• Bulletin of the Korean Chemical Society
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• 제30권1호
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• pp.92-96
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• 2009

A new precursor [$Zr(acac)_{3}(H_{2}O)_{2}$] was synthesized by Sonochemical technique and used to deposit thin $ZrO_{2}$ film on quartz and ceramic substrate via ultrasonic aerosol assisted chemical vapour deposition (UAACVD) at 300 ${^{\circ}C}$ in oxygen environment followed by annealing of the sample for 2-3 minutes at 500 ${^{\circ}C}$ in nitrogen ambient. The molecular structure of the precursor determined by single crystal X-ray analysis revealed that the molecules are linked through intermolecular hydrogen bonds forming pseudo six and eight membered rings. DSC and TGA/FTIR techniques were used to determine thermal behavior and decomposition temperature of the precursor and nature of evolved gas products. The optical measurement of annealed $ZrO_{2}$ film with tetragonal phase shows optical energy band gap of 5.01 eV. The particle size, morphology, surface structure and composition of deposited films were investigated by XRD, SEM and EDX.

• 한국해양공학회:학술대회논문집
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• 한국해양공학회 2003년도 춘계학술대회 논문집
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• pp.336-340
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• 2003

The frame synchronization should be acquired before performing other data-aided receiving algorithms, such as data-aided channel equalizing, beam-forming and phase, symbol timing, and frequency synchronizing, since all of them are using preamble or training sequence to estimate the amount of error from the received signal. In this paper, we present a new frame synchronization scheme for underwater ultrasonic image burst transmission system, which computes the correlation between received symbol sequence and one CAZAC sequence, composed of the latter half of the first CAZAC sequence of preamble and the first half of the second CAZAC sequence of preamble and then compares a threshold value. If the correlation value is bigger than the threshold value, the frame detector determines that the frame synchronization is achieved at that sample.

• Nuclear Engineering and Technology
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• 제54권11호
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• pp.4072-4083
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• 2022

Ultrasonic impact treatment (UIT) is carried out on the Ni-based alloy stainless steel pipe gas tungsten arc welding (GTAW) girth weld, the differences of microstructure, microhardness and shear strength distribution of the joint before and after ultrasonic shock are studied by microhardness test and shear punch test. The results show that after UIT, the plastic deformation layer is formed on the outside surface of the Ni-based alloy overlayer, single-phase austenite and γ type precipitates are formed in the overlayer, and a large number of columnar crystals are formed on the bottom side of the overlayer. The average microhardness of the overlayer increased from 221 H V to 254 H V by 14.9%, the shear strength increased from 696 MPa to 882 MPa with an increase of 26.7% and the transverse average residual stress decreased from 102.71 MPa (tensile stress) to -18.33 MPa (compressive stress), the longitudinal average residual stress decreased from 114.87 MPa (tensile stress) to -84.64 MPa (compressive stress). The fracture surface has been appeared obvious shear lip marks and a few dimples. The element migrates at the fusion boundary between the Ni-based alloy overlayer and the austenitic stainless steel joint, which is leaded to form a local martensite zone and appear hot cracks. The welded joint is cooled by FA solidification mode, which is forming a large number of late and skeleton ferrite phase with an average microhardness of 190 H V and no obvious change in shear strength. The base metal is all austenitic phase with an average microhardness of 206 H V and shear strength of 696 MPa.

• 한국음향학회지
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• 제43권3호
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• pp.361-367
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• 2024

