• 제목/요약/키워드: bonding temperature

검색결과 1,060건 처리시간 0.031초

FDM 방식을 활용한 3D 프린팅 복합직물의 박리강력 측정 연구 (Study on Peel Strength Measurement of 3D Printing Composite Fabric by Using FDM)

  • 한유정;김종준
    • 패션비즈니스
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    • 제23권2호
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    • pp.77-88
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    • 2019
  • One way of appling 3D printing to garments is through the combination of 3D polymer filaments in textile fabrics. it is essential to understand the interface between the polymer and the 3D composite fabric in order to enhance the adhesion strength between the polymers and the peeling strength between the fabric and the polymer. In this study, the adhesion of composite printed specimens using a combination of fabric and polymers for 3D printing was investigated, and also the change in adhesion was investigated after the composite fabric printed with polymers was subjected to constant pressure. Through this process, the aims to help develop and utilize 3D printing textures by providing basic data to enhance durability of 3D printing composite fabrics. The measure of the peeling strength of the composite fabric prepared by printing on a fabric using PLA, TPU, Nylon polymer was obtained as follows; TPU polymer for 3D printing showed significantly higher peel strength than polymers of composite fabric using PLA and Nylon polymer. In the case of TPU polymer, the adhesive was crosslinked because of the reaction between polyurethane and water on the surface of the fabric, thus increasing the adhesion. It could be observed that the adhesion between the polymer and the fiber is determined more by the mechanical effect rather than by its chemical composition. To achieve efficient bonding of the fibers, it is possible to modify the fiber surface mechanically and chemically, and consider the deposition process in terms of temperature, pressure and build density.

Effect of chemical concentrations on strength and crystal size of biocemented sand

  • Choi, Sun-Gyu;Chu, Jian;Kwon, Tae-Hyuk
    • Geomechanics and Engineering
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    • 제17권5호
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    • pp.465-473
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    • 2019
  • Biocementation due to the microbially induced calcium carbonate precipitation (MICP) process is a potential technique that can be used for soil improvement. However, the effect of biocementation may be affected by many factors, including nutrient concentration, bacterial strains, injection strategy, temperature, pH, and soil type. This study investigates mainly the effect of chemical concentration on the formation of calcium carbonate (e.g., quantity, size, and crystalline structure) and unconfined compressive strength (UCS) using different treatment time and chemical concentration in the biotreatment. Two chemical concentrations (0.5 and 1.0 M) and three different treatment times (2, 4, and 8 cycles) were studied. The effect of chemical concentrations on the treatment was also examined by making the total amount of chemicals injected to be the same, but using different times of treatment and chemical concentrations (8 cycles for 0.50 M and 4 cycles for 1.00 M). The UCS and CCC were measured and scanning electron microscopy (SEM) analysis was carried out. The SEM images revealed that the sizes of calcium carbonate crystals increased with an increase in chemical concentrations. The UCS values resulting from the treatments using low concentration were slightly greater than those from the treatments using high concentration, given the CCC to be more or less the same. This trend can be attributed to the size of the precipitated crystals, in which the cementation efficiency increases as the crystal size decreases, for a given CCC. Furthermore, in the high concentration treatment, two mineral types of calcium carbonate were precipitated, namely, calcite and amorphous calcium carbonate (ACC). As the crystal shape and morphology of ACC differ from those of calcite, the bonding provided by ACC can be weaker than that provided by calcite. As a result, the conditions of calcium carbonate were affected by test key factors and eventually, contributed to the UCS values.

활성탄 흡착탑의 실용화를 위한 최적 유동특성 선정 및 열처리 조건에 따른 황화수소 포집능 향상 연구 (Investigation of Optimum Condition of Heat Treatment and Flow to Improve H2S Adsorption Capacity for Practical use of an Activated Carbon Tower)

