• Journal of Korean Society of Disaster and Security
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• v.15 no.3
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• pp.67-77
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• 2022

In South Korea, U-type girder development was attempted as a means to increase the length of I-type girder, but due to the large self-weight according to the post-tension method, the application of rail bridges of 30m or less is typical. There are not many examples of application of pre-tension type girder. This study does not limit the post-tension method, but applies the pre-tension method to induce a reduction in self-weight and materials used due to the reduction of the cross-section. In addition, we intend to apply the on-site pre-tensioning method using the internal reaction arm of the U-type girder. The prestressed concrete U-type girder bridge is composed of a concrete deck slab and a composite section. Compared to the PSC I-type, which is an open cross-section because the cross section is closed, structural performance such as resistance and rigidity is improved, the safety of construction is increased during the manufacturing and erection stage, and the height ratio is reduced due to the reduction of its own weight. Therefore, it is possible to secure the aesthetic scenery and economical of the bridge. As a result, it is expected that efficient construction will be possible with high-quality factory-manufactured members and cast-in-place members. In this paper, the introduction of the pre-tension method on-site and the analytical performance verification of the anchoring block for tension are included.

• Korean Journal of Remote Sensing
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• v.28 no.4
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• pp.421-434
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• 2012

Colored Dissolved Organic Matter (CDOM) is one of the important components of optical properties of seawater to determine ecosystem dynamics in a given marine area. The optical characteristics of CDOM may depend on the various ecosystem and environmental variables in the sea and those variables may vary region to region. Therefore, the retrieval algorithm for determining light absorption coefficient of CDOM ($a_{CDOM}$) using satellite remote sensing reflectance ($R_{rs}$) developed from other region may not be directly applicable to the other region, and it must be validated using an in-situ ground-truth observation. We have tested 6 known CDOM algorithms (three Semi-analytical and three Empirical CDOM algorithms) developed from other regions of the world ocean with laboratory determined in-situ values for the East Sea using field data collected during seven oceanographic cruises in the period of 2009~2011. Our field measurements extended from the coastal waters to the open oceanic type CASE-1 Waters. Our study showed that Quasi-Analytical Algorithm (QAA_v5) derived $a_{CDOM}$(412) appears to match in-situ $a_{CDOM}$(412) values statistically. Semi-analytical algorithms appeared to underestimate and empirical ones overestimated $a_{CDOM}$ in the East Sea. $a_{CDOM}$(412) value was found to be relatively high in the relatively high satellite derived-chlorophyll-a area. $a_{CDOM}$(412) value appears to be influenced by the amount of chlorophyll-a in seawater. The outcome of this work may be referenced to develop $a_{CDOM}$ algorithm for the new Korean Geostationary Ocean Color Imager (GOCI).

• Korean Journal of Environmental Agriculture
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• v.34 no.2
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• pp.111-119
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• 2015

BACKGROUND: Ethychlozate (ECZ) is a plant growth regulator of synthetic auxin for agricultural commodities (ACs). Accurate and sensitive method to determine ECZ in diverse ACs on global official purpose is required to legal residue regulation. As the current official method is confined to the limited type of crops with poor validation, this study was conducted to improve and extend the ECZ method using high-performance liquid chromatography (HPLC) in all the registered crops with method verification. METHODS AND RESULTS: ECZ and its acidic metabolite (ECZA) were both extracted from acidified samples with acetone and briefly purified by dichloromethane partition. ECZ was hydrolyzed to form ECZA and the combined ECZA was finally purified by ion-associated partition including hexane-washing. The instrumental quantitation was performed using HPLC/ FLD under ion-suppression of ECZA with no interference by sample co-extractives. The average recoveries of intra- and inter-day experiment ranged from 82.0 to 105.2% and 81.7 to 102.8%, respectively. The repeatability and reproducibility for intra- and inter-day measurements expressed as a relative standard deviation was less than 8.7% and 7.4%, respectively. CONCLUSION: Established analytical method for ECZ residue in ACs was applicable to the nation-wide pesticide residues monitoring program with the acceptable level of sensitivity, repeatability and reproducibility.

