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Effect of Magnetic Field Annealing on Microstructure and Magnetic Properties of FeCuNbSiB Nanocrystalline Magnetic Core with High Inductance

  • Fan, Xingdu;Zhu, Fangliang;Wang, Qianqian;Jiang, Mufeng;Shen, Baolong
    • Applied Microscopy
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    • v.47 no.1
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    • pp.29-35
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    • 2017
  • Transverse magnetic field annealing (TFA) was carried out on $Fe_{73.5}Cu_1Nb_3Si_{15.5}B_7$ nano-crystalline magnetic core with the aim at decreasing coercivity ($H_c$) while keeping high inductance ($L_s$). The magnetic field generated by direct current (DC) was applied on the magnetic core during different selected annealing stages and it was proved that the nanocrystalline magnetic core achieved lowest $H_c$ when applying transverse field during the whole annealing process (TFA1). Although the microstructure and crystallization degree of the nanocrystalline magnetic core exhibited no obvious difference after TFA1 compared to no field annealing, the TFA1 sample showed a more uniform nanostructure with a smaller mean square deviation of grain size distribution. $H_c$ of the nanocrystalline magnetic core annealed under TFA1 decreased along with the increasing magnetic field. As a result, the certain size nanocrystalline magnetic core with low $H_c$ of 0.6 A/m, low core loss (W at 20 kHz) of 1.6 W/kg under flux density of 0.2 T and high $L_s$ of $13.8{\mu}H$ were obtained after TFA1 with the DC intensity of 140 A. The combination of high $L_s$ with excellent magnetic properties promised this nanocrystalline alloy an outstanding economical application in high frequency transformers.

Magnetic Properties of Transition Metal-implanted ZnO Nanotips Grown on Sapphire and Quartz

  • Raley, Jeremy A.;Yeo, Yung-Kee;Hengehold, Robert L.;Ryu, Mee-Yi;Lu, Yicheng;Wu, Pan
    • Journal of Magnetics
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    • v.13 no.1
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    • pp.19-22
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    • 2008
  • ZnO nanotips, grown on c-$Al_2O_3$ and quartz, were implanted variously with 200 keV Fe or Mn ions to a dose level of $5{\times}10^{16}cm^{-2}$. The magnetic properties of these samples were measured using a superconducting quantum interference device (SQUID) magnetometer. Fe-implanted ZnO nanotips grown on c-$Al_2O_3$ showed a coercive field width of 209 Oe and a remanent field of 12% of the saturation magnetization ($2.3{\times}10^{-5}emu$) at 300K for a sample annealed at $700^{\circ}C$ for 20 minutes. The field-cooled and the zero-field-cooled magnetization measurements also showed evidence of ferromagnetism in this sample with an estimated Curie temperature of around 350 K. The Mn-implanted ZnO nanotips grown on c-$Al_2O_3$ showed superparamagnetism resulting from the dominance of a spin-glass phase. The ZnO nanotips grown on quartz and implanted with Fe or Mn showed signs of ferromagnetism, but neither was consistent.

A Study of Magnetic Field Characteristic of Field coil in HTS motor (HTS 전동기용 계자코일의 자장 특성 연구)

  • 이정종;조영식;홍정표;손명환;김석환;권영길
    • Progress in Superconductivity and Cryogenics
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    • v.4 no.2
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    • pp.47-51
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    • 2002
  • In this paper, flux distribution and operating current is calculated according to the field coil change in HTS(High Temperature Superconducting) motor. In order to calculate magnetic field characteristic of the field coil. it is computed by changing the outer radius and the inner width of field coil Bio-Savart equation is used as the analysis method for the characteristic analysis of magnet. 2D and 3D FEA(Finite Element Analysis) is used for the magnetic field distribution in HTS motor The operating current is calculated by $B{\bot}$ linked With the field coil and $I_c-B curve of superconductor.

