• 대한화학회지
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• 제10권3호
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• pp.133-135
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• 1966

Stainless steel 속에 들어 있는 chromium, nickel, 및 manganess를 原子吸光分光分析法(atomic absorption spectrophotomer)으로써 보다 빨리 定量할 수 있는 方法을 記述하였다. 現行되고 있는 濕式分析法과 比較한 結果 原子吸光分光分析法도 stainless steel의 分析에 믿을만한 한가지 分析法임을 알게 되었다.

• Journal of Preventive Medicine and Public Health
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• 제15권1호
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• pp.111-114
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• 1982

To determine Pb level in blood, we usually .used to pull out about 5ml blood from venous vessel and this sample was digested with acids to decompose organic matter and then determined the Pb contents by Atomic Absorption Spectrophotometer with flame. But recent trend in quan titating Pb in small amount of sample is very much recommended in clinical chemistry specially pediatrics, and industrial hygiene and occupational health area. Authors tried to determine Pb contents in small amount blood of $25{\mu}l$ by using capillary tube method and got the possibility of determination of ng amount of Pb in $25{\mu}l$ whole blood sample without any pretreatment of sample.

• 셀메드
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• 제6권1호
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• pp.3.1-3.4
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• 2016

Consumption of herbal products from the medicinal plants contaminated with heavy metals can cause serious consequences on human health. This is a major concern for traditional and herbal medicine. The present study was carried out to analyze and quantify the levels of six potentially toxic heavy metals namely arsenic, lead, cadmium, mercury, chromium and nickel in ten important Indian medicinal herbs. The air dried raw herbs were processed by microwave assisted wet digestion and analyzed by using atomic absorption spectrophotometer equipped with graphite tube atomizer. Except the chromium content in three plants, all the levels of six heavy metals analyzed were found to be quite below the permissible limits in all the ten raw medicinal herbs analyzed. The present work implies that, regular and systematic screening of raw medicinal herbs is necessary to check the levels of the heavy metal contaminants before using them for consumption or preparation of herbal formulations so that the possible contamination cannot cumulate up to the finished products.

• 한국식품영양과학회지
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• 제10권1호
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• pp.107-116
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• 1981

This experiment was attempted to establish the optimal condition, e.g., the effects of pH, interferences of other elements, for the determination of the inorganic elements in the paddy soils by atomic absorption spectrophotometry. Inorganic elements of 100 paddy soils which were sampled in Jeon bug provincial farm land were determined by atomic absorption spectrophotometer in that condition. The results obtained in this experiment are summarized as follows: 1) The optimal pH for determination of inorganic elements in paddy soils is about 7.0. 2) It was investigated that the absorbance of potassium was increased, and that of calcium, magnesium and zinc was decreased by adding of $Fe^{++}$ and $Cu^{++}$ in the sample. 3) It was shown that paddy soils in Jeonbug provincial farm land contain the normal amounts of inorganic elements (K, Ca, Mg, Zn,). But comparing to the results of 1976 year, it was known that the contents of inorganic elements in paddy soils considerably was changed.

• Journal of Nutrition and Health
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• 제4권3호
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• pp.1-4
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• 1971

Zinc is an essential trace element. Previos methods for the determination of zinc in serum have been difficult and reported findings must be treated with caution. The normal range of zinc in serum varies significantly according to different methods and author. The scope of this work was to establish the normal range of zinc in serum values in healthy Korean persons. Methods are described for the determination of zinc in serum diluted ten-fold with deionised water using Hitachi Model 207, atomic absorption spectrophotometer. The values of zinc in serum of 23 healthy Korean persons by atomic absorption spectroscopy ranged from 87.6 to $131.2\;{\mu}g/100\;ml$ with the mean value $109.1\;{\mu}g/100\;ml$ and standard deviation 10.86. In this method, satifactory result was obtained with regard to the coefficient variation and recoveries of added zinc in the measurenents.