공기중 초음파 측정은 각종 기계 설비류의 이상 발생 예방 활동으로 산업계에서 사용되고 있다. 최근에는 다수의 초음파 센서 배열을 이용하여 설비의 이상 발생 위치를 찾을 수 있는 공기중 초음파 영상화 기법의 활용이 증가하고 있다. 초음파 음원의 위치를 가시화하기 위해 센서 별 위상 차이를 이용하는 빔형성법이 사용된다. 2차원 평면에 분포된 초음파 센서 배열을 이용해 3차원 공간에서 빔형성 파워 분포를 구할 수 있다. 본 논문에서는 관심 파장보다 크기가 큰 초음파 센서로 구성된 랜덤 희소배열(random sparse array)을 사용하고, 초음파 배열이 분포한 평면으로부터 일정한 거리만큼 떨어진 평행한 평면 내에서의 빔형성 파워 분포를 통해서 음원의 위치를 보여주는 영상화 기법을 구현하고자 한다. 기존의 빔형성법은 사용 하는 배열 센서의 개수와 그에 따른 구경의 크기 등에 의해 공간 해상도가 제한될 수 밖에 없다. 본 연구에서는 배열이 가지는 기하학적 제약을 극복할 수 있는 방법으로 기능성 빔형성법을 적용하여 고해상도 초음파 영상화 기법을 구현하였다. 기능성 빔형성법은 수학적으로 일반화된 형태의 빔형성법으로 표현가능하고, 기존의 빔형성법을 통해 얻어진 영상에서 주엽의 폭과 부엽의 크기를 저감시키는 역할을 하여 고해상도 영상화를 얻을 수 있는 장점이 있다. 컴퓨터 시뮬레이션을 통해 제안한 방법에 의한 영상화 성능을 관찰한 결과, 초음파 희소배열을 이용하여 공기중 초음파 음원의 해상도 증대가 성공적으로 구현됨을 확인할 수 있었다.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2008년도 추계학술대회A
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• pp.1821-1824
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• 2008

A novel in-mold packaging process has been developed to manufacture devices with closed channels. In this unified process, fabrication of open channels and forming the rigid cover on top of them are sequentially integrated in the same mold. The entire process is comprised of two phases. In the first phase, the open channels are fabricated under an exquisitely controlled temperature and pressure using the conventional micro injection molding technology. In the second phase, the closed channels are fabricated by conducting the injection molding process using the molded structure with the open channels as a mold insert. As a result, the in-mold technology can eliminate the bonding processes such as heating, ultrasonic or chemical processes for cohesion between the channel and the cover, which have been required in conventional methods.

• 한국세라믹학회지
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• 제30권4호
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• pp.325-331
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• 1993

Aqueous solutions of metallic salts, ZrO(NO3)2.2H2O and Y(NO3)3.5H2O were used as raw materials to synthesize crystalline submicron spherical powders of Zr0.94Y0.06O1.97 with tetragonal crystal phase. Each aqueous solution was mixed on the magnetic stirrer to homogenize for 12 hours. The concentration of the mixed solutionwas changed from 0.01mol/$\ell$ to 0.1mol/$\ell$ calculated as the concentration of Zr0.94Y0.06O1.97. Ultrafine droplets of starting mixed solution were sprayed by the ultrasonic vibrator and carried into the furnace kept at 55$0^{\circ}C$, $650^{\circ}C$, 75$0^{\circ}C$ and 85$0^{\circ}C$ using carrier gas of air (10$\ell$/min) and pyrolysed to form Y-TZP fine powders. The results of this exeriment were as follows. 1) Synthesized powders were nonagglomerated and spherical type. 2) Particle size distribution was narrow between 0.1${\mu}{\textrm}{m}$ and 1${\mu}{\textrm}{m}$. 3) Forming reaction Y-TZP was finished above synthetic temperature 75$0^{\circ}C$. 4) As the synthetic temperature rised from 55$0^{\circ}C$ to 85$0^{\circ}C$, the mean particle size decreased from 0.35${\mu}{\textrm}{m}$ to 0.22${\mu}{\textrm}{m}$ in the concentration of starting solution with 0.02mol/$\ell$. 5) At 75$0^{\circ}C$ of synthetic temperature, the concentration changes of starting solution from 0.01mol/$\ell$ to 0.1mol/$\ell$ increased the mean particle size from 0.24${\mu}{\textrm}{m}$ to 0.38${\mu}{\textrm}{m}$. 6) Chemical compositions of each synthesized particle were homogeneous nearly.

