• Title/Summary/Keyword: Uniform Film

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Effects of Co Thickness on the Formation of Epitaxial CoSi2 Thin Film (Co 두께가 $CoSi_2$ 에피박막 형성에 미치는 영향)

  • 김종렬;배규식
    • Journal of the Korean Institute of Telematics and Electronics D
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    • v.34D no.1
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    • pp.23-29
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    • 1997
  • Effects of Co thickness on the formation of epitaxial $CoSi_2$ from the Co/Ti bilayer have been investigated. Ti and Co were sequentially deposited with the Ti thickness fixed at 5 or 10nm, while the Co thickness was varied from 5 to 30nm. The metal-deposited samples were then rapidly thermal-annealed in $N_2$ at $900^{\circ}C$ for 20 sec. Material properties of $CoSi_2$ thin films were analyzed by the 4-point probe, XRD, AES, andXTEM. When the as-deposited Co thickness was below 15nm, the $CoSi_2$ with high resistivity and rough interface was formed. On the other hand, when the Co thickness was above 15 nm, the epitaxial $CoSi_2$ with the resistivity of about 16 ~ 19 $\mu\Omega.cm$, uniform composition and thickness and flat interface was formed. Initial Ti thickness has sizable effect on the formation of $CoSi_2$, when the Co layer was very thin (~ 5 nm). But there was no significant effect of the Ti thickness for the initial Co thickness of above 15 nm.

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A Study on Sputtering Method for Uniform Deposition of CdTe Thin Film on Large-area Substrates (대면적 기판에 균일한 CdTe 박막 증착을 위한 스퍼터링 방법 연구)

  • Park, Ju-Sun;Lim, Chae-Hyun;Ryu, Seung-Han;Kim, Nam-Hoon;Yang, Jang-Tae;Lee, Woo-Sun
    • Proceedings of the KIEE Conference
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    • 2009.07a
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    • pp.1264_1265
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    • 2009
  • Cadmium Telluride (CdTe)를 이용한 박막형 태양전지 제작과 실용화에 있어 가장 큰 이슈는 대면적화에 따른 에너지 변환효율의 저하를 줄임으로써 고효율의 대면적 태양전지를 대량으로 생산하는 것이다. 따라서 본 연구에서는 태양전지 박막의 대면적 증착시 문제점 중에 하나인 불균일한 CdTe 박막의 증착을 방지하기 위한 선행연구를 진행하였다. 실험 방법으로는 Sputtering 법을 적용하여 박막 증착시 출력과 진공도에 따른 박막 두께의 표준편차와 RMS 표면 거칠기($R_{rms}$), 최고-최저점간 표면 거칠기($R_{p-v}$) 등의 거동을 고찰하였다. 이를 통해 Sputtering 공정 변수 중에 박막 두께의 표준 편차에 더 큰 영향을 미치는 변수를 조사하고, 후행 연구로 진행될 Sputtering 법을 이용하여 대면적에 균일하게 증착하는 방법에 적용하고자 한다.

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The fabrication and analysis of BSCT thick films for uncooled infrared detectors (비냉각 검출기를 위한 BSCT 후막의 제작과 특성 분석)

  • Noh, Hyun-Ji;Lee, Sung-Gap;Bae, Seon-Gi
    • Proceedings of the KIEE Conference
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    • 2008.10a
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    • pp.171-172
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    • 2008
  • $(Ba_{0.57}Sr_{0.33}Ca_{0.10})TiO_3$ (BSCT) thick films doped with 0.1 mol% $MnCO_3$ and $Yb_2O_3$ ($0.1{\sim}0.7$ mol%) were fabricated by the screen printing method on the alumina substrate. And the structural and electrical properties as a function of $Yb_2O_3$ amount were investigated. The lattice constants of the BSCT thick film doped with 0.1 mol% is 0.3955 nm. The specimen doped with 0.7 mol% $Yb_2O_3$ showed dense and uniform grains with diameters of about 6.3 mm. The thickness of all BSCT thick films was approximately 60 mm. The Curie temperature of the BSCT specimen doped with 0.1 mol% $Yb_2O_3$ was $18^{\circ}C$, and the dielectric constantand dielectric loss at this temperature was 4637 and 4.2%, respectively. The BSCT specimen doped with 0.1 mol% $Yb_2O_3$ showed the maximum value of $349{\times}10^{-9}C/cm^2K$ at Curie temperature. The figure of merit $F_D$ for specific detectivity of the specimens doped with 0.1 mol% $Yb_2O_3$ showed the highest value of $10.9{\times}10^{-9}Ccm/J$.

