• 한국염색가공학회지
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• 제29권2호
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• pp.97-103
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• 2017

Polyketone fiber, a newly developed high strength fiber, has a tenacity and modulus similar to the p-aramid fiber, and can be used for reinforcing mechanical rubber goods(MRG), such as tires, hoses, and technical textiles. It will be expected for replacement of super fiber such as aramids and increasing the technical textile market share. This paper surveys the mechanical properties of polyketone fiber for technical textiles. For this purpose, dyed polyketone fabric is prepared, mechanical properties of coated and uncoated polyketone fabrics such as tensile strength, elongation and tear strength were examined before and after weather resistance test(temperature $63{\pm}3^{\circ}C$, humidity 60%, amount of power $0.35w/m^2$). The differences of mechanical properties between uncoated and coated fabrics for high functional technical textiles and composite materials are estimated through this study. The UV-stability of polyketone fabric showed obvious improvement after coating. After 168h(7day) of UV exposure, the coated fabric showed less deterioration in mechanical properties with the retained tensile strength and elongation at break greater than 22 and 17% of the uncoated polyketone fabrics values, respectively.

• 한국수산과학회지
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• 제35권6호
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• pp.696-701
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• 2002

Cellulase를 이용하여 키토산 올리고당을 제조하기 위한 최적조건을 반웅표면 분석법을 이용하여 설정하였다 키토산 분해능과 산업적 활용의 측면에서 유리한 Pen. funiculosum 유래의 cello-lase를 예비 실험을 통해 결정하였다. 이 효소의 적정 반응 조건에서 경시적 키토산 분해율을 측정한 결과, 반응 10시간까지는 대수적 증가를 보였으나, 10시간 이후로는 완만한 분해율을 나타내었다. 중심합성계획에 의해 총 26개의 실험을 행한뒤 반응표면분석법으로 설정한 키토산 분해 최적 조건은 기질 농도 $0.5\%$에 대해 효소 농도 143(U), 반응 온도 $49^{\circ}$, 반응 시간 13.2hr및 pH는 3.8이었다. 본 연구에서 설정된 최적의 조건에서 얻어진 키토산 분해물은 dimer와 trimer가 주된 올리고당이었고, 소량의 tetramer와 hexamer 그리고 monomer 등의 총 8종 정도의 올리고당이 검출되었다.

• Restorative Dentistry and Endodontics
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• 제7권1호
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• pp.77-83
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• 1981

The purpose of this study was to observe the bonding strength between tooth surface (enamel and dentin) and restorative filling materials which are two composite resins (Clearfil and Concise) and Glass ionomer cement, after etching with 50% phoshoric acid and 37% citric acid. To measure the bonding strength in enamel, the labial surface of upper anterior tooth was cut flatly with using carborundum disk and polished with sand paper disk, and to measure in dentin, the dentin surface was prepared by grinding upper part of posterior tooth horizontally. After washing the tooth surface with water and drying with air blast, the prepared tooth surface was etched. In glass ionomer cement, 50% phosphoric acid and 37% citric acid were used, in Clearfil 40% phosphoric acid was used and in Concise, 50% phosphoric acid and 37% citric acid were used as etchant for 1 minute. After the copper band which is 5 mm in diameter and 5 mm in height was fixed on the prepared surface and each filling material was inserted into the copper band, the hooking loop was inserted into filled material in the copper band before setting to make it easily that the load is applied on the specimen. After all specimens were immersed in water at $37^{\circ}C$ for 1 week, this specimen was placed on the load cell of tensile test apparatus, and specimen was pulled at the cross-head speed of 0.8 mm per minute. The following results were obtained 1) In glass ionomer cement, the bond strength obtained by 37% citric acid was higher than one obtained by 50% phosphoric acid in enamel and dentin surfaces. The bond strength obtained in non-etched surface was much less than one by etchants in enamel and dentin surface. 2) In Clearfil, the bond strength obtained by 40% phosphoric acid was 4 times more than one obtained by non etch ant. 3) In Concise, the bond strength obtained by 50% phosphoric acid was almost same as one obtained by 37% citric acid, and the bond strength obtained by non etch ant was much less than one obtained by etchants.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2007년도 추계학술대회 논문집
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• pp.275-275
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• 2007

Two sorts of electrode composed of Sulpur/CNT/PVDF and Silver/CNT/PVDF were prepared by in situ chemical method and their electrochemical performance were evaluated by using cyclic voltammetry, impedance measurement and constant-current charge/discharge cycling technique. Also, composite electrodes were characterized by FE-SEM and BET. Raw materials such as CNT/Silver and CNT/Sulfur were mixed in ethanol, dried. These mixed materials were heated at 900 and $320^{\circ}C$ for 2hr, respectively in order to enhance contact among CNT electrodes. Electric double layer capacitor cells were fabricated using these mixed powder with polymer of PVDF. For the charging and discharging characteristics measured at scan rate of 1 mA/s, Supercapacitor of Sulphur-CNT-PVDF electrode showed a better performance than that of Ag-CNT-PVDF, which seems to be related with lower contact resistance of Sulphur-CNT-PVDF electrode.

