• Title/Summary/Keyword: X-Ray scattering

Search Result 455, Processing Time 0.03 seconds

Temperature Dependent Octahedral Tilting Behaviors of Monoclinic and Tetragonal SrRuO3 Thin Films

  • Lee, Sung Su;Seo, Okkyun;Kim, Jaemyung;Song, Chulho;Hiroi, Satoshi;Chen, Yanna;Katsuya, Yoshio;Sakata, Osami
    • Journal of the Korean Physical Society
    • /
    • v.73 no.10
    • /
    • pp.1529-1534
    • /
    • 2018
  • We used in-situ synchrotron X-ray scattering to investigate phase transformations of octahedral tilted monoclinic $SrRuO_3$ (MSRO) and tetragonal SRO (TSRO) thin films on $SrTiO_3$ (STO) substrates. The octahedral tilted MSRO thin films were highly crystalline and the monoclinic distortion angle was $0.45^{\circ}$. The phase transition temperature from the MSRO to TSRO phase occurred at approximately $200^{\circ}C$ as a second order transition. Conversely, no phase transformations of the TSRO thin film occurred within the range from RT to $250^{\circ}C$. The octahedral $RuO_6$ rotation was strongly affected by the phase transformation in the SRO thin films.

Effect of X-ray Exposure on Phase Separation of Lysozyme-Water Mixture (X선 쬐임이 단백질-물 상분리에 미치는 영향)

  • Cho, Chang-Ho;Sung, Syng-Hoon;Lee, Sang-Soo;Cho, Kun-woo
    • The Journal of Natural Sciences
    • /
    • v.11 no.1
    • /
    • pp.23-26
    • /
    • 1999
  • Phase separation temperature of lysozyme-water mixture increased with X-ray exposure on lysozyme and decreased with impurity of saponin. The intensity of light scattering in lysozyme-water mixture with X-ray exposure on lysozyme decreased as a function as a function of temperature, and decreased with impurity of saponin.

  • PDF

High-pressure synchrotron X-ray diffraction study of tremolite and actinolite in various fluids

  • Kong, Mihye;Vogt, Thomas;Lee, Yongjae
    • Current Applied Physics
    • /
    • v.18 no.11
    • /
    • pp.1218-1224
    • /
    • 2018
  • Pressure-dependent structural and morphological changes of two amphibole minerals, tremolite and actinolite, were investigated up to 7.0 GPa using synchrotron X-ray powder diffraction underthree different pressure transmission media (PTM): water (W), $CO_2$ and silicone oil (SI). The elastic response of tremolite and actinolite are found to be dependent on the PTM used. When using water (W) as PTM, tremolite and actinolite show normal volume contractions with bulk moduli of 74(1) and 78(1) GPa, respectively. When using $CO_2$ as PTM, we observe the formation of calcite from tremolite above 3.8(1) GPa, whereas actinolite did not show any carbonation reaction. Under silicone oil PTM, we observe modulated volume contraction behaviors in both samples, compared to water and $CO_2$ PTM, with bulk moduli in the order of 90(1) and 94(4) GPa for tremolite and actinolite, respectively.

Evaluation of Scattered Rays of Jelly Type Shielding Body by L-spine AP using X-ray (L-Spine X-선 촬영에서의 Jelly type 차폐체의 산란선 차폐평가)

  • Jang, Hui-Min;Kim, Do-Gwon;Kim, Hyeong-Bin;Yoon, Joon
    • Journal of the Korean Society of Radiology
    • /
    • v.14 no.7
    • /
    • pp.907-913
    • /
    • 2020
  • There have been continuous controversies on medical X-ray protection and numerous researchers have been trying to prevent unnecessary exposure to radiation. As X-ray passes through the patient and obtains an image, it creates scattered ray due to interactions such as photoelectric effect and Compton scattering with the subject. As a result, both medical radiation staff and patient are exposed to unnecessary radiation on areas other than the target area. In response, this study will be assuming a body of a female, radiating X-ray on the phantom under the conditions of lumbar spine AP test, and measuring scattered ray around breasts and thyroid glands. Then, The experiment results were as follows. After application of non-shielding material, the average of scattered ray was 0.88 mR in thyroid measurement, 3.34 mR, Lt Axillary 3.54 mR, and Rt Axillary 3.03 mR in mamonary measurement but, After application of shielding material, the average of scattered ray was 0.16 mR in thyroid measurement, 0.60 mR, Lt Axillary 0.64 mR, and Rt Axillary 0.54 mR in mamonary measurement showing average scattered ray protection effect of about 82%. This study suggested the manufacturing method of a Jelly-type shielding material, identified the possibilities of researches on mixing various substances with radiology field, and verified the usability of the Jelly-type shielding material as a substitute for existing protection tools.

