• Title/Summary/Keyword: analytical methods

Search Result 3,048, Processing Time 0.029 seconds

Studies on the Analytical Methods and Quantity of Residual Chlorfluazuron in Meat (식육중 Chlorfluazuron의 잔류분석법 및 잔류량에 관한 연구)

  • 박건상;홍무기;백선영;정병곤;박종세
    • Journal of Food Hygiene and Safety
    • /
    • v.12 no.4
    • /
    • pp.288-293
    • /
    • 1997
  • Analytical method using capillary GC/ECD was developed to determine trace residues of chlofluazuron, 1-[3, 5-dichloro-5-trifluoromethyl-2-pyridyloxy)phenyl]-3-(2, 6-difiuorobenzoyl), in meat, and applied to analyze the residues in domestic and imported meats. The analytical scheme developed does not require column chromatographic cleanup; chlorfiuazuron was extracted with diethyl ether and petroleum ether (50: 50), partitioned against acetonitrile, cleaned up with silica Sep-Pak cartridge, identified GC/ECD, and comfirmed by GC/MS. The mean recoveries of the pesticide in meat fortified with standard solution 0.1, 0.5, 0.1 mg/kg were ranged from 82 to 95%. The limit of detection and limit of quantitation were 0.001 and 0.005 mg/kg, respectively. Chlorfluazuron residues were not found in domestic samples, but found in imported Australian beef ranging from 0.02 to 0.17 mg/kg, detected by 18% among the samples.

  • PDF

An Analytical Study of the Flexural Deformation for High Strength Concrete Structures using Reliability Theory (신뢰성 이론을 이용한 500kgf/$\textrm{cm}^2$의 고강도콘크리트 구조물에 대한 휨변형의 해석적 연구)

  • 송재호;최광진;김민웅;홍원기
    • Proceedings of the Korea Concrete Institute Conference
    • /
    • 1995.04a
    • /
    • pp.231-236
    • /
    • 1995
  • The object of this thesis is an analytical study on flexural deformation of high strength concrete structures using reliability theory. Using the established experimental data that have been presented in various documents the stress-strain relationship curves of high strength(500kgf/$\textrm{cm}^2$)models are proposed. Based on both methods of logarithm regression analysis and multiple regression analysis adopted in order to establish the relationships between design parameters, response random variables and flexural deformation analyzed using Monte Carlo simulation and Simpson composite formula. Additional random variables are introduced to incorporate both the confidence in the analytical accuracy of engineering mechanics associated with structural response quantities and the uncertainty in the construction quality control. The result is expected to accomodate other important design parameter of high strength concrete design in treating reliability theory that practicing engineers, structural engineering often face.

  • PDF

Quasi-3D analysis of Axial Flux Permanent Magnet Rotating Machines using Space Harmonic Methods (공간고조파법을 이용한 축 자속 영구자석 회전기기의 준(準)-3D 특성 해석)

  • Choi, Jang-Young
    • The Transactions of The Korean Institute of Electrical Engineers
    • /
    • v.60 no.5
    • /
    • pp.942-948
    • /
    • 2011
  • This paper deals with characteristic analysis of axial flux permanent magnet (AFPM) machines with axially magnetized PM rotor using quasi-3-D analysis modeling. On the basis of magnetic vector potential and a two-dimensional (2-D) polar-coordinate system, the magnetic field solutions due to various PM rotors are obtained. In particular, 3-D problem, that is, the reduction of magnetic fields near outer and inner radius of the PM is solved by introducing a special function for radial position. And then, the analytical solutions for back-emf and torque are also derived from magnetic field solutions. The predictions are shown in good agreement with those obtained from 3-D finite element analyses (FEA). Finally, it can be judged that analytical solutions for electromagnetic quantities presented in this paper are very useful for the AFPM machines in terms of following items : initial design, sensitivity analysis with design parameters, and estimation of control parameters.

Analytical Inverse Kinematics Algorithm for a 7 DOF Anthropomorphic Robot Arm Using Intuitive Elbow Direction (7자유도 인간형 로봇 팔의 직관적인 팔꿈치 위치 설정이 가능한 역기구학 알고리즘)

  • Kim, Young-Loul;Song, Jae-Bok
    • The Journal of Korea Robotics Society
    • /
    • v.6 no.1
    • /
    • pp.27-33
    • /
    • 2011
  • Control and trajectory generation of a 7 DOF anthropomorphic robot arm suffer from computational complexity and singularity problem because of numerical inverse kinematics. To deal with such problems, analytical methods for a redundant robot arm have been researched to enhance the performance of inverse kinematics. In this research, we propose an analytical inverse kinematics algorithm for a 7 DOF anthropomorphic robot arm. Using this algorithm, it is possible to generate a trajectory passing through the singular points and intuitively move the elbow without regard to the end-effector pose. Performance of the proposed algorithm was verified by various simulations. It is shown that the trajectory planning using this algorithm provides correct results near the singular points and can utilize redundancy intuitively.

Determination of Rare Earth Elements Abundance in Alkaline Rocks by Inductively Coupled Plasma Mass Spectrometry (ICP-MS) (ICP-MS를 이용한 알칼리암의 희토류원소 정량분석)

  • Hur, Soon-Do;Lee, Jong-Ik;Lee, Mi-Jung;Kim, Yea-Dong
    • Ocean and Polar Research
    • /
    • v.25 no.1
    • /
    • pp.53-62
    • /
    • 2003
  • Inductively coupled plasma mass spectrometry (ICP-MS) is useful instrument for determining abundance of rare earth elements, due to very low detection limits and rapid data acquisition. In this article, two methods are used for decomposition of alkaline rocks; close vessel acid digestion and $Na_2Co_3$ fusion. The two analytical results show good agreements. Considering total dissolved solids and detection limits, the most adequate dilution factor is 5,000 times. Polyatomic ion interferences during analysis can give rise to Inaccuracies. After correction from oxide and hydroxide interference, the analytical result show 20-30% decrease for Gd and Tm, 10-20% decrease for Tb and Er. In comparing the analytical results from KORDI with other institutes, most rare earth elements abundance show good agreements except Lu.

