of Zn (0 or 30 ppb) and dissolved hydrogen ($H_2$) (30 or 50 cc/kg) for various durations without applying desirable heat flux. Microstructural analysis indicated that there was no noticeable change in the microstructure of the oxide corresponding to water chemistry changes within the test duration of 100 days (pretransition stage) and no significant difference in the overall thickness of the oxide layer. Equiaxed grains with nano-size pores along the grain boundaries and microcracks were dominant near the water/oxide interface, regardless of water chemistry conditions. As the metal/oxide interface was approached, the number of pores tended to decrease. However, there was no significant effect of $H_2$ concentration between 30 cc/kg and 50 cc/kg on the corrosion of the oxide after free immersion in water at $360^{\circ}C$. The adsorption of Zn on the cladding surface was observed by X-ray photoelectron spectroscopy and detected as ZnO on the outer oxide surface. From the perspective of $OH^-$ ion diffusion and porosity formation, the absence of noticeable effects was discussed further.

Mechanical Properties of OFC Copper Fabricated by Multi-Axial Diagonal Forging (MADF) (다축대각단조(MADF) 가공한 구리의 기계적 성질)

  • Kwon, S.C.;Kim, S.T.;Kim, D.V.;Lee, J.K.;Seo, S.J.;Yoon, T.S.;Jeong, H.T.
    • Transactions of Materials Processing
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    • v.27 no.4
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    • pp.250-256
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    • 2018
  • Oxygen-free copper (OFC) was prepared as a 90 mm cube and then processed with Multi-Axial Diagonal Forging - Initialization of Prior manufacturing History (MADF). The MADF process has been newly developed as a severe plastic deformation method. The MADF process consists of upset forging with a thickness reduction of 30% and diagonal forging with a diagonal angle of $135^{\circ}$. 1 cycle process consists of a 12 passes forging process. In order to analyze the characteristic changes according to the number of iterations, 1, 2, and 3 cycles of the MADF process were performed. The OFC specimens were MADF processed without surface cracks up to 3 cycles. The microstructure, hardness and tensile test of processed materials were analyzed to study the change of material properties according to the amount of MADF process. The results showed that the MADF process effectively refined the microstructure and increased the strength of OFC. In the case of specimens processed for more than 2 cycles, the grains of all measurement regions were refined to be less than $7{\mu}m$ of grain size. The 1 cycle MADF processed OFC showed the highest mechanical properties with the hardness of 132 HV and tensile strength of 395 MPa. Hardness and strength seemed to be saturated when processed over 2 cycles.

Effect of Austenitizing Temperature and Cooling Rate on Microstructure and Hardness of Low-carbon SCM415 Steel (오스테나이타이징 온도와 냉각 속도가 SCM415 저탄소강의 미세조직과 경도에 미치는 영향)

  • Lee, J.U.;Lee, G.M.;Cha, J.W.;Park, S.H.
    • Transactions of Materials Processing
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    • v.31 no.4
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    • pp.207-213
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    • 2022
  • In this study, variations in the microstructure and hardness of a low-carbon SCM415 steel with austenitizing temperature and cooling rate are investigated. When the austenitizing temperature is lower than the A1 temperature (738.8 ℃) of the SCM415 steel, the microstructures of both the air-cooled and water-cooled specimens consist of ferrite and pearlite, which are similar to the microstructure of the initial specimen. When heat treatment is conducted at temperatures ranging from the A1 temperature to the A3 temperature (822.4 ℃), the microstructure of the specimen changes depending on the temperature and cooling rate. The specimens air- and water-cooled from 750 ℃ consist of ferrite and pearlite, whereas the specimen water-cooled from 800 ℃ consists of ferrite and martensite. At a temperature higher than the A3 temperature, the air-cooled specimens consist of ferrite and pearlite, whereas the water-cooled specimens consist of martensite. At 650 ℃ and 700 ℃, which are lower than the A1 temperature, the hardness decreases irrespective of the cooling rate due to the ferrite coarsening and pearlite spheroidization. At 750 ℃ or higher, the air-cooled specimens have smaller grain sizes than the initial specimen, but they have lower hardness than the initial specimen owing to the increased interlamellar spacing of pearlite. At 800 ℃ or higher, martensitic transformation occurs during water cooling, which results in a significant increase in hardness. The specimens water-cooled from 850 ℃ and 950 ℃ have a complete martensite structure, and the specimen water-cooled from 850 ℃ has a higher hardness than that water-cooled from 950 ℃ because of the smaller size of prior austenite grains.