DETECTABILITY OF SUNGRAZING COMET SOFT X-RAY IRRADIANCE (SUNGRAZING 혜성이 방출하는 X-선 관측 가능성에 관한 연구)

  • Oh, Su-Yeon;Yi, Yu;Nah, Ja-Kyoung;Kim, Yong-Ha
    • Journal of Astronomy and Space Sciences
    • /
    • v.24 no.4
    • /
    • pp.309-314
    • /
    • 2007
  • Originating from the Oort cloud, some comets disappear to impact against the Sun or to split up by strong gravitational force. Then they don't go back to the Oort cloud. They are called sungrazing comets. The comets are detected by sublimation of ices and ejection of gas and dust through solar heat close to the Sun. There exists the charge transfer from heavy ions in the solar wind to neutral atoms in the cometary atmosphere by interaction with the solar wind. Cometary atoms would be excited to high electronic levels and their do-excitation would result in X-ray emission, or it would be scattering of solar X-ray emission by very small cometary grains. We calculated the X-ray emission applying the model suggested by Mendis & Flammer (1984) and Cravens (1997). In our estimation, the sungrazing comet whose nucleus size is about 1 km in radius might be detectable within a distance of 3 solar radius from the sun on soft X-ray solar camera.

Numerical Modeling and Experiment for Single Grid-Based Phase-Contrast X-Ray Imaging

  • Lim, Hyunwoo;Lee, Hunwoo;Cho, Hyosung;Seo, Changwoo;Lee, Sooyeul;Chae, Byunggyu
    • Progress in Medical Physics
    • /
    • v.28 no.3
    • /
    • pp.83-91
    • /
    • 2017
  • In this work, we investigated the recently proposed phase-contrast x-ray imaging (PCXI) technique, the so-called single grid-based PCXI, which has great simplicity and minimal requirements on the setup alignment. It allows for imaging of smaller features and variations in the examined sample than conventional attenuation-based x-ray imaging with lower x-ray dose. We performed a systematic simulation using a simulation platform developed by us to investigate the image characteristics. We also performed a preliminary PCXI experiment using an established a table-top setup to demonstrate the performance of the simulation platform. The system consists of an x-ray tube ($50kV_p$, 5 mAs), a focused-linear grid (200-lines/inch), and a flat-panel detector ($48-{\mu}m$ pixel size). According to our results, the simulated contrast of phase images was much enhanced, compared to that of the absorption images. The scattering length scale estimated for a given simulation condition was about 117 nm. It was very similar, at least qualitatively, to the experimental contrast, which demonstrates the performance of the simulation platform. We also found that the level of the phase gradient of oriented structures strongly depended on the orientation of the structure relative to that of linear grids.

Performance Analysis of Low-level Radiation Shielding Sheet with Diamagnetic Nanoparticles

  • Cho, Jae-Hwan;Kim, Myung-Sam
    • Journal of Magnetics
    • /
    • v.20 no.2
    • /
    • pp.103-109
    • /
    • 2015
  • In this study, the authors attempted to produce a medical radiation shielding fiber that can be produced at a nanosize scale and that is, unlike lead, harmless to the human body. The performance of the proposed medical radiation shielding fiber was then evaluated. First, diamagnetic bismuth oxide, an element which, among elements that have a high atomic number and density, is harmless to the human body, was selected as the shielding material. Next, 10-100 nm sized nanoparticles in powder form were prepared by ball milling the bismuth oxide ($Bi_2O_3$), the average particle size of which is $1-500{\mu}m$, for approximately 10 minutes. The manufactured bismuth oxide was formed into a colloidal solution, and the radiation shielding fabric was fabricated by curing after coating the solution on one side or both sides of the fabric. The thicknesses of the shielding sheets prepared with bismuth oxide were 0.1, 0.2, 0.3, 0.4, 0.5, 0.6, 0.7, 0.8, and 1.0 mm. An experimental method was used to measure the absorbed dose and irradiation dose by using the lead equivalent test method of X-ray protection goods presented by Korean Industrial Standards; the resultant shielding rate was then calculated. From the results of this study, the X-ray shielding effect of the shielding sheet with 0.1 mm thickness was about 55.37% against 50 keV X-ray, and the X-ray shielding effect in the case of 1.0 mm thickness showed shielding characteristics of about 99.36% against 50 keV X-ray. In conclusion, it is considered that nanosized-bismuth radiation shielding fiber developed in this research will contribute to reducing the effects of primary X-ray and secondary X-ray such as when using a scattering beam at a low level exposure.

