• The Journal of Korean Academy of Prosthodontics
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• v.45 no.6
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• pp.769-779
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• 2007

Statement of problem. When TiN coating is applied to the abutment screw, occurrence of greater preload and prevention of the screw loosening could be expected due to decrease of frictional resistance. However, the proper thickness of TiN coating on abutment screw has not been yet reported. Purpose. The purpose of this study is to find out the appropriate TiN coating thickness by evaluating the detorque force and the surface change of titanium abutment screw with various TiN coating thickness. Material and methods. 1. Material Thirty five non-coated abutment screws were prepared for TiN coating. TiN coatings were prepared by Arc ion plating method. Depending on the coating deposition time(CDT), experimental groups were divided into 6 groups(CDT 30min, 60min, 90min, 120min, 150min, 180min) and those of 1 group was not coated as a control group. Each group was made up of 5 abutment screws. 2. Methods FE-SEM(Field Emission Scanning Electron Microscoper) and EDX(Energy Dispersive X-ray Spectroscopy) were used to observe the surface of the abutment screw. Electric scales was used to measure the weight of the abutment screw after the repeated closing and opening of 10 trials. Detorque force was measured with digital torque gauge, at each trial. Results. 1. As the coating deposition time increased, the surface became more consistent and smooth. 2. As for the abutment screws that were TiN coated for more than 60 minutes, no surface change was found after the repeated closing and opening. 3. The TiN coated abutment screws showed less weight change than the non-coated abutment screws. 4. The TiN coated abutment screws showed higher mean detorque force than the noncoated abutment screws. 5. The abutment screw coated for 60 minutes showed the highest mean detorque force. Conclusion. The coating layer of proper thickness is demanded to obtain consistent and smooth coating surface, resistance to wear, and increased detorque force of the abutment screw. In conclusion, the coating deposition time of 60 minutes indicated improved mechanical property, when TiN coating was conducted on titanium abutment screw.

• Journal of Electrochemical Science and Technology
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• v.14 no.4
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• pp.311-319
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• 2023

This work was performed to characterize the electrochemical behavior of AZ31 Mg alloy in neutral aqueous solutions where Cl^-, SO₄^2-, PO₄^3-, and F^- ions were present and pH was adjusted to 6 to exclude the contribution of H⁺ and OH^- ions. Open-circuit potential (OCP) transient, electrochemical impedance spectroscopy (EIS) and potnetiodynamic polarization curves were employed. The OCP value appeared to decrease in the order of F^- > Cl^- > SO₄^2- > PO₄^3- ions while corrosion current density increased in the same order. Electrochemical impedance spectroscopy (EIS) data showed two capacitive arcs in all the solutions and one more inductive arc appeared in PO₄^3--containing solution. By fitting of two capacitive arcs, capacitance of dense film (C_df), resistance of porous film (R_pf) and double layer capacitance (C_dl) and charge transfer resistance (R_ct) beneath the porous films were obtained. A simplified model in which various thicknesses and coverages of dense and porous films are assumed to be present on the AZ31 Mg alloy surface, is suggested to explain the effects of four different anions on the electrochemical behavior of AZ31 Mg alloy.

• Journal of Conservation Science
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• v.25 no.4
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• pp.373-381
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• 2009

To preserve steel cultural properties on display outdoors, the surface of these relics is processed with a covering treatment, which is a typical anti-corrosion method. Since the registered cultural heritage of Korea No. 78 Locomotive at Jangdan Station of Gyeongui Line will be treated by preservation process and displayed in the open outdoor area, effective surface covering agents were selected through testing to prevent the corrosion of the locomotive. The mixed wax are based on two types of microcrystalline wax which is one of regular surface covering agents for locomotives and bee‘s wax. For the weather resistance test, 3 types of wax were applied to each specimen of the locomotive and the specimens were tested in the Xenon-Arc Accelerated Weathering Tester for 1000 hours in accordance with the ISO 4892-1981 criteria and the test results were compared. As a result, on the surface of the specimen coated with the bee's wax, a whitening event appears after 400 hours which causes aging, and the specimens coated by the microcrystalline wax showed signs of a whitening event after 800 hours. The moisture contact angle with the microcrystalline wax coating was also less than with the bee's wax. Therefore, it was found that the high temperature microcrystalline wax is the most effective coating agent in terms of weather resistance and moisture blocking capability and the high temperature microcrystalline wax was adopted for coating the surface of the locomotive.

