• Title/Summary/Keyword: Wet coating

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Mechanical Device Design for Solvent Usage Reduction for Amine Group Substitution and Production of NH2-HNT (아민기 치환 시 용매 사용량 절감을 위한 기계 장치 설계 및 NH2-HNT 제조)

  • Moon il Kim
    • Journal of Environmental Science International
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    • v.32 no.6
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    • pp.477-482
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    • 2023
  • Halloysite nanotube (HNT) has a nanotube structure with the chemical formula of Al2Si2O5(OH)4 · nH2O and is a natural sediment of aluminosilicate. A lot of research has been conducted to improve the mechanical properties of epoxy composites by generating interactions between HNTs and polymers through surface treatment of HNTs, such as exchange of amine group as a terminal functional group. However, most of the surface modification methods are performed under wet conditions, which require a relatively large amount of time, manpower and solvent. In order to save time and simplify complicated procedures, a dry coating machine was designed and used for amine group exchange. Comparing the XPS results, it was found that the results of NH2-HNT prepared using a dry coating machine and the substitution through the wet method were not significantly different, and it has been confirmed that the amount of solvent used and the time savings can be made.

Fabrication of Transparent Color Coating Glass by Sol-gel Method (솔-젤법을 이용한 투명 칼라 코팅유리 제조)

  • Park, Jong-Guk;Jeon, Dae-Woo;Lee, Mi-Jai;Lim, Tea-Young;Hwang, Jonghee;Kim, Jin-Ho
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.29 no.1
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    • pp.40-43
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    • 2016
  • Transparent color coating films were fabricated on a glass substrate by using sol-gel hybrid binder and organic dye. Sol-gel hybrid binder coating film fabricated with PTMS of 0.03 mole showed a very high pencil hardness of 9 H. As the withdrawal speed increased from 1.0 mm/s to 5.0 mm/sec, The yellowness ($b^*$) of coating glass also gradually increased. The transmittance of yellow color coating glass was 82.6% and the haze of coating glass was 0.35%. Red and blue color coating glasses also showed the high transmittance of 62.4% and 80.6% respectively. The surface hardness of color coating films was 6 H.

Effect of Solvents on Physical Properties and Release Characteristics of Monolithic Hydroxypropylmethylcellulose Matrix Granules and Tablets

  • Cao Qing-Ri;Choi Yun-Woong;Cui Jing-Hao;Lee Beom-Jin
    • Archives of Pharmacal Research
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    • v.28 no.4
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    • pp.493-501
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    • 2005
  • Effect of solvents on physical characteristics and release characteristics of monolithic acetaminophen (APAP) hydroxypropylmethylcellulose (HPMC) matrix granules and tablets were examined. Various types and amounts of solvents were employed for granulation and coating. APAP and other excipients were mixed and were then wet-granulated in a high-speed mixer. The dried granules were then directly compressed and film-coated with low viscosity grade HPMC. As the amount of water increased, the size of granules also increased, showing more spherical and regular shape. However, manufacturing problems such as capping and lamination in tableting occurred when water was used alone as a granulating solvent. The physical properties of HPMC matrix granules were not affected by the batch size. The initial release rate as well as the amount of APAP dissolved had a tendency to decrease as the water level increased. Addition of nonaqueous solvent like ethanol to water resulted in good physical properties of granules. When compared to water/ethanol as a coating solvent, the release rate of film-coated HPMC matrix tablets was more sensitive to the conditions of coating and drying in methylene chloride/ethanol. Most of all, monolithic HPMC matrix tablet when granulated in ethanol/water showed dual release with about $50\%$ drug release immediately within few minutes followed by extended release. It was evident that the type and amount of solvents (mainly water and ethanol) were very important for wet granulation and film-coating of monolithic HPMC matrix tablet, because the plastic deforming and fragmenting properties of material were changed by the different strengths of the different solvents.

Analysis of the Sol-Gel Coating Process for the Preparation of Supported TiO2 Composite Membranes ($TiO_2$ 복합 분리막의 제조를 위한 졸-겔 코팅공정 분석)

  • 현상훈;최영민
    • Journal of the Korean Ceramic Society
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    • v.29 no.5
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    • pp.403-409
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    • 1992
  • The titania membrane thickness coated on the porous alumina support by the sol-gel method was analyzed using the slipcasting model. The thickness of calcined membrane layers increased linearly from 1.3 to 3.8 ${\mu}{\textrm}{m}$ with the square root of the dipping time (4~40 min). Growth rates of the thickness of wet gels and calcined layers were well described quantitatively by the slipcasting model. Through the regression of experimental data using model equations, the permeability and the pressure drop across wet gels, and the thickness and their growth rate constants of wet gels and calcined layers could be determined. It was also known that the gellation concentration of the TiO2 sol used in this work and the porosity of wet gel layes were 25 mol/ι and 0.53, respectively.