Contemplation on Usefulness of Plane Cone for Taking Image of Intercondyloid Fossa (무릎 과간와(Intercondyloid fossa) 촬영용 평면 Cone의 유용성에 대한 고찰)

  • Shin, WoonJae
    • Journal of the Korean Society of Radiology
    • /
    • v.9 no.7
    • /
    • pp.501-508
    • /
    • 2015
  • There are various Intercondyloid fossa X-ray taking methods. The methods carried out in clinics are Holmblad method, Camp-Conventry method, and Beclere method. Taking image of Intercondyloid fossa is carried a lot as basic examination for diagnosis related to simple fracture and cruciate ligament. Considering the condition and pains of patients, safe method is chosen but because Holmblad method can cause pains to knee part adhering to cassette, it is not easily used. In this study self-produced plane circular cone was attached to a cassette and in the posture for Holmblad method questionnaires of 100 applicants were analyzed to understand cognition on alleviation of pains, and the concentration of imge quality by scattering rays was measured with densitometer by taking human body phantom with X-ray. As a result, in the posture for Holmblad method, cognition on pains was alleviated by average 99%, and the change of concentration of X-ray film taken using phantom by scattering rays decreased statistically significantly compared to the cassette which did not use self-produced plane cone, therefor it is thought that the method can be valuably used in clinics.

Phase Analysis of Immiscible V-Cu MA Powders by Neutron and X-ray Diffraction (비고용 V-Cu계 MA합금의 중성자 및 X선 회절에 의한 상분석)

  • Lee Chung-Hyo;Cho Jae-Moon;Lee Sang-Jin;Kim Ji-Soon
    • Korean Journal of Materials Research
    • /
    • v.14 no.5
    • /
    • pp.348-352
    • /
    • 2004
  • The mechanical alloying (MA) effect in immiscible V-Cu system with positive heat of mixing was studied by not only the neutron and X-ray diffraction but also the analysis of DSC spectra. The total energy, ΔHt accumulated during MA for the mixture of $V_{50}$ $Cu_{50}$ / powders increased with milling time and approached the saturation value of 14 kJ/mol after 120 h of milling. It can be seen that the free energy difference between the amorphous phase and the pure V and Cu powders with an atomic ratio 5:5 is estimated to be 11 kJ/mol by Miedema et al. This is thermodynamically taken as one of the evidences for the amorphization. The structural changes of V-Cu MA powders were characterized by the X-ray diffraction and neutron diffraction. We take a full advantage of a negligibly small scattering length of the V atom in the neutron diffraction measurement. The neutron diffraction data definitely indicate that the amorphization proceeds gradually but incompletely even after 120 h of MA and bcc-Cu Bragg peaks appears after 60 h of MA.

6H-SiC epitaxial growth and crystal structure analysis (6H-SiC 에피층 성장과 결정구조 해석)

  • Kook-Sang Park;Ky-Am Lee
    • Journal of the Korean Crystal Growth and Crystal Technology
    • /
    • v.7 no.2
    • /
    • pp.197-206
    • /
    • 1997
  • A SiC epilayer on the 6H-SiC crystal substrate was grown by chemical vapor deposition (CVD). The crystal structure of the SiC epilayer was investigated by using the X-ray diffraction patterns and the Roman scattering spectroscopy. The SiC epilayer on the 6H-SiC substrate was grown to be homoepilayer by CVD. In order to distinguish a certain SiC polytype mixed in the SiC crystal grown by the modified Lely method, we have calculated the X-ray diffraction intensities and Brags angles of the typical SiC crystal powders. By comparing the measured X-ray diffraction pattern with the calculated ones, it was identified that the SiC crystal grown by the modified Lely method was the 6H-SiC crystal mixed some 15R-SiC.

  • PDF