• 한국건설순환자원학회논문집
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• 제5권4호
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• pp.395-402
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• 2017

최근 들어 박테리아를 이용하여 콘크리트의 수복하거나 박테리아 대사를 이용한 보수재료에 대한 연구가 수행되고 있다. 본 연구는 박테리아 대사를 이용하여 슬라임을 형성하며 이를 이용한 보수재료의 개발에 대한 기초적 연구로서 박테리아 슬라임을 포함한 시멘트 코팅재의 내구성 평가를 다루고 있다. 기초연구를 위해 4가지 박테리아(Rhodobacter capsulatus, Rhodopseudomonas palustris, Bacillus thuringiensis, Bacillus subtilis)과 2가지 배양조건이 고려되었으며, 제조된 코팅재를 사용하여 황산 5% 수용액에 노출에 따른 강도 변화, 염화물 확산계수, 초음파속도 평가가 수행되었다. 박테리아가 혼입된 코팅재의 경우 강도가 개선되었으며, 황산 5% 수용액 침지 이후에도 7일까지는 강도가 개선되었다. 염화물 확산계수도 Rhodopseudomonas palustris를 제외한 경우 충분한 염해저항성능을 나타내었으며, 초음파 속도 역시 우수하게 평가되었다. 장기열화에 대한 슬라임의 저항과 박테리아의 수명을 연장할 수 있는 호기성 환경이 유지된다면 대상 박테리아는 열화환경에 노출된 콘크리트 구조의 보수재 적용에 사용될 수 있는 공학적 가능성을 보여준다.

• 한국컴퓨터그래픽스학회논문지
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• 제25권3호
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• pp.31-41
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• 2019

포그 스크린은 미세한 물방울들로 구성된 스크린으로 관찰자는 포그 스크린을 투과한 영상을 관찰하게 된다. 일반 스크린과는 달리 관찰자는 무대 위에서 연기자가 포그 스크린에 표시된 이미지를 뚫고 들어가는 모습을 볼 수 있다. 본 논문에서는 상부에서 생성된 포그 입자 집단이 중력에 의하여 아래로 떨어질 때 평평한 수직 스크린을 이루도록 하는 하향식 포그 스크린 생성 장치 구현 방법을 기술한다. 본 기법은 수조안에 배치된 초음파 진동자에 의해 수조 표면에서 포그 입자가 발생되는 원리를 이용한다. 생성된 포그 집단이 하나의 평면을 유지할 수 있도록 포그가 나오는 통로 출구 양옆에 가이드 바람을 형성하는 기법과 포그 스크린 생성 장치의 설계와 제작 방법을 기술한다.

• 한국입자에어로졸학회지
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• 제6권2호
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• pp.61-67
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• 2010

In this paper, we describe a new method to form polymer thin films, in which carbon nanotubes (CNTs) are homogeneously distributed so that they can strengthen the mechanical property of resulting polymer film. To do so, we first homogeneously mixed CNTs with polymer in a DMF solvent. With the assistance of ultrasonic nebulizer, the polymer/CNT solution was then aerosolized into micro-sized droplets and finally turned into solidified polymer/CNT composite particles by gas-phase drying process. As the results of SEM and TEM analysis, CNTs were found to be homogeneously immobilized in the polymer matrix particles due to rapid drying process in the gas phase. For comparison purpose, (i) the polymer/CNTs composite particles prepared by aerosol processing method and (ii) polymer/CNTs sheets prepared by simple solution-evaporation method were employed to form polymer/CNTs composite thin films using a hot press. As the result, the aerosol processing of composite particles was found to be a much more effective method to form homogeneously distributed-CNTs in the polymer matrix thin film.

• 한국염색가공학회지
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• 제22권4호
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• pp.362-372
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• 2010

This paper surveys the physical properties of the multiwall carbon nanotube (MWNT) and polyurethane composite film for improvement of mechanical properties and electrical characteristics. The modification of MWNT was carried out by acid treatment with nitric and sulphuric acid mixed solution, and then followed by thermal treatment for enhancing MWNT dispersion with polyurethane. This modified MWNT was mixed with polyurethane by changing the loading content of MWNT and dispersion time under the dimethylformamide solution in the ultrasonic wave apparatus. Various physical characteristics of the modified PU/MWNT films were measured and analyzed in terms of the loading content and dispersion time. The maximum absorbance of the PU/MWNT films were observed with the 2wt% loading at dispersion times of 2 and 24 hour, respectively. The minimum electrical volume resistivity of PU/MWNT film was shown at the loading content of 0.5wt% or more irrespective of dispersion treating time. However the optimum condition was assumed to 2wt% loading at dispersion time of 2 hours by assessing the surface profile of the film using video microscope. The breaking stress and strain of the PU/MWNT film decreased with increasing loading content, but no change of physical properties was shown with increasing in dispersion time.