• Corrosion Science and Technology
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• v.8 no.2
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• pp.89-92
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• 2009

Pure Ti as well as Ti-6Al-4V alloy exhibit excellent properties for dental implant applications. However, for a better biocompatibility it seems important to avoid in the composition the presence of V due to the toxic effects of V ion release. Thus Al and V free and composed of non-toxic element such as Nb, Zr alloys as biomaterials have been developed. Especially, Zr contains to same family in periodic table as Ti. The addition of Zr to Ti alloy has an excellent mechanical properties, good corrosion resistance, and biocompatibility. In this study, the electrochemical characteristics of Ti-Zr alloys for biomaterials have been investigated using by electrochemical methods. Methods: Ti-Zr(10, 20, 30 and 40 wt%) alloys were prepared by arc melting and homogenized for 24 hr at $1000^{\circ}C$ in argon atmosphere. Phase constitutions and microstructure of the specimens were characterized by XRD, OM and SEM. The corrosion properties of the specimens were examined through potentiodynamic test (potential range of -1500 ~ 2000 mV), potentiostatic test (const. potential of 300 mV) in artificial saliva solution by potentiostat (EG&G Co, PARSTAT 2273. USA).

• Proceedings of the KIEE Conference
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• 2004.07c
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• pp.1637-1639
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• 2004

In order to analyze the physical and chemical characteristics of the home production porcelain insulators by change of the alumina addition amount, 36000lbs ball socket type suspension insulators which were manufactured in 1989, 1995 and 2001 removed in transmission line and an experiment was performed. By the result, 8 [wt.%] alumina that influences the mechanical properties and arc resistance properties in case of insulators that were manufactured in 1989 was contained, and the relative density and the fracture toughness of insulators appeared by 94.2% and 1.4 [MPa $M^{1/2}$], respectively. However, 12 [wt.%] alumina was contained in case of insulators that were manufactured in 1995, and the relative density and the fracture toughness of insulators appeared preferably lower by 92% and 1.3 [MPa $M^{1/2}$], respectively. Amount of alumina was contained most by 17 [wt.%] in case of insulators that were manufactured in 2001. It was confirmed that the electrical and mechanical characteristics such as the relative density and the fracture toughness appeared excellently by 96% and 1.7 [MPa $m^{1/2}$], respectively.

• Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
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• 2004.05a
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• pp.352-355
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• 2004

Inconel 625 is useful in variety of industrial applications because of the resistance to attack in various corrosive media at temperatures from $200^{\circ}C$ to over $1090^{\circ}C$, in combination with good law- and high temperature mechanical strength. Rencently, this material is also used widely in offshore processing piping in order to extend the maintenance tenn and improve the quality of anti-corrosion. In general, high quality weldments for this material are readily produced by commonly used processes. Not all processes are applicable to this material group, Ni-alloys. Metallurgiad characterictics or the unavailability of matching, position or suitable welding processes. Nowadays, the flux cored wire is developed and applied for the better productivity in several welding position including the vertical position. in this study, the weldability and weldment characteristics of inconel 625 are considered in FCAW weld associated with the several shielding gases($80\%Ar\;+\;20\%\;CO_2,\;50\%Ar\;+\;50\%\;CO_2,\;100\%\;CO_2$) in viewpoint of welding productivity.

