• Title/Summary/Keyword: Ultra-low temperature

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Effects of Ultra-high Pressure Homogenization on the Emulsifying Properties of Whey Protein Isolates under Various pH

  • Lee, Sang-Ho;Subirade, Muriel;Paquin, Paul
    • Food Science and Biotechnology
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    • v.17 no.2
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    • pp.324-329
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    • 2008
  • The effect of ultra-high pressure homogenization on the emulsifying properties of whey protein was investigated in a model emulsion made with whey protein isolate and soya oil under various pH. The emulsifying properties, the average diameter of the oil droplets ($d_{vs}$), and the protein load, were measured for each emulsion produced at different homogenization pressures (50 to 200 MPa) and pH values (4.6 to 8.0). According to the results of variance analysis and response surface, the pH had more influence on oil droplet size and protein load than homogenization pressure. The model equations, which were obtained by response surface analysis, show that pH and homogenization pressure had the major effect on oil droplet size and protein load. Higher homogenization pressure decreased the average droplet size and the protein load. Homogenization at high pressure, as opposed to low pressure, causes no overprocessing, but the effect was pH-dependent. The average diameter of the oil droplets increased slightly by decreasing the pH from 8.0 to 6.5 and then increased dramatically toward the isoelectric point of whey protein (i.e., at pH 4.6). Moreover associated droplets were found at acidic pH and their size was increased at high temperature.

A Study on the Characteristic of Weld Joint and Tensile Fracture of SUS304 and Cu High-Speed Dissimilar Lap Welds by Single Mode Fiber Laser (싱글모드 파이버 레이저를 이용한 SUS304와 Cu의 고속 겹치기 용접에서 접합부 및 인장시험 파단부의 특성에 관한 연구)

  • Lee, Su-Jin;Kim, Jong-Do;Katayama, Seiji
    • Journal of Welding and Joining
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    • v.32 no.6
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    • pp.56-63
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    • 2014
  • To develop and understand dissimilar metals joining of Stainless steel and Copper, ultra-high speed laser lap welding was studied using single mode fiber laser in this study. SUS304 and Cu have large differences in materials properties, and Cu and Fe have no intermetallic compounds by typical binary phase of Cu and Fe system. In this study, ultra-high speed lap welds of SUS304 and Cu dissimilar metals using single-mode fiber laser was generated, and weldability of the weld fusion zone was evaluated using a tensile shear test. To understand the phenomenon of tensile shear load, weld fusion zone of interface weld area and fracture parts after tensile shear test were observed using scanning electron microscopy (SEM) and energy dispersive X-ray spectroscopy (EDX) analysis system. And it was confirmed that Cu was easily melting and penetrating in the grain boundaries of SUS304 because of low melting temperature. And high thermal conductivity of copper occurred dissipate heat energy rapidly. These properties cause the solidification cracking in weld zone.

Study on Charge Transport in Nanoscale Organic Monolayers for Molecular Electronics Using Liquid Phase Electrodes

  • Hwang, Jin-Ha
    • Journal of the Microelectronics and Packaging Society
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    • v.12 no.3 s.36
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    • pp.235-241
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    • 2005
  • Incorporation of solid electrodes frequently involves plasma-based processing. The effect of plasma can influence the physical characteristics, depending on the magnitude in plasma. The undesired feature of plasma-induced damage should be prevented in characterizing the ultra-thin materials, such as ultra-thin films and organic monolayers. The current work at first proves the applicability of a liquid phase electrode in the electrical/dielectric properties through comparative work using Al and Hg on ultrathin $Al_2O_3$ films deposited through atomic layer deposition at low temperature: Two types of metals such as Aluminum (Al) and mercury (Hg) were used as electrodes in $Al_2O_3$ thin films in order to investigate the effect of electrode preparation on the current-voltage characteristics and impedance features as a function of thickness in $Al_2O_3$ film thickness. The success of Hg in $Al_2O_3$ thin films is applied to the AC and DC characterization of the organic monolayers obtained using the Langmuir-Blodgett method. From the DC current-voltage characteristics, the diode-like response is found to originate from the bulk response of the organic materials, evidenced by the fact and the capacitance is inversely related to the absolute thickness of organic layers.