Path Planning of Mobile Robot using a Potential Field (퍼텐셜 필드를 이용한 이동 로봇의 경로 계획)

  • Jung Kyung-Kwon;Kang Seung-Ho;Chung Sung-Boo;Eom Ki-Hwan
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2006.05a
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    • pp.701-705
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    • 2006
  • This paper propose a method of mobile robot path planning for prevention of slip using potential field. The path planning minimizes robot slip for the potential field method to smooth a potential barrier. In order to verify the effectiveness of the proposed method, we performed simulations on path planning with C-obstacles in the workspace. The results show that the proposed method considerably improves on the performance of the general potential field method.

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A Study on the Rotation of Uniaxial Anisotropy Field of NiFe Thin Film by Magnetic Annealing (자기장 내 열처리에 의한 퍼멀로이 박막의 일축 이방성 자기장의 회전에 관한 연구)

  • 송용진;김기출;이충선
    • Journal of the Korean Magnetics Society
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    • v.11 no.4
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    • pp.163-167
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    • 2001
  • The rotation of uniaxial anisotropy field of 700 ${\AA}$ thick sputtered NiFe thin film due to magnetic annealing was investigated. NiFe film was annealed in a magnetic field which is perpendicular to the initial induced uniaxial anisotropy field. The NiFe film becomes nearly isotropic after 1 hour annealing at 160 $^{\circ}C$. With increase of annealing temperature over 160 $^{\circ}C$, the film gets uniaxial anisotropy field again. An abrupt increase of H$\sub$c/ was observed with annealing temperature over 400 $^{\circ}C$. The X-ray diffraction analysis and Auger electron spectroscopy with Ar ion etching showed extensive grain growth in NiFe film with (111) texturing and interdiffusion with adjacent Au electrode layer by 400 $^{\circ}C$ magnetic annealing.

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EVENTUAL SHADOWING FOR CHAIN TRANSITIVE SETS OF C1 GENERIC DYNAMICAL SYSTEMS

  • Lee, Manseob
    • Journal of the Korean Mathematical Society
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    • v.58 no.5
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    • pp.1059-1079
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    • 2021
  • We show that given any chain transitive set of a C1 generic diffeomorphism f, if a diffeomorphism f has the eventual shadowing property on the locally maximal chain transitive set, then it is hyperbolic. Moreover, given any chain transitive set of a C1 generic vector field X, if a vector field X has the eventual shadowing property on the locally maximal chain transitive set, then the chain transitive set does not contain a singular point and it is hyperbolic. We apply our results to conservative systems (volume-preserving diffeomorphisms and divergence-free vector fields).

Oxygen Profiles and Precipitation Behavior in CZ Silicon Crystals Grown in A Transverse Magnetic Field (수평자장 하에서 성장된 CZ 실리콘 단결정의 산소 분포 및 석출거동)

  • Kim, Kyeong-Min;Choi, Kwang-Su;P. Smetana;T.H. Strudwick;Lee, Mun-Hui
    • Korean Journal of Materials Research
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    • v.2 no.2
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    • pp.119-125
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    • 1992
  • Oxygen segregation in horizontal-magnetic-field-applied Czochralski (HMCZ) silicon crystals has been studied as a function of magnetic field strength (B) and crucible rotation rate (C). Along the axis of 57mm din. <100> crystals grown under B=2, 3, 4 kG and C=4-15rpm, the oxygen distribution was usually saw-tooth shaped and fluctuated unevenly. Compared to the conventional CZ method, this result seems to indicate that the horizontal magnetic field, at levels used in the present experiment, had a destabilizing influence on oxygen transport to the growth interface. On the other hand, as C increased, the oxygen fluctuation lessened, and [0] increased overall. At B=2 kG, an oxygen profile in a level of 27-36 ppma was achieved by a programmed ramp of C. Oxygen precipitation behavior of the HMCZ silicon during a simulated device manufacturing process was compared and found to be inferior to that of typical CZ silicon. The uneven oxygen profile in the as-grown state was identified as the major source of poor precipitation uniformity in the HMCZ silicon.