Effect of Nb Doping on the Dielectric and Strain Properties of Lead-free 0.94(Bi1/2Na1/2)TiO3-0.06BaTiO3 Ceramics

  • Han, Hyoung-Su;Hong, In-Ki;Kong, Young-Min;Lee, Jae-Shin;Jo, Wook
    • Journal of the Korean Ceramic Society
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    • v.53 no.2
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    • pp.145-149
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    • 2016
  • $(Bi_{1/2}Na_{1/2})_{0.94}Ba_{0.06}(Ti_{1-x}Nb_x)O_3$ (BNBTxNb) ceramics were investigated in terms of the crystal structure as well as the ferroelectric, dielectric, and piezoelectric properties. While little change was observed in the microstructure except for a slight decrease in the average grain size, a significant change was noticed in the temperature dependence of dielectric and piezoelectric properties. It was shown that the property changes are closely related to the downward shift in the position of the ferroelectric-to-relaxor transition temperature with increasing amount of Nb doping. A special emphasis is put on the fact that Nb doping is so effective at decreasing the ferroelectric-to-relaxor transition temperature that even at no more than 2 at.% Nb addition, the transition temperature was already brought down slightly below room temperature, resulting in the birth of a large strain at 0.46 %, equivalent to $S_{max}/E_{max}=767pm/V$.

Sedimentologic Characteristics of Tidal Flat Sediments after the Construction of Sea Dyke in Kwangyang Bay, South Coast of Korea (호안 건설 후 광양만 조간대 퇴적물의 퇴적학적 특성)

  • Ryu, Sang-Ock;Sin, Yong-Sik
    • Journal of the Korean earth science society
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    • v.27 no.6
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    • pp.659-669
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    • 2006
  • In Kwangyang Bay, the south coast of Korea, surface sediments and sedimentation rates have been investigated to understand the distribution and variation of tidal flat sediments after the construction of sea dyke. The mean grain size of the surface sediments during autumn is coarser, and decrease from winter to summer except for temporarily coarsening in the early summer. The depositional processes are prevalent in spring, while erosional processes are dominant in summer and autumn. This seasonal variation of sedimentary processes show similar results monitored from 2001 to 2003 before the construction of sea dyke. In the northern area of the bay, net annual sedimentation rates show similar results monitored from 2001 to 2003 before the construction of sea dyke. However, in the western area of the bay, net annual sedimentation rates change from erosion-dominated to deposition-dominated environments. It is considered that the western area of the bay is changed to erosion-dominated environments, as a result of the changes of hydrodynamic conditions, caused by sea dyke construction.

A Processor Allocation Policy using Program Characteristics on Shared Bus (공유 버스상에서 프로그램 특성을 사용한 프로세서 할당 정책)

  • Jeong, In-Beom;Lee, Jun-Won
    • Journal of KIISE:Computer Systems and Theory
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    • v.26 no.9
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    • pp.1073-1082
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    • 1999
  • 본 논문에서는 시스템 내의 프로세서들을 효과적으로 사용하기 위한 적응적 프로세서 할당 정책을 제안한다. 프로그램의 병렬성을 향상시키기 위하여 일반적으로 병렬 처리에 사용될 프로세서 개수를 증가시킨다. 그러나 증가된 프로세서들은 그레인 크기에 변화를 일으키며 이는 캐쉬 성능에 영향을 미친다. 특히 대역이 제한된 공유 버스를 사용하는 시스템에서는 프로세서 개수의 증가는 공유 버스에 대한 접근 경쟁을 크게 증가하므로 버스에서 대기하는 시간이 프로세서 증가에 의한 계산 능력 이득을 상쇄시키는 주요한 원인이 되고 있다. 본 논문에서 제안한 적응적 프로세서 할당 정책은 프로그램이 수행되는 도중에 임의의 기간동안 공유버스에 대기중인 프로세서 분포에 관한 정보를 얻는다. 그리고 이 정보를 바탕으로 프로세서 개수를 변경하는 방법이다. 모의 시험에서 적응적 프로세서 할당 정책은 프로그램들의 버스 트래픽 특성에 따른 최적의 적합한 프로세서 개수를 발견함을 보인다. 그리고 적응적 프로세서 할당 정책은 고정된 프로세서 개수를 사용한 가장 좋은 성능보다는 다소 떨어진 성능을 나타내었으나 시스템의 프로세서 활용성을 높여 효과적 시스템 사용에 기여함을 보인다. Abstract In this paper, the adaptive processor allocation policy is suggested to make effective use of processors in system. To enhance the parallelism, the number of processors used in the parallel computing may be increased. However, increasing the number of processors affects the grain size of the parallel program. Therefore, it affects the cache performance. In particular, when the shared bus is employed, since increasing the number of processors can result in a significant amount of contention to achieve the shared-bus, the increased computing power is offset by the bus waiting time due to these contentions. The adaptive processor allocation policy acquires the information about the distribution of waiting processors on shared bus for any execution period of programs. And it changes the number of processors working in parallel processing during the program's run. Our simulation results show that the adaptive processor allocation policy finds the optimum feasible number of processors based on the bus traffic characteristic of programs. Thus, it contributes to effective system utilization, even though it performs slightly less efficiently than using a fixed number of processors with the best performance.