• 한국강구조학회 논문집
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• 제17권4호통권77호
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• pp.481-490
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• 2005

본 논문은 중력하중의 지배를 받는 CFT기둥-RC 무량판 접합부의 실물대 실험결과를 요약한 것이다. CFT구조는 여러 가지 구조 및 시공상의 장점으로 인하여 국내 건설 현장에서 상대적으로 짧은 시간에 폭넓게 수용되고 있다. 주차장 용도로 주로 사용되는 지하층은 철근콘크리트 무량판으로 시공하여 경제성을 도모하는 것이 국내에서 일반적으로 요구되는 시공관행이다. 그러나 CFT기둥-RC 무량판 접합부의 효율적인 디테일은 아직 국내 외적으로 제시된 바가 없어서 이 분야의 연구가 매우 필요한 실정이다. 현장 시공시 경제성을 극대화할 수 있는 몇 가지 전략을 기초로 해서, 여러 가지 접합 상세를 제안하였고 실험을 통하여 검증하였다. 실험결과 본 연구에서 제시된 CFT기둥-RC 무량판 접합 상세의 펀칭강도 및 강성이 RC 무량판 접합부와 동등하거나 이를 상회하는 것을 확인할 수 있었다.

• 한국강구조학회 논문집
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• 제25권2호
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• pp.209-222
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• 2013

800MPa급 강재와 100MPa급 콘크리트를 적용한 매입형 합성기둥에 대하여 편심압축실험을 수행하였다. 강재단면의 모멘트팔길이와 변형(응력)을 증가시켜 고강도강재의 성능활용을 극대화할 수 있도록, ㄱ형 강재단면을 네 모서리에 집중 배치한 후, 래티스철근, 링크철근, 띠판을 이용하여 일체화하였다. 이 경우 강재단면의 강력한 횡구속효과로 인해 심부콘크리트의 성능도 개선된다. 실험결과 ㄱ형 강재 매입형 기둥은 H형 강재 매입형 기둥에 비하여 최대강도와 유효휨강성이 1.4배 이상 증가하였다.

• 한국재료학회지
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• 제22권7호
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• pp.362-367
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• 2012

Magnetite nanoparticles(NPs) have been the subject of much interest by researchers owing to their potential use as magnetic carriers in drug targeting and as a tumor treatment in cases of hyperthermia. However, magnetite nanoparticles with 10 nm in diameter easily aggregate and thus create large secondary particles. To disperse magnetite nanoparticles, this study proposes the infiltration of magnetite nanoparticles into hybrid silica aerogels. The feasible dispersion of magnetite is necessary to target tumor cells and to treat hyperthermia. Magnetite NPs have been synthesized by coprecipitation, hydrothermal and thermal decomposition methods. In particular, monodisperse magnetite NPs are known to be produced by the thermal decomposition of iron oleate. In this study, we thermally decomposed iron acetylacetonate in the presence of oleic acid, oleylamine and 1,2 hexadecanediol. We also attempted to disperse magnetite NPs within a mesoporous aerogels. Methyltriethoxysilicate(MTEOS)-based hybrid silica aerogels were synthesized by a supercritical drying method. To incorporate the magnetite nanoparticles into the hybrid aerogels, we devised two methods: adding the synthesized aerogel into a magnetite precursor solution followed by nucleation and crystal growth within the pores of the aerogels, and the infiltration of magnetite nanoparticles synthesized beforehand into aerogel matrices by immersing the aerogels in a magnetite nanoparticle colloid solution. An analysis using a vibrating sample magnetometer showed that approximately 20% of the magnetite nanoparticles were well dispersed in the aerogels. The composite samples showed that heating under an inductive magnetic field to a temperature of $45^{\circ}C$ is possible.

