• 제목/요약/키워드: acidic condition

검색결과 463건 처리시간 0.023초

홍미삼 알콜 추출박을 이용한 산성다당체 다량 함유 홍삼 엑기스 제조 (Preparation of Red Ginseng Extract Rich in Acidic Polysaccharide from Red Tail Ginseng Marc Produced After Extraction with 70% Ethyl Alcohol)

  • 도재호;이종원
    • Journal of Ginseng Research
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    • 제20권1호
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    • pp.60-64
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    • 1996
  • In this study, we investigated the appropriate conditions to extract acidic polysaccharide and to prepare red ginseng extract being rich in acidic polysaccharide from red tail ginseng marc produced after manufacturing alcoholic extract from red tail ginseng. Amount of acidic polysaccharide in red tail ginseng marc was about 11%. The best condition for the extraction of acidic polysaccharide from the marc was using of 3~5 mg of $\alpha$-amylase/g residue/15 ml of distilled water, and the amount of acidic polysaccharide in water extract of the residue treated with $\alpha$-amylase was about 27%. So, it is possible to manufacture red ginseng extract being rich in acidic polysaccharide using water extract of red tail ginseng alcoholic residue as extraction solvent. From the above results, we suggest that red tail ginseng residue produced by manufacturing alcoholic extract of red tail ginseng has high potencies in the utilization of waste material.

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Comparing Bioavailability of Cadmium and Arsenic in Agricultural Soil Under Varied pH Condition

  • Oh, Se Jin;Kim, Sung Chul;Ok, Yong Sik;Oh, Seung Min;Lee, Bup Yeol;Lee, Sang Hwan;Yang, Jae E.
    • 한국토양비료학회지
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    • 제48권1호
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    • pp.57-63
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    • 2015
  • Bioavailability of cadmium (Cd) and arsenic (As) can be different depending on soil pH. For this reason, main purpose of this research was to compare bioavailability of Cd and As in agricultural field under varied soil pH and different extractants. Bioavailable fraction of Cd and As in soil was extracted with $CaCl_2$, $NaNO_3$, DTPA, EDTA, and low molecular weight organic acids (LMWOAs). Soil samples and cultivated crops were collected at the range of soil pH 4.5-8.5 and correlation analysis was conducted between bioavailable fraction of Cd and As in soil and total concentration of Cd and As in crops. Results showed that concentration of Cd and As in acidic soil was ranged $0.002-0.462mg\;kg^{-1}$ and $0.041-4.903mg\;kg^{-1}$ respectively. In alkaline condition, concentration of Cd and As were ranged $0.006-0.351mg\;kg^{-1}$ and $0.039-2.807mg\;kg^{-1}$ respectively. Comparing bioavailable fraction of Cd and As in acidic and alkaline soil condition, higher concentration was measured in acidic condition. Similarly, higher average concentration of Cd and Asin crops was observed in acidic condition (0.398 and $0.751mg\;kg^{-1}$ respectively) than alkaline condition (0.248 and $0.264mg\;kg^{-1}$). Among different extractants, LMWOAs method showed higher correlation ($r^2=0.545$) for Cd in acidic condition indicating that LMWOAs method could be applied for evaluating bioavailability of Cd in acidic soil. However, no high correlation was observed for As in both acidic and alkaline condition. Overall, bioavailable fraction of Cd and As can be higher in acidic condition of soil than alkaline condition resulting higher uptake of Cd and As from soil to crops. Therefore, efficient best management practice (BMPs) for Cd and As in acidic soil should be conducted for minimizing uptake of Cd and As into crops.

인삼 산성다당체의 비색정량 방법과 그 추출조건 및 안정성 (Colorimetric Determination of Acidic Polysaccharide from Panax ginseng, its Extraction Condition and Stability)

  • 도재호;이형옥
    • Journal of Ginseng Research
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    • 제17권2호
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    • pp.139-144
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    • 1993
  • The method for colorimetric determination of acidic polysaccharide from Panax ginseng was investigated. It is possible to apply the method of carbazole-sulfuric acid to determination of pectin, and also to measure the amount of pectin in the mixture of various high molemlu compounds such as starch. cellulose and gum, etc. When the method of carbazole-sulfuric acid was applied to determine the amount of acidic polysaccharide, optical density at 525 nm increased linearly with an increase in the concentration of pure acidic polysaccharide. Effective extraction temperature with water for the determination of the amount of ginseng acidic polysaccharide (GAP) was $80{\circ}C$. In order to separate or concentrate GAP it was appropriate to precipitate the extract only once with 80% ethyl alcohol. GAP was very stable at $100{\circ}C$ for 4 hrs in aqueous solution and between pH values of 5.0~ 12.0.