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Comparative molecular field analyses (CoMFA) on the antifungal activity against phytophthora blight fungus of 3-phenylisoxazole and 3-phenyl-2,5-dihydroisoxazol-5-one derivatives (고추 역병균에 대한 3-phenylisoxazole과 3-phenyl-2,5-dihydroisoxazol-5-one 유도체들의 살균 활성에 관한 비교 분자장 분석 (CoMFA))

  • Sung, Nack-Do;Lee, Hee-Chul
    • The Korean Journal of Pesticide Science
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    • v.6 no.2
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    • pp.72-79
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    • 2002
  • 3D-QSAR between fungicidal activitives ($pI_{50}$) against metalaxyl-sensitive (SPC: 95CC7105) or metalaxyl-resisitant (RPC: 95CC7303) isolate of phytophthora blight fungus (Phytophthora capsici), and a set of 3-phenylisoxazole (A) and 3-phenyl-2,5-dihydroisoxazole (B) derivatives as substrates were conducted using comparative molecular field analyses (CoMFA). The antifungal activities of (A) were generally higher than those of (B). And it is assumed that the most stable conformation of the active substrate was approximately planar from conformational search. The CoMFA models proved a good predictive ability and suggested that the electronic field of substrates were higher than hydropohobic field and steric field requirements for recognition forces of the receptor site. And the factors were strongly correlated (cross-validated $q^2>0.570$ & conventional $r^2>0.968$) with the fungicidal activitives. According to the CoMFA analyses, the selectivity factors for RPC suggested that the sterically bulky groups (C14 & C15) and electron withdrawing groups (C15 & C16) have to be introduced to the ortho, meta and para-position on the benzoyl moiety of substrates.

Effect of deposition temperature on field emission property of carbon thin film grown by PECVD (PECVD에 의해 작성된 탄소계 박막의 전계전자방출특성에 대한 증착온도 의존성에 관한 연구)

  • ;;M. Katayama;;K. Oura
    • Journal of the Korean Vacuum Society
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    • v.12 no.1
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    • pp.35-39
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    • 2003
  • Using RF plasma enhanced chemical vapor deposition, amorphous carbon films were grown in pure methane plasma. Field electron emission of these films were examined at a function of deposition temperature. It was found that the electron emission current of the sample prepared at deposition temperature above $600^{\circ}C$ was considerably improved. The film grown at deposition temperature of $800^{\circ}C$ had the best threshold field of 8 V/$\mu\textrm{m}$ in this experiment. According to the results of Raman spectroscopy. growth of graphite crystallites was promoted with higher deposition temperatures. Moreover the surface morphology was abruptly changed at deposition temperature above $600^{\circ}C$. We discuss the field electron emission characteristics of amorphous carbon films with regard to the structural feature and surface morphology.

Synthesis and Lubricant Properties of Nitrogen doped Amorphous Carbon (a-C:N) Thin Films by Closed-field unbalanced Magnetron Sputtering Method (비대칭 마그네트론 스퍼터링법에 의한 비정질 질화탄소 박막의 합성 및 윤활 특성)

  • Park, Yong-Seob;Cho, Hyung-Jun;Choi, Won-Seok;Hong, Byung-You
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.20 no.8
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    • pp.701-705
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    • 2007
  • The incorporation of N in a-C film is able to improve the friction coefficient and the adhesion to various substrates. In this study, a-C:N films were deposited on Si and steel substrates by closed-field unbalanced magnetron (CFUBM) sputtering system in $Ar/N_2$ plasma. The lubricant characteristics was investigated for a-C:N deposited with total working pressure from 4 to 7 mTorr. We obtained high hardness up to 24GPa, friction coefficient lower than 0.1 and the smooth surface of having the extremely low roughness (0.16 nm). The physcial properties of a-C:N thin film are related to the increase of cross-linked $sp^2$ bonding clusters in the film. However, the decrease of hardness, elastic modulus and the increase of surface roughness, friction coefficient with the increase of $N_2$ partial pressrue might be due to the effect of energetic ions as a result of the increase of ion bombardment with the increase of ion density in the plasma.