• Korean Journal of Veterinary Service
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• v.40 no.4
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• pp.253-258
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• 2017

The aim of this study is to develop an optimal analytical method for gonadorelin, progesterone, oxytocin and estradiol, the major components of hormones. A relatively simple and reproducible method using high performance liquid chromatography was developed and as a result of the measurement of specificity, linearity, repeatability, accuracy and intermediated precision, the validity of the developed method was verified with the result of meeting the verification criteria of analytical method validation. Using this newly developed method, 12 post-market veterinary products were tested and the ingredient content were 91.9~116.4%, which satisfied the 90~120% condition of the administrative measure standard. Therefore, if the newly developed method is used for the collection examination of hormone in veterinary medicine, it can be useful as an approved test method.

• Analytical Science and Technology
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• v.8 no.4
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• pp.759-770
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• 1995

By extensive studies with the quantitative status of the mineral constituents of thousands of water samples, it was found that almost in all natural waters irrespective of the surface or sub-surface sources, minimum 99.5% of the total amount of the cationic constituents are generally the contributions of 3 commonly present parameters viz. Ca, Mg and Na and that of the anionic species are same and contributed by $HCO_3$, Cl and $SO_4$ only. In the field of water works, all these major mineral substances are conventionally measured as their individual ions. But till now, no reliable and generalised methods or rules have been developed for the determination of the exact kinds of the individual salt components and their amounts from these ionic constituents normally present in water. As salt content, only the TDS (Total Dissolved Solids) parameter is frequently measured by evaporation of the water sample. But TDS can tell nothing about the kinds and amounts of the individual salts present in it. Considering the analytical importance of the estimation of the mineral substances as their individual salts, some generalised mathematical models have been developed by this research which are based on the 'hypothetical order of chemical combinations' as may occur among the ionic constituents. With the help of these models, one can easily assume the most probable salts with approximate quantities derived from the ionic constituents. In addition, approximate amount of Na content can also be estimated mathematically with simultaneous verification of the correctness of the water analysis results. The models are stated in this paper with practical illustrations and descriptions of the method of applications.

• Journal of the Korea institute for structural maintenance and inspection
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• v.18 no.2
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• pp.74-81
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• 2014

In this study, it was conducted to improve the performance of stud of Steel Plate Concrete(SC) walls subjected to bending moment. Non-linearity of contact interface, connection, and material properties were considered in finite element modeling of SC wall. In order to validate the analytical model, furthermore, a foregoing laboratory experiment was simulated by FEM, so that comparison between the measured result and the analysis result have be done. The size of the analytical model was determined by reflecting various references and the analyses were performed according to various shapes and arrangements of stud. Additionally, the validity of the model considering the related provisions in the KEPIC SNG standard was also considered. As a result, the optimal shape and spacing of studs was proposed through this numerical analysis and standard verification.

• Korean Journal of Fisheries and Aquatic Sciences
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• v.55 no.2
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• pp.218-223
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• 2022

Cholesterol is an essential component for maintaining health; however, excessive consumption can lead to diseases. Thus, continuous monitoring of cholesterol content is important in food research. The cholesterol analysis method used in Korea follows the Korean Food Standards Codex. As this method uses gas chromatography, derivatization of the sample is required, and analysis time is more than 30 min. Kim developed a new method using liquid chromatography; however saponification by the non-heat saponification method is insufficient. To address these limitations, a new cholesterol analysis method was developed and verified. The correlation coefficients for the cholesterol standard (STD) were maintained above 0.99. The limit of detection and limit of quantitation of cholesterol STD were 2.41 ㎍/mL and 7.31 ㎍/mL, respectively. The accuracies for cholesterol were 92.21-99.02%. The developed analytical method was also verified using three standard reference materials, and their accuracies were 93.71-97.09%. In addition, the cholesterol content of fishes was analyzed, and the values were compared with those recorded by the United States Department of Agriculture. Our results suggest that this method could be used as a new analytical method for cholesterol in seafood.