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인삼박으로부터 수용성 산성다당체의 추출 조건 분석 (Analysis of the Extraction Condition of Soluble Acidic Polysaccharides from Ginseng Marc)

  • 최유진;황금희
    • 생약학회지
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    • 제42권1호
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    • pp.82-88
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    • 2011
  • This study was carried out to investigate the optimum conditions for extraction of soluble acidic polysaccharides from ginseng marc. Method of carbazole-sulfuric acid was applied to determine the amount of acidic polysaccharides in ginseng marc. The amounts of soluble acidic polysaccharides in water extract of ginseng marc were increased with increasing extraction temperature. The contents of acidic polysaccharides were not significantly different despite the extraction time increasing from 0.5 hours to 6 hours. To estimate the rehydration rate of the freeze dried polysaccharide, the extracted acidic polysaccharide fraction powder was determined the amount of soluble acidic polysaccharides by carbazole-sulfuric acid method again. The rehydration rate of acidic polysaccharides from water-extract of red ginseng marc at room temperature was 100%. On the other hand, the rehydration rate of acidic polysaccharide of red ginseng marc at boiling temperature was about 50%. The rehydration rate of acidic polysaccharides from water-extract of white ginseng marc at room temperature was 50%. The rehydration rate of acidic polysaccharide of red ginseng marc at boiling temperature was about 40%. The rate of soluble acidic polysaccharide of Red Ginseng is higher than that of White Ginseng. We can find out the maximum extraction method of soluble acidic polysaccharide from ginseng marc.

Accurate Chiral Discrimination of Acidic- and Amino acidic-Chiral Drugs by Indirect GC and Direct CE Enantiomeric Separation Methods

  • Kim, Kyoung-Rae
    • 대한약학회:학술대회논문집
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    • 대한약학회 2002년도 Proceedings of the Convention of the Pharmaceutical Society of Korea Vol.2
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    • pp.167-168
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    • 2002
  • Because of the differences between biological and pharmacological properties of chiral drugs in human body, accurate determinations of their optical purities have been in great need. There are two major approaches in chiral separation: indirect method performed under achiral condition, and direct method under the chiral environment. We have been conducting chiral separation of acidic chiral compounds and also amino acidic chiral compounds employing indirect GC methods and direct CE enantiomeric separation methods. (omitted)

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닭발의 침지조건이 닭발 젤라틴에 미치는 영향 (Effect of Soaking Condition on the Physicochemical Properties of Chicken Feet Gelatin)

  • 장은경;임주연;김광옥
    • 한국식품과학회지
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    • 제34권3호
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    • pp.425-430
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    • 2002
  • 본 연구에서는 축산 부산물인 닭발을 산과 알칼리에 각각 침지하여 제조한 젤라틴의 이화학적 특성을 조사하였다. 침지조건에 따른 아미노산 함량은 큰 차이가 없었으나 상업적으로 판매되는 돈피나 소가죽 젤라틴과는 그 조성이 달랐다. 이는 원료의 특성과 제조공정의 차이에서 기인하는 것으로 사료된다. 젤라틴의 수율과 젤라틴 겔의 경도는 산성 조건에서 24시간 침지한 경우에, 알칼리 조건에서 1주 침지한 경우에 가장 높다고 평가되었다. 점도와 투명도는 침지기간이 증가함에 따라 산성 조건에서는 증가한 반면 알칼리 조건에서는 감소하였다. 색도는 산처리 닭발 젤라틴 겔이 알칼리처리 젤라팅 겔에 비해 L값은 높고, a값과 b값이 낮아 미관상 더 바람직하다. 이화학적 특성이 우수한 산처리 24시간 침지 시료와 알칼리 처리 1주 침지 시료의 분자량 분포를 Gel permeation chromatography로 살펴본 결과, 두 시료 모두 12개의 획분으로 구성되었다. 가장 많이 발견되는 분자량은 669 kD으로 알칼리 처리 시료가 산처리 시료에 비해 두 배나 많았으며, 300 kD 이하는 산처리 시료가 알칼리 처리군에 비해 현저히 많아 산처리 시료가 알칼리 처리군에 비해 상대적으로 저분자화 되어있었다.

