• Title/Summary/Keyword: batch test

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Potential Environmental Influences in Soil by Accidental Fluorine (F) Leakage, Using Leaching Test (용출시험을 통한 불산 누출사고지역의 토양 내 불소(F)의 거동특성)

  • Kim, Doyoung;Lee, Junseok;Kwon, Eunhye;Lee, Hyun A;Yoon, Hye-On;Lee, Sanghoon
    • Journal of Korean Society of Environmental Engineers
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    • v.37 no.4
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    • pp.234-239
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    • 2015
  • Various leaching tests were applied to the soil affected by accidental leakage of HF in an industrial area in Korea. Three different leaching methods including pH-stat, continuous batch leaching, and column tests were adopted to assess leaching characteristics and mobility of fluorine(F) in soil and the potential risks to ecosystem. Both natural and spiked samples were used for the leaching tests. F concentrations in the batch tests increased by leaching rapidly in the early stage of leaching and then maintained rather constant levels. Column leaching test also show similar result to that of the batch test. pH also controlled the leaching behavior of the soil. With increasing pH, more F was released in the pH-stat test. This is mainly due to the competition and exchange with hydroxyl ions, as pH increase to the alkaline range. Most of the F released by the accident seem to have removed in the very early stage of leaching, whereas some natural proportion from soil minerals are thought to have been released very slowly. Therefore, little F released during the accident remained, based on the results of this study on the samples after two years of the accident. We could conclude that soil contaminated by external effects such as chemical accidents should be managed immediately, especially with F.

Comparison of Batch Assay and Random Assay Using Automatic Dispenser in Radioimmunoassay (핵의학 체외 검사에서 자동분주기를 이용한 Random Assay 가능성평가)

  • Moon, Seung-Hwan;Lee, Ho-Young;Shin, Sun-Young;Min, Gyeong-Sun;Lee, Hyun-Joo;Jang, Su-Jin;Kang, Ji-Yeon;Lee, Dong-Soo;Chung, June-Key;Lee, Myung-Chul
    • Nuclear Medicine and Molecular Imaging
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    • v.43 no.4
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    • pp.323-329
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    • 2009
  • Purpose: Radioimmunoassay (RIA) was usually performed by the batch assay. To improve the efficiency of RIA without increase of the cost and time, random assay could be a choice. We investigated the possibility of the random assay using automatic dispenser by assessing the agreement between batch assay and random assay. Materials and Methods: The experiments were performed with four items; Triiodothyronine (T3), free thyroxine (fT4), Prostate specific antigen (PSA), Carcinoembryonic antigen (CEA). In each item, the sera of twenty patients, the standard, and the control samples were used. The measurements were done 4 times with 3 hour time intervals by random assay and batch assay. The coefficient of variation (CV) of the standard samples and patients' data in T3, fT4, PSA, and CEA were assessed. ICC (Intraclass correlation coefficient) and coefficient of correlation were measured to assessing the agreement between two methods. Results: The CVs (%) of T3, fT4, PSA, and CEA measured by batch assay were 3.2$\pm$1.7%, 3.9$\pm$2.1%, 7.1$\pm$6.2%, 11.2$\pm$7.2%. The CVs by random assay were 2.1$\pm$1.7%, 4.8$\pm$3.1%, 3.6$\pm$4.8%, and 7.4$\pm$6.2%. The ICC between the batch assay and random assay were 0.9968 (T3), 0.9973 (fT4), 0.9996 (PSA), and 0.9901 (CEA). The coefficient of correlation between the batch assay and random assay were 0.9924(T3), 0.9974 (fT4), 0.9994 (PSA), and 0.9989 (CEA) (p<0.05). Conclusion: The results of random assay showed strong agreement with the batch assay in a day. These results suggest that random assay using automatic dispenser could be used in radioimmunoassay.

A Study on the Monodispersed Silica Fine Particles Prepared by Using Batch-Semibatch Mixed Process (회분과 반회분의 혼합형 공정에 의해 생성된 단분산 실리카 미립자에 관한 연구)

  • Kim, Ki Do;Kim, Hee Taik
    • Applied Chemistry for Engineering
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    • v.10 no.8
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    • pp.1180-1185
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    • 1999
  • Modispersed silica fine particles were produced from the hydrolysis of $Si(OC_2H_5)_4$ by using batch-semibatch mixed systems. Four types of mixed process, i.e., batch-batch, batch-semibatch, semibatch-batch, semibatch-semibatch, were used in order to measure mean particle size, particle size distribution, yield, and packing density. As a result of the test, silica particles prepared by semibatch-semibatch process were larger than those prodeced from any other systems in particle size and yield. On the other hand, silica particles prepared by batch-semibatch process were better than those produced from any other systems in particle size distribution and packing density. Especially, it was found that particle size of $SiO_2$ prepared by semibatch-batch process decreased with increasing the reaction time. Therefore, batch-semibatch process was a successful method for controlling the size, i.e., a narrow distribution of a particle size which ranges to several microns.