Calculating Inductance of Switched Reluctance Motors with overlapping soles of rotor and stator (SRM 고정자와 회전자 중첩에 따른 인덕턴스 계산)

  • Choi, Kyeong-Ho;Back, Won-Sik;Kim, Dong-Hee;Kim, Min-Huei
    • Proceedings of the KIEE Conference
    • /
    • 2001.07b
    • /
    • pp.933-935
    • /
    • 2001
  • This paper presents a calculating method for inductance of the Switched Reluctance Motor(SRM) for torque characteristics and driving by analytical model. The approaches for calculating inductance have taken vary from detailed finite element analysis(FEA) and Fitting method in magnetization curves using complex nonlinear magnetic circuit models. But those methods have not satisfactory approach for machine performance calculations, because of having a long time and remodeling for analyses, therefore thus an alternative approach is required. So it is suggested simply calculating method of the inductance based on designed data of machinery by analytical model in unaligned and aligned rotor. In order to prove the calculating, there are compare with analytical FEM, direct measurement, this method, and simulation. The compared result is shown to obtain good accuracy.

  • PDF

Nonlinear vibration of conservative oscillator's using analytical approaches

  • Bayat, Mahmoud;Pakar, Iman;Bayat, Mahdi
    • Structural Engineering and Mechanics
    • /
    • v.59 no.4
    • /
    • pp.671-682
    • /
    • 2016
  • In this paper, a new analytical approach has been presented for solving nonlinear conservative oscillators. Variational approach leads us to high accurate solution with only one iteration. Two different high nonlinear examples are also presented to show the application and accuracy of the presented approach. The results are compared with numerical solution using runge-kutta algorithm in different figures and tables. It has been shown that the variatioanl approach doesn't need any small perturbation and is accurate for nonlinear conservative equations.

Analysis of Orthotropic Spherical Shells under Symmetric Load Using Runge-Kutta Method (Runge-Kutta법을 이용한 축대칭 하중을 받는 직교 이방성 구형쉘의 해석)

  • Kim, Woo-Sik;Kwun, Ik-No;Kwun, Taek-Jin
    • Journal of Korean Association for Spatial Structures
    • /
    • v.2 no.3 s.5
    • /
    • pp.115-122
    • /
    • 2002
  • It is often hard to obtain analytical solutions of boundary value problems of shells. Introducing some approximations into the governing equations may allow us to get analytical solutions of boundary value problems. Instead of an analytical procedure, we can apply a numerical method to the governing equations. Since the governing equations of shells of revolution under symmetric load are expressed by ordinary differential equations, a numerical solution of ordinary differential equations is applicable to solve the equations. In this paper, the governing equations of orthotropic spherical shells under symmetric load are derived from the classical theory based on differential geometry, and the analysis is numerically carried out by computer program of Runge-Kutta methods. The numerical results are compared to the solutions of a commercial analysis program, SAP2000, and show good agreement.

  • PDF

Evaluation for Operational Efficiency of Road Management Equipment using Analytical Hierarchy Process (계층분석법을 이용한 도로관리장비 운영의 효율성 평가)

  • Yang, Choong-Heon;Kim, In-Su
    • International Journal of Highway Engineering
    • /
    • v.14 no.5
    • /
    • pp.157-164
    • /
    • 2012
  • PURPOSES: Regional offices of the Ministry of Land, Transport and Maritime Affairs use a computerized system called KAMIS so as to manage road equipment systematically. Road agencies can record number of operating days by equipment, actual working hours, accumulated operating hours (or distance) by equipment, and operating cost. However, KAMIS does not provide critical information, although it is strongly related to efficient road management equipment operation. In other words, road agencies do not know whether they have sufficient equipment to handle their actual work. METHODS: Therefore, this study suggests a methodology to evaluate for operational efficiency of road management equipment using analytical hierarchy process(AHP). First of all, estimated weights related criteria can be produced by AHP, and then use operational history by pieces of equipment. RESULTS: Results show that importance of management work can differ from weather conditions through five areas. CONCLUSIONS: Commonly, this results can imply to help save money for the purchase and maintenance of road management equipment, and they would improve the functional performance of KAMIS.

A probabilistic analytical seismic vulnerability assessment framework for substandard structures in developing countries

  • Kyriakides, Nicholas;Ahmad, Sohaib;Pilakoutas, Kypros;Neocleous, Kyriacos;Chrysostomou, Christis
    • Earthquakes and Structures
    • /
    • v.6 no.6
    • /
    • pp.665-687
    • /
    • 2014
  • This paper presents a framework for analytical seismic vulnerability assessment of substandard reinforced concrete (RC) structures in developing countries. Amodified capacity-demand diagram method is used to predict the response of RC structures with degrading behaviour. A damage index based on period change is used to quantify the evolution of damage. To demonstrate the framework, a class of substandard RC buildings is examined. Abrupt accumulation of damage is observed due to the brittle failure modes and this is reflected in the developed vulnerability curves, which differ substantially from the curves of ductile structures.