산성 및 유기성 가스의 동시제거를 위한 준건식 세정시스템의 적정 운전 조건 (Optimal Operation Condition of Spray Drying Sorber for Simultaneous Removal of Acidic and Organic Gaseous Pollutants)

  • 백경렬;구자공
    • 한국환경과학회지
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    • 제10권1호
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    • pp.59-64
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    • 2001
  • The effect of major operating parameters in spray drying sorber(=SDS) for automatic control for the simultaneous removal of acidic and organic gaseous pollutants from solid waste incinerator was performed. The field experiment was carried out in pilot scale test for the quantification of major operating parameters of hydrophilic and the hydrophobic pollutants. The removal efficiencies of $SO_2$and HCI in the 5wt% slurry condition were being increased with the increase of the stoichiometric ration which is the molecular ratio of lime to the pollutant concentration, and with the decrease of inflow flue gas temperature in the pilot SDS reactor. The removal efficiency along the height of spray drying sorber was closely related to the temperature profile, and more than 90% of total removal efficiency was achieved in an absorption region. For the removal of acidic gas the optimum operating condition considering the economics and a stable operation is the 5wt% of slurry concentration, 1.2 of stoichiometric ratio and 25$0^{\circ}C$ of inflow flue gas temperature. For the organic gases of benzene and toluene the removal efficiencies were 20-60% which is much lower than that of acidic gas. The best removal efficiency was obtained at 1.5 of stoichiometric ratio and 25$0^{\circ}C$ of inflow flue gas temperature. The organic\`s removal efficiency along the height of spray drying sorber was quite different from that of acidic gas, that is, more than 60% of the total removal efficiency for benzene and 90% of the total removal for toluene were achieved in the dried adsorption region, which was formed at the lower or exit part of the reactor.

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산당화과정을 이용한 볏짚으로부터 셀룰로스 에탄올의 제조 (Production of Rice Straw Based Cellulosic Ethanol Using Acidic Saccharification)

  • 이승범;정수경;이재동
    • 공업화학
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    • 제21권3호
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    • pp.349-352
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    • 2010
  • 이산화탄소 저감을 위한 바이오에너지의 개발이 활발히 진행되고 있는 가운데 본 연구에서는 산당화과정을 이용하여 볏짚으로부터 셀룰로스 에탄올의 제조공정을 해석하고자 하였다. 전처리 과정으로는 초음파에너지를 이용한 수화과정과 10~30 wt%의 황산을 이용한 산당화과정을 진행하였으며, 발효과정에서는 10~50 wt%의 효모를 이용하여 3~6 일간 발효시켜 셀룰로스 에탄올 수율을 결정하였다. 최적 전처리조건으로는 375W의 초음파세기로 30 min 간 수화시킨 후 20 wt%의 황산을 이용하여 산당화과정을 2 h 동안 진행하는 것을 추천할 수 있으며, 30 wt%의 효모를 이용하여 3일간 발효하는 것이 가장 높은 셀룰로스 에탄올 수율을 얻을 수 있었다.

토양 세척을 통한 살충제 (파라티온, 다이아지논)로 오염된 토양의 정화 (Remediation of Insecticides (Parathion, Diazinon) Contaminated Soil by Washing Process)

  • 현재혁;백정선;조미영
    • 한국지하수토양환경학회:학술대회논문집
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    • 한국지하수토양환경학회 1999년도 추계학술발표회
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    • pp.3-6
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    • 1999
  • Several chemical washing procedures were applied to Parathion and Diazinon contaminated soil. Batch and column tests were performed to determine the insecticides extraction efficiency as a function of pH. Washing efficiency of methanol is more higher than that of water and HCl when washed parathion and diazinon are. Those are completely miscible with most organic solvents. For parathion, release trend is increased as pH is increased because it is hydrolyzed easily at the condition of alkali. But diazinon shows reverse because diazinon is decomposed rapidly at the condition of acidic So, diazinon is more released than parathion is because this experiment is peformed in acidic and weak acidic conditions. Generally, parathion and diazinon are classified as having low mobility, so they can be easily controlled if the proper washing process are applied.

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효소에 의한 초지용 펠트의 세척효과 (Cleaning Effect of Papermaking Felt with Enzymes)

  • 윤병태;김성보;엄태진;최명재
    • 펄프종이기술
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    • 제37권3호
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    • pp.17-22
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    • 2005
  • The cleaning efficiency of papermaking felt which is contaminated with fiber fines and various micro-materials was investigated and compared between the application of enzyme and commercial detergent. It was found that the cleaning efficiency by the treatment of acidic-based detergent was more efficient than that of alkaline-based one in the conventional commercial detergent. it was also observed that the treatment design of first acidic-based detergent treatment to second alkaline-based detergent procedure was better in the cleaning efficiency, compared to alkaline based-to-acidic based one. The cleaning property of felt with enzyme was resulted in good cleaning efficiency, without any addition of surfactant. Especially, the enzyme treatment under alkaline condition (pH 10) showed a better cleaning result than that under acidic condition(pH 5). The addition of nonionic surfactant to the enzyme increased the cleaning efficiency of felt and decreased the cationic demand of wastewater. These results showed more favour than the application of conventional commercial detergent.