  • 장영희;김봉환;김성수
    • 공업화학
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    • 제32권1호
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    • pp.91-96
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    • 2021
  • 본 연구에서는 다양한 환경 공정에서 사용되는 황화수소 제거용 흡착탑 효율을 향상시키기 위해 유동 분석 및 흡착성능 향상 연구를 수행하였다. 연구를 위해 상업적으로 이용 가능한 다양한 활성탄에 칼륨(potassium, K)을 담지하여 개질 활성탄을 제조하였다. 또한 열처리 여부에 따라 흡착 성능과 열처리 과정에서 변화된 표면 특성 사이의 높은 상관관계를 고찰하고자 하였다. 함침법을 통해 K로 코팅된 활성탄은 57배 이상의 흡착 성능을 확인하였다. 이는 균일한 기공 형성과 탄소 표면의 K의 강한 결합은 황화수소의 화학적 및 물리적 흡수에 기여한다고 판단하였다. 다양한 상용 활성탄의 표면 구조에 대한 SEM 분석은 열처리를 통한 표면 특성의 변형으로 인해 기공 구조가 파괴되어 흡수 성능이 저하되는 것으로 확인하였다. 각 활성탄의 압력 손실 특성은 입자 크기와 모양에서 가장 낮은 압력 손실이 관찰되었다. 따라서 2~4 mesh 크기의 탄소입자 범위와 불규칙한 모양이 흡착탑의 성능을 향상시키고 경제적 효율성을 확보할 수 있다고 제안하였다.

Effect of pumice powder and artificial lightweight fine aggregate on self-compacting mortar

  • Etli, Serkan;Cemalgil, Selim;Onat, Onur
    • Computers and Concrete
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    • 제27권3호
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    • pp.241-252
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    • 2021
  • An experimental program was conducted to investigate the fresh properties, mechanical properties and durability characteristics of the self-compacting mortars (SCM) produced with pumice powder and Artificial Lightweight Fine Aggregate (aLWFA). aLWFA was produced by using fly ash. A total of 16 different mixtures were designed with a constant water-binder ratio of 0.37, in which natural sands were partially replaced with aLWFA and pumice powder at different volume fractions of 5%, 10% and 15%. The artificial lightweight aggregates used in this study were manufactured through cold bonding pelletisation of 90% of class-F fly ash and 10% of Portland cement in a tilted pan with an ambient temperature and moisture content. Flowability tests were conducted on the fresh mortar mixtures beforehand, to determine the self-compacting characteristics on the basis of EFNARC. To determine the conformity of the fresh mortar characteristics with the standards, mini-slump and mini-V-funnel tests were carried out. Hardened state tests were conducted after 7, 28 and 56 days to determine the flexural strength and axial compressive strength respectively. Durability, sorptivity, permeability and density tests were conducted at the end of 28 days of curing time. The test results showed that the pumice powder replacement improved both the fresh state and the hardened state characteristics of the mortar and the optimum mixture ratio was determined as 15%, considering other studies in the literature. In the aLWFA mixtures used, the mechanical and durability characteristics of the modified compositions were very close to the control mixture. It is concluded in this study that mixtures with pumice powder replacement eliminated the negative effects of the aLWFA in the mortars and made a positive contribution.

AlInGaN - based multiple quantum well laser diodes for Blu-ray Disc application

  • O. H. Nam;K. H. Ha;J. S. Kwak;Lee, S.N.;Park, K.K.;T. H. Chang;S. H. Chae;Lee, W.S.;Y. J. Sung;Paek H.S.;Chae J.H.;Sakong T.;Kim, Y.;Park, Y.
    • 한국재료학회:학술대회논문집
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    • 한국재료학회 2003년도 추계학술발표강연 및 논문개요집
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    • pp.20-20
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    • 2003
  • We developed 30 ㎽-AlInGaN based violet laser diodes. The fabrication procedures of the laser diodes are described as follows. Firstly, GaN layers having very low defect density were grown on sapphire substrates by lateral epitaxial overgrowth method. The typical dislocation density was about 1-3$\times$10$^{6}$ /$\textrm{cm}^2$ at the wing region. Secondly, AlInGaN laser structures were grown on LEO-GaN/sapphire substrates by MOCVD. UV activation method, instead of conventional annealing, was conducted to achieve good p-type conduction. Thirdly, ridge stripe laser structures were fabricated. The cavity mirrors were formed by cleaving method. Three pairs of SiO$_2$ and TiO$_2$ layers were deposited on the rear facet for mirror coating. Lastly, laser diode chips were mounted on AlN submount wafers by epi-down bonding method. The lifetime of the laser diodes was over 10,000 hrs at room temperature under automatic power controlled condition. We expect the performance of the LDs to be improved by the optimization of the growth and fabrication process. The detailed characteristics and important issues of the laser diodes will be discussed at the conference.