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Electrical Characterization of PZT and Electrodes after Dry Etching in Inductively Coupled plasma (유도결합 플라즈마를 이용한 PZT/전극의 식각 후 전기적 특성)

  • Kim, Kyung-Tae;Kang, Myoung-Gu;Park, Young;Song, Jun-Tae;Lee, Cheol-In;Jang, Eui-Goo;Kim, Chang-Il
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.07a
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    • pp.275-278
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    • 2001
  • Ferroelectric PZT thin films were fabricated on the RuO$_2$/Pt, Pt bottom electrode with a PZT(53/47) metal alkoxide solutions. All PZT thin films showed a uniform grain structure without the presence of rosette structure. The PZT thin films were etched as a function of Cl$_2$/Ar and additive CF$_4$ into Cl$_2$(80%)/Ar(20%). The etch rates of PZT thin films were 1970 ${\AA}$/min at 30 % additive CF$_4$ into Cl$_2$(80%)/Ar(20%). The remanent polarization and leakage current density in PZT thin film on the RuO$_2$/Pt were 64.2 ${\mu}$C/cm$^2$, 1.4${\times}$10$\^$-6/ respectively.

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The Preparation and Characterization of BLT Thin Films by MOD Process (MOD법을 이용한 BLT박막의 제초 및 특성에 관한 연구)

  • 이진한;장건익
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.07a
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    • pp.186.1-189
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    • 2001
  • Ferroelectric $Bi_{4-x}$La$_{x}$Ti$_3$O$_{12}$ (BLT)thin films with various compositions(x=0.65, 0.70, 0.75) were prepared on Pt//Ti/SiO$_2$/Si(100) substrate by metal-organic deposition. The electrical and structural characteristics of BLT thin films were investigated to develop ferroelectric thin films for capacitor layers of FRAM. After spin coating, thin films were annealed at $650^{\circ}C$ for 1hour in oxygen atomosphere. Scanning electron micrographs showed uniform surfaces composed of rod-like grains. The $Bi_{4-x}$La$_{x}$Ti$_3$O$_{12}$ (x=0.70) thin film capacitors with a Pt top electrode showed better ferroelectric properties than other films. At the applied voltage of 5V, the dielectric constant($\varepsilon$$_{r}$), dissipation factor(tan$\delta$),remanent polarization(2Pr), and coercive field(2Ec) of the $Bi_{4-x}$La$_{x}$Ti$_3$O$_{12}$ (x=0.70)thin films were about 272.54, 0.059, 32.4 $\mu$C/cm$^2$, 2Ec=119.9kV/cm. Also the capacitor did not show any significant fatigue up to 4.8$\times$10$^{10}$ read/write switching cycles.hing cycles.s.

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The Preparation and Characterization of BNdT Thin Films by MOD Process (MOD법을 이용한 BNdT박막의 제조 및 특성 연구)

  • Kim, Ki-Beom;Jang, Gun-Eik
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.07b
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    • pp.861-864
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    • 2002
  • Ferroelectric $Bi_{4-x}Nd_xTi_3O_{12}$(BNdT) thin films with the composition(x=0.75) were prepared on pt/Ti/$SiO_2$/Si(100) substrate by metal-organic deposition. The electrical and structural characteristics of BNdT thin films were investigated to develop ferroelectric thin films for capacitor layers of FRAM. After spin coating, thin films were annealed at $650^{\circ}C$ for 1hour in oxygen atmosphere. Scanning electron micrographs showed uniform surfaces composed of rod-like grains. The $Bi_{4-x}Nd_xTi_3O_{12}$(X=0.75) thin film capacitors with a Pt top electrode showed better ferroelectric properties. At the applied voltage of 5V, the dielectric constant$(\varepsilon_r)$, dissipation factor$(tan{\delta})$, remanent polarization(2Pr) and nonvolatile swiching charge of the $Bi_{4-x}Nd_xTi_3O_{12}$(x=0.75)thin films were about 346.7, 0.095, $56{\mu}C/cm^2$ and $38{\mu}C/cm^2$ respectively. Also the capacitor did not show any significant fatigue up to $8{\times}10^{10}$ read/write switching cycles at a frequency of 1MHz.