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A Study on SiC Buffer Layer Prepared by Ultra High Vacuum Electron Cyclotron Resonance CVD (초고진공 전자공명 플라즈마를 이용한 SiC buffer layer 형성에 관한 연구)

  • Joen, Woo-Gon;Pyo, Jae-Hwak;Whang, Ki-Woong
    • Proceedings of the KIEE Conference
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    • 1995.11a
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    • pp.326-328
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    • 1995
  • SiC buffer layers were grown on Si(100) substrates by ultra-high-vacuum electron cryclotron resonance plasma (UHV ECR plasma) from $CH_4/H_2$ mixture at 700$^{\circ}C$. The electron densities and temperature were measured by single probe. The axial plasma potentials measured by emissive probe had the double layer structure at positive substrate bias. Piranha cleaning was carried out as ex-situ wet cleaning. Clean and smooth silicon surface were prepared by in-situ hydrogen plasma cleaning at 540$^{\circ}C$. A short exposure to hydrogen plasma transforms the Si surface from 1$\times$1 to 2$\times$1 reconstruction. It was monitored by reflection high energy electron diffraction (RHEED). The defect densities were analysed by the dilute Schimmel etching. The results showed that the substrate bias is important factor in hydrogen plasma cleaning. The low base pressure ($5\times10^{-10}$ torr) restrains the $SiO_2$ growth on silicon surface. The grown layers showed different characteristics at various substrate bias. RHEED and K-ray Photoelectron spectroscopy study showed that grown layer was SiC.

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An Experimental Study for Basic Properity of Ultra High-strength Concrete (초고강도 콘크리트의 기초물성에 관한 실험적 연구)

  • Kim Ji-Man;Gong Min-Ho;Yang Dong-Il;Jung Sang-Jin
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2006.05a
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    • pp.39-42
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    • 2006
  • Recently, more highly effective construction materials are needed for the reasonable and economical structure system is required as the construction structures become more multi storied, large-sized and diversified. That is to say, the highly qualified concrete, the molt universal construction material is positively promoted as a part of plan to establish the effective space according to the dead load of structures and diminish of segment profile and to build up the economic structures. In particular, it is tendency of that the study for high strength concrete increases and construction example of reinforced concrete (RC) using the high strength concrete partially increases. However, the high strength concrete has the problems such high brittleness and low ductility. Specially, for the high strength concrete, it has different strength from normal concrete as the internal temperature goes up steadily due to high heat of hydration by the quantities of highly level of cement, so the concrete which is mixed with various scible materials is used. This study conducted a basic experiment to conclude an adequate selection of materials and to calculate an optimal mixing proportion of those materials to produce High-strength concrete. And also we conducted an experiment to find out basic properties of this concrete such as slump-flow, strength.

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Study of strength Development of Ultra High-Strength Concrete (초고강도 콘크리트의 강도발현에 관한 기초적 연구)

  • Min, Hong-Jun;Gong, Min-Ho;Lim, Nam-Gi;Lee, Young-Do;Jung, Sang-Jin
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2006.11a
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    • pp.75-79
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    • 2006
  • Recently, more highly effective construction materials are needed for the reasonable and economical structure system is required as the construction structures become more multi storied, large-sized and diversified. That is to say, the highly qualified concrete is positively promoted as a part of plan to establish the effective space according to the dead load of structures and diminish of segment profile and to build up the economic structures. However, the high strength concrete has the problems such high brittleness and low ductility. Specially, for the high strength concrete, it has different strength from normal concrete as the internal temperature goes up steadily due to high heat of hydration by the quantities of highly level of cement, so the concrete which is mixed with various miscible materials is used. As the development and study for high strength concrete (more than $100N/mm^2$) is under way actively and the strength of high strength concrete increases, the strength different from the existing high strength concrete of ten than $100N/mm^2$, but the study for this is not adequate and indefinite. In addition, the study and report to apply the strength expression and analysis results of internal structure. Therefore, this study is an experiment about using the miscible materials affects what happens to the longitudinal physical property.