• Corrosion Science and Technology
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• v.12 no.1
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• pp.50-55
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• 2013

The purpose of this study was to investigate corrosion characteristics of Ti-xTa alloys with Ta contents. Ti-xTa alloys used as samples (x=30, 40%) were arc-melted under argon atmosphere of 99.9% purity. Ti-xTa alloys were homogenized for 12hr at $1000^{\circ}C$ and then water quenched. The surface characteristics of Ti-xTa alloys were investigated using optical microscopy (OM) and X-ray diffractometer (XRD). The anodic corrosion behaviors of the specimens were examined through potentiodynamic, potentiostatic and galvanostatic test in 0.9 % NaCl solution at $36.5{\pm}1^{\circ}C$. After corrosion test, the surface characteristics of Ti-xTa alloys were investigated using OM. The microstructure of Ti-Ta alloy showed the beta structure with Ta content. The corrosion resistance of Ti alloy was improved by increasing Ta content and the corrosion morphology of Ti-Ta alloy showed that the site attacked by chloride ion decreased from the active to passive region with Ta content. Potential of Ti-40Ta alloy increased as time increased, whereas, current density of Ti-40Ta alloy decreased as time increased compared to Ti-30 alloy.

• Proceedings of the Korean Vacuum Society Conference
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• 2016.02a
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• pp.200.2-200.2
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• 2016

Carbon-based materials have been known as ablative material and have been used for thermal protection systems. Ablation is an erosive phenomenon that results in thermochemical and thermomechanical changes on materials. Ablation resistance is one of the key properties that determines performance and life-time of the thermal protection material under ablative conditions. In this study, ablation properties of graphite, 3-dimensional (C/C) composites (needle-punched type and rod type) were investigated byusing a plasma wind tunnel which produce a supersonic plasma flow from a segmented arc heater with the power level of 0.4 MW. The mass losses and surface roughness changes which contain main result of the ablation are measured. A morphological analysis ofthe carbon-based materials, before and after the ablation test, are performed through field emission scanning electron microscopy (FE-SEM) and non-contact 3D surface measuring system. Electronic balance and a portable surface roughness tester were used for evaluation of the recession and mass loss of the test samples.

• Progress in Superconductivity and Cryogenics
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• v.19 no.4
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• pp.40-44
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• 2017

This paper analyzed the fault current limiting characteristics of the previously proposed transformer superconducting fault current limiter (TSFCL) interruption system according to its transformer type. The TSFCL interruption system is an interruption technology that combines a TSFCL, which uses a transformer and a superconductor, and a mechanical DC circuit breaker. This technology first limits the fault current using the inductance of the transformer winding and the quench characteristics of the superconductor. The limited fault current is then interrupted by a mechanical DC circuit breaker. The magnitude of the limited fault current can be controlled by the quench resistance of the superconductor in the TSFCL and the turns ratio of the transformer. When the fault current is controlled using a superconductor, additional costs are incurred due to the cooling vessel and the length of the superconductor. When the fault current is controlled using step-up and step-down transformers, however, it is possible to control the fault current more economically than using the superconductor. The TSFCL interruption system was designed using PSCAD/EMTDC-based analysis software, and the fault current limiting characteristics according to the type of the transformer were analyzed. The turns ratios of the step-up and step-down transformers were set to 1:2 and 2:1. The results were compared with those of a transformer with a 1:1 turns ratio.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.15 no.1
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• pp.110-115
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• 2016

The need for high-strength galvanized steel has recently increased because of the increased number of car consumers who want improved efficiency and exterior quality. High-strength galvanized steel with high corrosion resistance improves the durability of products and exterior quality. Furthermore, the gilt of zinc does not come off during machining because of the fine adhesive property of zinc. When these are welded, zinc has a lower melting temperature than iron, so zinc is more quickly vaporized than iron. Vaporized zinc can stick to electrodes, which increases spatter in welding transportation. Created spatter can enter the molten pool and develop into inner defects or blowholes and pits. Scattered spatter sticks to the product, which leads to the secondary cost of spatter removal. Therefore, in this study, comparisons of amounts of spatter generated are conducted according to the composition of shielding gas in the MIG and CMT processes to find optimal welding parameters.