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Nano-Hydroxyapatite Modified by Grafting Polylactide and its Tissue Engineering Application

  • Zhuang, Xiuli;Zhang, Peibiao;Qiu, Xueyu;Chen, Xuesi;Jing, Xiabin
    • Proceedings of the Polymer Society of Korea Conference
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    • 2006.10a
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    • pp.182-182
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    • 2006
  • PLLA grafted Hydroxyapatite / polylactide (g-HA/PLA) composites were prepared by three grafting methods. The modified particles (p-HA) were dispersed more uniformly in the PLLA matrix than pure n-HA. The p-HA/PLLA composites exhibited better mechanical properties and thermal stability than the n-HA/PLLA composites. The composites also demonstrated improved cell compatibility due to the good biocompatibility of the HAP nanoparticles and the more uniform distribution of the PLLA-grafted HAP nanoparticles on the film surface. All of these results indicated that the p-HAP/PLLA nano-composites might have a promising medical application in bone repair and in bone tissue-engineering.

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Reactor design of PECVD system using a liquid aerosol feed method (미립액상법을 위한 PECVD 반응로설계)

  • 정용선;오근호
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.7 no.2
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    • pp.235-243
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    • 1997
  • The high-$T_c$ superconducting phase, $YBa_2Cu_3O_x$, was deposited on the single crystal MgO substrate, using a liquid aerosol feed method in a plasma enhanced chemical vapor deposition(PECVD) reactor. The effect of the plasma distribution depending on the design of a reactor was studied by the analysis of the microstructures of thin films. The particles landed were frequently observed on the films and the two causes that were responsible for the particle deposition were explained. The particles were deposited by the unstable and non-uniform plasma and the low evaporation rate of the precursors. Also, the thin film deposition rate decreased significantly as the distance between the evaporating location and the substrate increased.

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Preparation of Nano Wire by Anodic Oxidation I. Characteristics of Alumina Nano-Template by Anodic Oxidation (양극산화법에 의한 나노와이어 제조I. 알루미나 나노 템플레이트의 특성)

  • Jo, Su-Haeng;O, Han-Jun;Park, Chi-Seon;Jang, Jae-Myeong;Ji, Chung-Su
    • Korean Journal of Materials Research
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    • v.12 no.2
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    • pp.121-128
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    • 2002
  • Anodic alumina layer can be used as templates for preparation of nano-structured materials, because porous oxide layer on aluminum shows a uniform pore size and a high pore density. In order to find out possibility for template material to prepare nano wire, the effects of the anodic applied potential, anodic time and the temperature of electrolyte on pore diameter of anodic alumina layer were studied using SEM and AFM. The pore diameter of anodic alumina layer increased with applied anodic potential and electrolytic temperature. Especially, the pore diameter of anodic oxide layers formed in chromic acid can be well replicated by widening process in $H_3$$PO_4$solution.

A study on the characterization of stearic acid and PDA LB films and the optimum conditions for the stable films on the water (Stearic acid와 PDA LB막의 특성 분석과 막 형성 조건에 관한 연구)

  • Jeon, Yong-Joo;Kwon, O-Dae;Jeong, Sang-Don;Jeong, Cheol-Hyeong;Kim, Jang-Joo
    • Proceedings of the KIEE Conference
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    • 1989.11a
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    • pp.102-104
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    • 1989
  • The characteristics of stearic acid and PDA (pentacosaDiyonicAcid) LB films were studied using the XRD spectra for regularity of layers and ellipsometer for the total thickness of multilayer films. From the experiments of varying the PH and temperature, it was found that the stability of monolayer on the water subphase was very sensitive to its PH and temperature. The optimum condition of PH for the stable stearic acid LB film was 6$\sim$6.5. The PDA LB films were stable at the lower temperature than room temperature: we obtained very uniform PDA LB films at 12$^{\circ}C$.

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