• 한국대기환경학회지
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• 제6권2호
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• pp.147-154
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• 1990

A sensitive method for the determination of total selenium in aerosol particles is described. The method involves dissolution of aerosol particles by $HNO_3-HClO_4$ mixed acids, pre-reduction of Se (VI) to Se (IV) by boiling hydrochloric acid, and hydride generation followed by atomic absorption detection. Dissolved Se (IV) in 4M hydrochloric acid is reacted with $NaBH_4$ to form $H_2Se$, which is subsequently collected in an U-tube cooled in liquid nitrogen. Upon the completion of $H_2Se$ generation, the collected $H_2Se$ is rapidly vaporized into a quartz cuvette burner by removing the U-tube from liquid nitrogen, atomized, and then detected by an atomic absorption spectrophotometer. The absolute sensitivity of the method is 0.49 ng/0.0044 Abs. The accuracy of the method evaluated by analyzing standard reference materials for urban aerosol is better than 10%. Analytical results for urban and rural aerosol particles are reported.

• 분석과학
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• 제5권2호
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• pp.185-190
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• 1992

글로우방전장치를 기존의 원자흡수분광기의 버너 대신에 장착하였다. 정확도를 측정하기 위하여 철강표준물질을 이용하여 측정된 값과 농도를 비교하였다. 검정곡선을 작성하였으며 작성된 검정곡선으로 원자흡광감고를 측정하였다. 감도에 영향을 미치는 인자들 및 개선된 장치의 개발에 필요한 분야에 관하여 연구하였다.

• 한국식품영양과학회지
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• 제22권5호
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• pp.592-595
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• 1993

인삼의 재배년근별, 국내산지별 및 국가별 무기물의 분포를 조사하기 위하여 시험한 결과 Mn은 2년근에 비하여 5년근에서 4배 가까운 증가추세를 나타내었다. 재배산지별로 볼때 P은 각 지역별로 큰 차이를 나타내지 않았다. 한편 각국 인삼별로는 중국 천칠삼에서 N의 함량이 적제 나타났으며 P은 한국산 정상홍삼에서 가장 높게 나타났다.

• 한국식품위생안전성학회지
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• 제2권4호
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• pp.209-214
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• 1987

A survey to determine the zinc content of early-infant food sources was conducted. Collected samples from various lots were human milk from volunteer mothers and infant formula and market milk from markets. The determined results by Atomic absorption Spectrophotometer were as follows: 1. Averages of Zn were 201$\pm$144 $\mu\textrm{g}$/dl in human milk, 2.243$\pm$0.888 mg/100g in infant formula, 292$\pm$90$\mu\textrm{g}$/dl in market milk and showed the decline trend by the lactation periods in human milk. (p<0.01) 2. Estimated daily intake of Zn from human milk was higher than that from infant formula in 3 months old infants.

• Journal of Preventive Medicine and Public Health
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• 제7권2호
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• pp.377-381
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• 1974

Determination of lead in urine is important in industrial hygiene and toxicology. Dithizone method has been principally used for the determination of lead in urine, which gives accurate results in skilful hands but is usually complex and time-consuming. Atomic absorption spectrophotometry is a new simple method and several procedures have been described. However, the influences of pH and the presence of chelating agents during treatment of lead poisoning are not clear. The purpose of this study was to find out the effect of pH and chelating agents on the determination of lead using Shimadzu atomic absorption/flame spectrophotometer, model AA-610. The results obtained were as follows: 1. The atomic absorption spectrophotometry(AAS) could be applied without prior acid digestion to specimens in the absence of chelating agents. The absorbance at $2,170\;{\AA}$, though more sensitive, was more noisy electronically. Therefore, we selected the wavelength of $2,833\;{\AA}$ plus scale expansion. 2. The optimal pH was in the range from 2 to 3. 3. The sensitivity was $0.075{\mu}g/ml/%$ and detection limit was about $0.2{\mu}g/ml$. 4. In the presence of EDTA, lead could not be completely determined without prior acid digestion. 5. On specimens from patients receiving penicillamine therapy, a comparison was made between the values obtained with dithizone method and AAS method with prior acid digestion. The results of comparison showed a very good agreement.