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Fabrication of a (100) Silicon Master Using Anisotropic Wet Etching for Embossing

  • Jung, Yu-Min;Kim, Yeong-Cheol
    • Journal of the Korean Ceramic Society
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    • v.42 no.10 s.281
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    • pp.645-648
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    • 2005
  • To fabricate a (100) silicon hard master, we used anisotropic wet etching for the embossing. The etching chemical for the sili­con wafer was a TMAH 25$\%$ solution. The anisotropic wet etching produces a smooth sidewall surface inclined at 54.7°, and the surface roughness of the fabricated master is about 1 nm. After spin coating an organic-inorganic sol-gel hybrid resin on a silicon substrate, we used the fabricated master to form patterns on the silicon substrate. Thus, we successfully obtained patterns via the hot embossing technique with the (100) silicon hard master. Moreover, by using a single hydrophobic surface treatment of the master, we succeeded in achieving uniform surface roughness of the embossed patterns for more than ten embossments.

Influences of Wet-Pressing Types on Internal Structure of Paper (습부압착 방식이 종이의 내부구조에 미치는 영향)

  • Lee Jin-Ho;Park Jong-Moon
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.37 no.4 s.112
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    • pp.32-37
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    • 2005
  • To Increase the productivity of a paper machine, the maximization of the machine speed is a kind of simple way As the machine speed increases, more intense wet pressing is required to persist the outlet consistency of press part and reduce the water removal of dryer part. With more intense pressing, there are concerns that the quality of paper will be affected. This study was carried out to evaluate the influence of wet-pressing on internal structure of paper, The nip pressure at the first and third nip in triple nip press was controlled. Paper structures, strength properties and pore properties were evaluated. As a result, first nip pressure more strongly influenced the paper structural properties than third nip pressure in triple nip pressing condition. Because of the high water content and low wet-web strength of paper web in first nip, increasing the first nip pressure induced the incipient crushing of wet-web and then caused a potential of web break during the following coating or printing processes.

Recent progress of Ergonomics Studying in CRTs Design and Manufacturing

  • Wu, Mingli;Duan, Cheng
    • 한국정보디스플레이학회:학술대회논문집
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    • 2004.08a
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    • pp.450-452
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    • 2004
  • This paper analyzes some important achievements in Ergonomics field in CRT industry. After introducing principal regulatory requirements for CRTs, including ISO 9241 and TCO standards, the paper indicates some theoretical research in ergonomics of the display devices, such as new contrast parameter for appraising the display devices and effects of environment on visual performance at the ergonomic. Then, as the pivot of this paper, some practical progress, in the ergonomics field in CRT manufacturing , are described, such as vacuum sputtering process for advanced CRTs, new developed wet process for getting the multi-coating layers on surface of the panel.

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Plastic Substrate for Flexible Display

  • Kim, In-Sun;Hwang, Hee-Nam;Choi, Jae-Moon;Yeom, Eun-Hee;Park, Yong-Ho
    • 한국정보디스플레이학회:학술대회논문집
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    • 2005.07b
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    • pp.995-997
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    • 2005
  • A plastic substrate for flexible display is developed. The gas barrier and optical properties of the substrate is improved through depositing silicon oxide/nitride layer and coating polymer layer on plastic film by sputtering process and wet coating process. Roll to roll processes will guarantee the productivity in the whole production process of the plastic substrate.

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Electrochemical Properties of Needle Coke through a Simple Carbon Coating Process for Lithium Ion Battery (침상 코크스의 피치 코팅에 따른 리튬 이차전지 탄소계 음극소재의 전기화학적 특성)

  • Hwang, Jin Ung;Lee, Jong Dae;Im, Ji Sun
    • Applied Chemistry for Engineering
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    • v.31 no.5
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    • pp.514-519
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    • 2020
  • Graphite materials for lithium ion battery anode materials are the most commercially available due to their structural stability and low price. Recently, research efforts have been conducted on carbon coatings by improving side reactions at the edge site of carbon materials. The carbon coating process has classified into a CVD by chemical reaction, wet coating process with solvent and dry coating by mechanical impact. In this paper, the rapid crush/coating process was used to solve the problem of which only few parts of the carbon precursor (pitch) can be used and also environmental problems caused by solvent removal in the wet coating process. When the ratio of needle coke to pitch was 8 : 2 wt%, and the rapid crush/coating process was carried out, it was confirmed that the fracture surface was coated by pitch. The pitch-coated sample was treated at 2400 ℃ and 41.8% improvement in 10C/0.1C rate characteristic was observed. It is considered that the material simply manufactured through the simple crush/coating process can be used as an anode electrode material for a lithium ion battery.

Effects of Montmorillonite Clay on Properties of paper Coating Additives

  • Seo Yoon-Seok;Nah Chang-Woon
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.38 no.1 s.113
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    • pp.34-44
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    • 2006
  • A new composition of paper coating adhesives was prepared by using a nano-filler of an organically-modified montmorillonite (O-MMT). The new O-MMT coating adhesives were applied to the paper, and the properties of coated papers including surface morphology, optical and physical properties, and printing properties were investigated. The use of O-MMT improved the mechanical properties, such as folding endurance, tearing strength, and tensile strength, while the surface smoothness decreased. It decreased especially when the dosage was high enough, approximately above 6 parts. The printing properties such as wet- and dry-pick were enhanced with addition of O-MMT.