• Proceedings of the Korean Society of Near Infrared Spectroscopy Conference
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• 2001.06a
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• pp.1516-1516
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• 2001

During the recent years, wine analysis has played an increasing role due the health benefits of phenolic ingredients in red wine [1]. On the other hand there is the need to be able to distinguish between different wine varieties. Consumers want to know if a wine is an adulterated one or if it is based on the pure grape. Producers need to certificate their wines in order to ensure compliance with legal regulations. Up to now, the attempts to investigate the origin of wines were based on high-performance liquid chromatography (HPLC), gas chromatography (GC) and pyrolysis mass spectrometry (PMS) [l,2,3]. These methods need sample pretreatment, long analysis times and therefore lack of high sample throughput. In contradiction to these techniques using near infrared spectroscopy (NIRS), no sample pretreatment is necessary and the analysis time for one sample is only about 10 seconds. Hence, a near infrared spectroscopic method is presented that allows a fast classification of wine varieties in bottled red wines. For this, the spectra of 50 bottles of Cabernet Sauvignon, Lagrein and Sangiovese (Chianti) were recorded without any sample pretreatment over a wavelength range from 1000 to 2500 nm with a resolution of 12 cm$\^$-1/. 10 scans were used for an average spectrum. In order to yield best reproducibility, wines were thermostated at 23$^{\circ}C$ and a optical layer thickness of 3 mm was used. All recorded spectra were partitioned into a calibration and validation set (70% and 30%). Finally, a 3d scatter plot of the different investigated varieties allowed to distinguish between Cabernet Sauvignon, Lagrein and Sangiovese (Chianti). Considering the short analysis times this NRS-method will be an interesting tool for the quality control of wine verification and also for experienced sommeliers.

• Korean journal of applied entomology
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• v.61 no.4
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• pp.659-664
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• 2022

Putrescine generated by the action of microorganisms in the decay generally used as a measure of freshment in food. However, the analytical method of putrescine in freeze-dried royal jelly has not yet been established. In the present study, the UPLC method for putrescine in lyophilized royal jelly was established using C18 column. The newly established method was able to analyze putrescine accurately within 7 minutes and was validated by analytical parameters such as specificity, linearity, precision, accuracy, limit of detection, and limit of quantification. These results provide for the analytical method to evaluate the level of freshment in freeze-dried royal jelly, which will useful in further studies of safety verification.

• Advances in concrete construction
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• v.17 no.4
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• pp.233-243
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• 2024

The behavior of confined steel fiber-reinforced concrete (including confinement models) with compressive strengths ranging from normal to high strength is still rarely studied. This paper presents the results of an investigation of fifteen confined concrete cylinders containing steel fiber. The design parameters evaluated in the experiment included concrete compressive strength (covers normal to high strength), volume fraction of steel fiber and hoop spacing. The main objective of this study was to evaluate the behavior of confined steel fiber concrete by reviewing several design parameters, such as concrete strength (normal to high strength). It is then developed to be an analytical stress-strain expression for confined steel fiber concrete. The experimental program was carried out by making cylindrical specimens with a diameter of 100 mm and a height of 200 mm. The cylindrical test object is compressed in a monotonic uniaxial loading. Experimental results have shown steel fiber in concrete has an important role in increasing the compressive strength and strain of cylindrical concrete without steel fiber. In addition, the value of strength enhancement of confined concrete (K) along with increasing fiber fraction volume; which applies to normal to high-strength concrete. The value of K also increases if the compressive strength of the concrete tends to decrease and the spacing of the hoops is closer. The comparison of stress-strain behavior between the confined steel fiber concrete proposed by other researchers and the experimental results in general significantly different in post-peak response. The statistical analysis indicates that the value of Coefficient of Variation for the confinement model by Campione is the closest compared to other existing confinement models in predicting the values of K and Toughness Index. Furthermore, the analytic stress-strain expression of confined steel fiber concrete was developed by adopting and modifying several equations from the present models. The proposed analytical expression is then verified with the experimental results. The results of the verification show that the stress-strain behavior of confined steel fiber concrete is relatively close.