• 한국식품조리과학회지
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• 제21권6호통권90호
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• pp.823-828
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• 2005

비만방지 및 성인병 예방식품의 일환으로 메밀국수를 제조하는 과정에서 glucomannan, RS전분 등을 처리하여 열량까지 낮춘 새로운 타입의 메밀국수 제조조건을 확립하고자 하였다. 밀가루 단독으로 제조한 생면에 비하여 몇 가지 원료를 처리한 메밀생면의 열량은 약 $30\%$ 수준의 감소효과가 있었다. 제조된 메밀국수를 조리 후 최근 웰빙식품의 일환으로 각광 받고 있는 올리브유를 coating하여 퍼짐성을 방지하고 90일까지 상온에서 유통이 가능한 즉석국수 타입의 메밀국수를 제조할 수 있었다. 원재료 배합비율은 4종의 시료 중 RS전분 함유 밀가루, 메밀가루, glucomannan을 주원료로 하여 여기에 활성글루텐과 유화제를 처리한 것이 가장우수하였으며, 식염은 처리하지 않은 것의 품질특성이 우수하였다. 포장재질은 6종을 검토한 결과 단독재질보다는 OPP/Al/PE의 복합다층필름을 포장재로 이용하는 것이 가장 우수한 것으로 밝혀졌다.

• Restorative Dentistry and Endodontics
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• 제21권2호
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• pp.585-601
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• 1996

The purpose of this study was to elucidate the effect of blood-and saliva-contamination during dentin pretreatment procedure on tensile bond strength, and to investigate the effect of contaminant-removing treatments on the recovery of bond strength of dentin bonding agents. Dentin specimens prepared from freshly extracted bovine mandibular anterior teeth were divided into non-contaminated control and contaminated experimental groups. The specimens of the contaminated group were contaminated with saliva or blood after etching or priming procedure, followed by contaminant-removing treatments. All the specimens were bonded with All Bond$^{(R)}$ 2 dentin bonding agent and Bisfil$^{TM}$ composite resin or Scotchbond$^{TM}$ Multipurpose and Z100. After all the bonded specimens were stored in $37^{\circ}C$ distilled water for 24 hours, tensile bond strengths were measured. The contaminated dentin and fractured dentin surfaces were examined under the scanning electron microscope. The results were as follows : Contaminated specimens showed lower bond strength than non-contaminated ones regardless of the kind of contaminant, contamination time and contaminant-removing treatments, except specimens which were acid-etched following saliva contamination after etching in All Bond$^{(R)}$ 2 groups (p<0.05). Blood contaminant resulted in much bond strength decrease than saliva ones (p<0.01), and contamination after priming resulted in much decrease in bond strength than after etching (p<0.01). Re-etching resulted in increase of bond strength in the specimens contaminated with saliva after etching but not in blood contaminated ones. Re-priming resulted in increase of bond strength in the specimens contaminated after priming regardless of the kind of contaminant.

• Restorative Dentistry and Endodontics
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• 제21권2호
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• pp.569-584
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• 1996

The purpose of this study was to elucidate the effect of benzalkonium chloride on tensile bond strength of BPDM/HEMA dentin bonding. One hundred sixty dentin specimens from freshly extracted bovine mandibular incisors were used, and 0, 0.02, 0.1 or 0.5% benzalkonium chloride solution was applied to the dentin specimen with/after phosphoric acid. 32% phosphoric acid was used when the specimens were bonded with One-Step$^{TM}$, a BPDM/HEMA system and 10% was used when bonded with All-Bond$^{(R)}$ 2, a NTG-GMA/BPDM system. Aelitefil$^{TM}$ composite resin was bonded to the pretreated dentin specimen with the use of All-Bond$^{(R)}$ 2 or One-Step$^{TM}$ dentin bonding agent. After the bonded specimens were stored in $37^{\circ}C$ distilled water for 24 hours, tensile bond strength was measured. The fractured dentin specimens were examined under the scanning electron microscope. The results were as follows : Benzalkonium chloride application after acid-treatment resulted in decrease of dentin bond strength of One-Step$^{TM}$, a BPDM/HEMA system (p>0.05). Benzalkonium chloride application did not exert any influence on dentin bond strength of All-Bond$^{(R)}$ 2, a NTG-GMA/BPDM system (p>0.05). There was no relationship between the concentration or application method of benzalkonium chloride and the dentin bond strength of One-Step$^{TM}$ or All-Bon$^{(R)}$ 2 (p<0.05). On SEM examination of the fractured dentin-resin interface, while mixed failure was prominent in dentin bonding with One-Step$^{TM}$, adhesive and mixed failures were seen together in dentin bonding with All-Bond$^{(R)}$ 2 regardless of the concentration and application method of benzalkonium chloride.