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비파괴 기법을 이용한 스마트 복합재료의 열충격손상평가 (Evaluation on Thermal Shock Damage of Smart Composite using Nondestructive Technique)

  • 이진경;박영철;이규창;이준현
    • Composites Research
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    • 제20권3호
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    • pp.37-42
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    • 2007
  • 금속복합재료에서는 강화재와 기지재 사이의 열팽창계수 차이에 의해 복합재료 내부에 잔류응력이 남아있어 복합재료 전체의 강도저하를 가져온다. 본 연구에서는 TiNi 형상기억합금을 강화재료로써 이러한 잔류응력 문제를 해결하기 위하여 이용하였다. TiNi 형상기억합금은 형상기억효과를 이용하여 복합재료의 잔류응력문제를 해결할 뿐만 아니라 복합재료의 인장강도를 증가시키는 역할을 한다. 핫프레스 방법에 의해 제작된 형상기억복합재료의 강도증가를 위하여 냉간압연을 실시하여 실험을 실시하였다. 이와 같이 제작된 형상기억복합재료의 저온에서의 미시적 손상거동을 평가하기 위하여 음향방출기법을 이용하였다. 또한 열충격을 받은 시험편의 손상에 대한 연구도 이루어졌다.

인장 시험을 이용한 열가소성 복합재료 유도용접 전단강도 평가방법에 대한 고찰 (A Study on the Evaluation Method of Lap Shear Strength for Induction Welding of Thermoplastic Composites using Tensile Test)

  • 백인석;이석순
    • 항공우주시스템공학회지
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    • 제16권1호
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    • pp.12-16
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    • 2022
  • 유도 용접은 비접촉식으로 깨끗하고 빠른 공정으로 현재 주목받고 있다. 하지만 열가소성 수지는 전자기장에 영향을 받지 않기 때문에 유도 용접은 서셉터(Susceptor)라는 발열체가 필요하다. 고품질 접합을 목표로 연구가 진행되고 있지만, 결국 발열체라는 이물질이 들어가기 때문에 기준이 필요하다. 시편의 제작과 시험은 ASTM D5868에 근거하여 진행된다. 본 논문에서 평가 기준은 용접된 접합면의 상태와 기공률, 전단강도로 총 3가지를 근거로 판단할 것을 제안한다. 용접되는 접착면은 용융되고 냉각되면서 고형화가 되기 때문에 급격한 온도 변화는 기공을 발생시킬 수 있다. 또한 가열이 균일하지 않다면 원하는 성능을 기대하기 힘들다. PA6 (CF 30%) 엔지니어링 플라스틱을 이용하여 서셉터 제작과 유도 용접 그리고 성능 검증으로 진행하였다.

RF 열플라즈마를 이용한 이차전지 음극재용 탄소나노실리콘복합소재 합성 (Synthesis of Carbon Nano Silicon Composites for Secondary Battery Anode Materials Using RF Thermal Plasma)

  • 이순직;김대신;연정미;박원규;신명선;최선용;주성후
    • 한국재료학회지
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    • 제33권6호
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    • pp.257-264
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    • 2023
  • To develop a high capacity lithium secondary battery, a new approach to anode material synthesis is required, capable of producing an anode that exceeds the energy density limit of a carbon-based anode. This research synthesized carbon nano silicon composites as an anode material for a secondary battery using the RF thermal plasma method, which is an ecofriendly dry synthesis method. Prior to material synthesis, a silicon raw material was mixed at 10, 20, 30, 40, and 50 wt% based on the carbon raw material in a powder form, and the temperature change inside the reaction field depending on the applied plasma power was calculated. Information about the materials in the synthesized carbon nano silicon composites were confirmed through XRD analysis, showing carbon (86.7~52.6 %), silicon (7.2~36.2 %), and silicon carbide (6.1~11.2 %). Through FE-SEM analysis, it was confirmed that the silicon bonded to carbon was distributed at sizes of 100 nm or less. The bonding shape of the silicon nano particles bonded to carbon was observed through TEM analysis. The initial electrochemical charging/discharging test for the 40 wt% silicon mixture showed excellent electrical characteristics of 1,517 mAh/g (91.9 %) and an irreversible capacity of 133 mAh/g (8.1 %).