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양이온 물질로 오염된 지하수 정화를 위한 반응벽체 개발 : 제올라이트의 적용성 평가

  • 이승학;이재원;김시현;박준범;박상권
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 2001.09a
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    • pp.23-26
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    • 2001
  • Batch test and column test were performed to develop the design factors for PRBs against the contaminated groundwater by ammonium and lead. Clinoptilolite, one of the natural zeolites having excellent cation exchange capacity(CEC), was chosen as the reactive material through the ion-exchange mechanism. In the batch test, the reactivity of Clinoptilolite to ammonium and lead was examined with varying the particle size of Clinoptilolite. The nit weight of Clinoptilolite showed removal efficiencies of 65 % against the ammonium and 98% against lead. The effect of particle size of Clinoptilolite was not noticeable. In the column test, the permeability was examined using flexible-wall permeameters with varying the particle size of Clinoptilolite. When the washed Clinoptilolite having the diameter of 0.42-0.85 nm was mixed with Jumunjin sands in 20:80 ratio (w/w), the highest permeability of 2$\times$10$^{-3}$ -7 x 10$^{-4}$ cm/s was achieved. The reactivity and the strength property of the mixed material were investigated using fixed wall column having 8 sampling ports on the wall and the direct shear test, respectively. Clinoptilolite was found to be a suitable material for PRBs against the contaminated groundwater with ammonium and/or heavy metals.

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An Experimental Study on the Performance Evaluation Method of Padder Roll by Hydraulic Multi Cell with Acceleration Test (유압제어식 멀티셀 패더롤의 가속시험을 통한 성능평가 기법 연구)

  • Cho, Kyung Chul;Lee, Eun Ha;Park, Si Woo;Kim, Soo Youn
    • Journal of Drive and Control
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    • v.15 no.3
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    • pp.43-48
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    • 2018
  • The hydraulic control valve, used in the CPB (cold-pad-Batch) cold dyeing system, passes through a pressurized material that absorbs the dye. The hydraulic control of the hydraulic control panel shall be driven in a uniform and precisely controlled manner, as it interferes directly with the dyschromatism. In this study, an acceleration test model was employed to verify the durability of the hydraulic control of the hydraulic control panel, which was manufactured by the scenic model, and the pre-roll angle was analyzed before the performance of acceleration test. Based on the change in the amount of deformation of the padder roll the durability of the padder roll was analyzed along with verification of the durability of the skin and the rubber coating in contact with the fabric. Furthermore, the accelerated test method used for hydraulic controlled multi-cell padder rolls was verified.

The behavior characteristics of immobilized sludge in waste water treatment using sequencing batch reactor(SBR). (연속 회분식 반응기를 이용한 폐수처리에서 고정화 슬러지의 거동 특성)

  • 최석순
    • Journal of environmental and Sanitary engineering
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    • v.11 no.2
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    • pp.1-7
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    • 1996
  • The behavior of total organic carbon (TOC) and phosphate were observed for 15 days with immobilized activated sludge using polyacrylamide (PAA) by sequencing batch reactor (SBR). In the preparation of immobilized sludge by PAA, it was found that suitable acrylamide concentration for actual wastewater treatment was to be 15% through the batch test. When SBR system was operated in the repeated aerobic and anaerobic conditions, TOC removal efficiency was 92%. The uptake rate of phosphate was increased from 1.78 mg-P/g cell/hr on the 5th day of acclimation to 2.5 mg-P/g cell/hr on the 15th day of acclimation. And the total phosphorus content in PAA bead was increased from 40 mg-P/g cell on the 1st day of operation to 55 mg-P/g cell on the 15th day of operation. From this study, lowering the volume of aeration tank was possible when PAA bead was used in wastewater treatment and long operation was also possible without the settler.

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Statistical Inference of Shelf -life in Drug's Stability Study (의약품 안정성 연구에서의 사용기간에 관한 통계적 추론)

  • Kim, Tai-Kyoo;Park, Sang-Gue
    • Journal of Korean Society for Quality Management
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    • v.36 no.1
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    • pp.1-6
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    • 2008
  • The purpose of stability study of pharmaceutical products is to establish the shelf life based on the change of the quality with time. Stability study generally consists of a random sample of dosage units from a batch or several batches placed in a storage room and periodically assayed for their drug content. The statistical methods of assessing the shelf-life of drug in the market is considered with the current KFDA regulations. An illustrated application to some stability data from the pharmaceutical industry is also presented with the discussion.

Double-stage Batch Fermentation of Beer Part II. Trials under Plant Fermention Conditions (이단회분식 맥주발효 제II보 공장발효조건하에서의 시양)

  • Pack, M.Y.
    • Microbiology and Biotechnology Letters
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    • v.3 no.2
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    • pp.89-93
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    • 1975
  • In order to ferment beer more effectively under conditions similar to the conventional batch fermentation, a part of the wort which had been fermenting for three days was replaced with un-pitched fresh wort and completed the rest of the fermentation in four to six days. The taste test panel accepted the beers fermented for five days after diluting with one third or one half volume of freshl wort giving fermentation efficiency gains by 22% or 28% over the regular nine-day batch fermentation respectively.

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A Study on the Compressive Strength & Pore Structure of Shotcrete using for Mine Ready-mixed Materials (광산용 레디믹스트 재료를 사용한 숏크리트의 압축강도 및 공극구조에 대한 고찰)

  • Lee, Heung-Soo;Kim, Dong-Min;Choi, Seung-Kyung;Lee, Ju-Hoe
    • Proceedings of the Korean Geotechical Society Conference
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    • 2009.09a
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    • pp.1517-1521
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    • 2009
  • A variation of pore structure of shotcrete matrix was experimented by Mercury Intrusion Porosimetry, and the relation with compressive strength was also examined. As a result of the Mercury Intrusion Porosimetry(MIP) test, RM-P1 Batch the macropore diameter of the RM-BFS2 and RM-BFS3 Batch than to have a relatively macropore can see a lot of long-term durability performance degradation. Also, K and N Batch the current is applied to the mine if the factors on shotcrete durability performance of the macropore volume of the entire appears to be a long-term durability performance in the fall.

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