A comparative experimental study on the mechanical properties of cast-in-place and precast concrete-frozen soil interfaces

  • Guo Zheng;Ke Xue;Jian Hu;Mingli Zhang;Desheng Li;Ping Yang;Jun Xie
    • Geomechanics and Engineering
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    • 제36권2호
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    • pp.145-156
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    • 2024
  • The mechanical properties of the concrete-frozen soil interface play a significant role in the stability and service performance of construction projects in cold regions. Current research mainly focuses on the precast concrete-frozen soil interface, with limited consideration for the more realistic cast-in-place concrete-frozen soil interface. The two construction methods result in completely different contact surface morphologies and exhibit significant differences in mechanical properties. Therefore, this study selects silty clay as the research object and conducts direct shear tests on the concrete-frozen soil interface under conditions of initial water content ranging from 12% to 24%, normal stress from 50 kPa to 300 kPa, and freezing temperature of -3℃. The results indicate that (1) both interface shear stress-displacement curves can be divided into three stages: rapid growth of shear stress, softening of shear stress after peak, and residual stability; (2) the peak strength of both interfaces increases initially and then decreases with an increase in water content, while residual strength is relatively less affected by water content; (3) peak strength and residual strength are linearly positively correlated with normal stress, and the strength of ice bonding is less affected by normal stress; (4) the mechanical properties of the cast-in-place concrete-frozen soil interface are significantly better than those of the precast concrete-frozen soil interface. However, when the water content is high, the former's mechanical performance deteriorates much more than the latter, leading to severe strength loss. Therefore, in practical engineering, cast-in-place concrete construction is preferred in cases of higher negative temperatures and lower water content, while precast concrete construction is considered in cases of lower negative temperatures and higher water content. This study provides reference for the construction of frozen soil-structure interface in cold regions and basic data support for improving the stability and service performance of cold region engineering.

열가소성수지 필름의 적층방법에 따른 합판의 접착성능 (Adhesion Performance of Plywoods Prepared with Different Layering Methods of Thermoplastic Resin Films)

  • 강은창;이상민;박종영
    • Journal of the Korean Wood Science and Technology
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    • 제45권5호
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    • pp.559-571
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    • 2017
  • 본 연구에서는 열가소성수지 필름의 사용량과 적층방향에 따른 합판의 접착성능을 알아보고자 하였다. 사용된 표판과 이판은 열대산 활엽수 잡목(Mixed light hardwood) 단판과 심판은 라디에타파인(Pinus radiata D. Don) 단판을 사용하였다. 필름은 폴리프로필렌(Polypropylene, PP) 필름과 폴리에틸렌(Polyethylene, PE) 필름을 사용하였다. 먼저 PP와 PE 필름의 특성을 알아보기 위하여 열분석과 인장강도를 조사하였다. 그 결과, PP 필름과 PE 필름의 용융온도는 $163.4^{\circ}C$, $109.7^{\circ}C$였으며, 결정화온도는 $98.9^{\circ}C$, $93.6^{\circ}C$로 나타났다. 각 필름별 인장강도와 신장률은 길이방향보다 폭방향이 더 큰 것으로 나타났다. 필름의 특성을 고려하여, 필름 사용량에 대한 시험은 단판 상에 목표두께별로 필름을 적층하는 방법으로 실시하였다. 그리고 필름의 적층방향에 따른 시험은 단판의 목리방향을 기준으로 필름의 길이방향과 폭방향을 구분하여 각각 적층한 후 합판을 제조하였다. 각각 제조된 합판으로 접착성능을 시험한 결과, 준내수 인장 전단 접착력은 PP 필름의 두께가 0.05 mm 이상, PE 필름은 0.10 mm 이상일 때 KS기준을 만족하였다. 내수 인장 전단 접착력은 PP 필름 두께가 0.20 mm일 때 KS기준을 상회하였다. 필름의 적층방향별 접착성능 시험에서, 단판의 목리방향과 필름의 폭방향으로 적층했던 합판은 필름의 길이방향으로 적층했던 합판보다 더 우수한 결과를 보였다. 현미경으로 관찰된 합판의 표면과 접착층에서 열가소성수지가 단판 내부와 할렬부위로 침투하여 기계적 결합을 이룬 것으로 확인되었다.