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Formation of a MnSixOy barrier with Cu-Mn alloy film deposited using PEALD

  • Moon, Dae-Yong;Hwang, Chang-Mook;Park, Jong-Wan
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.02a
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    • pp.229-229
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    • 2010
  • With the scaling down of ultra large integrated circuits (ULSI) to the sub-50 nm technology node, the need for an ultra-thin, continuous and conformal diffusion barrier and Cu seed layer is increasing. However, diffusion barrier and Cu seed layer formation with a physical vapor deposition (PVD) method has become difficult as the technology node is reduced to 30 nm and beyond. Recent work on self-forming barrier processes using PVD Cu alloys have attracted great attention due to the capability of conformal ultra-thin barrier formation using a simple technique. However, as in the case of the conventional barrier and Cu seed layer, PVD of the Cu alloy seed layer will eventually encounter the difficulty in conformal deposition in narrow line trenches and via holes. Atomic layer deposition (ALD) has been known for its good step coverage and precise thickness control, and is a candidate technique for the formation of a thin conformal barrier layer and Cu seed layer. Conformal Cu-Mn seed layers were deposited by plasma enhanced atomic layer deposition (PEALD) at low temperature ($120^{\circ}C$), and the Mn content in the Cu-Mn alloys were controlled form 0 to approximately 10 atomic percent with various Mn precursor feeding times. Resistivity of the Cu-Mn alloy films decreased by annealing due to out-diffusion of Mn atoms. Out-diffused Mn atoms were segregated to the surface of the film and interface between a Cu-Mn alloy and $SiO_2$, resulting in self-formed $MnO_x$ and $MnSi_xO_y$, respectively. No inter-diffusion was observed between Cu and $SiO_2$ after annealing at $500^{\circ}C$ for 12 h, indicating an excellent diffusion barrier property of the $MnSi_xO_y$. The adhesion between Cu and $SiO_2$ was enhanced by the formation of $MnSi_xO_y$. Continuous and conductive Cu-Mn seed layers were deposited with PEALD into 32 nm $SiO_2$ trench, enabling a low temperature process, and the trench was perfectly filled using electrochemical plating (ECD) under conventional conditions. Thus, it is the resultant self-forming barrier process with PEALD Cu-Mn alloy film as a seed layer for plating Cu that has further potential to meet the requirement of the smaller than 30 nm node.

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Transparent Capacitor of the $Bi_2Mg_{2/3}Nb_{4/3}O_7$(BMNO)-Bi Nanostructured Thin Films grown at Room Temperature

  • Song, Hyeon-A;Na, Sin-Hye;Jeong, Hyeon-Jun;Yun, Sun-Gil
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2011.10a
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    • pp.20.2-20.2
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    • 2011
  • BMNO dielectric materials with a pyrochlore structure have been chosen and they have quite high dielectric constants about 210 for the bulk material. In the case of thin films, 200-nm-thick BMNO films deposited at room temperature showed a low leakage current density of about $10^{-8}\;A/cm^2$ at 3 V and a dielectric constant of about 45 at 100 kHz. Because high dielectric constant BMNO thin films kept an amorphous phase at a high temperature above $900^{\circ}C$. High dielectric constant BMNO thin films grown at room temperature have many applications for flexible electronic devices. However, because the dielectric constant of the BMNO films deposited at room temperature is still low, percolative BMNO films (i.e., those were grown in a pure argon atmosphere) sandwiched between ultra-thin BMNO films grown in an oxygen and argon mixture have greater dielectric constants than standard BMNO films. However, they still showed a leakage problem at a high voltage application. Accordingly, a new nano-structure that uses BMNO was required to construct the films with a dielectric constant higher than that of its bulk material. The fundamental reason that the BMNO-Bi nano-composite films grown by RF-Sputtering deposition had a dielectric constant higher than that of the bulk material was addressed in the present study. Also we used the graphene as bottom electrode instead of the Cu bottom electrode. At first, we got the high leakage current density value relatively. but through this experiment, we could get improved leakage current density value.

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Evaluation on Spalling Properties of Ultra High Strength Concrete with Melting and Vaporization of Fiber (유기섬유의 용융 및 기화에 따른 초고강도 콘크리트의 폭렬 특성 평가)

  • Kim, Gyu-Yong;Choe, Gyeong-Cheol;Lee, Joo-Ha;Lee, Seung-Hoon;Lee, Tae-Gyu
    • Journal of the Korea Concrete Institute
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    • v.24 no.2
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    • pp.173-183
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    • 2012
  • Recently, experimental studies to prevent explosive spalling based on spalling mechanism and addition of Polypropylene fiber in high strength concrete (HSC) are performed actively. However, with respect to ultra high strength concrete (UHSC), its compact internal structure is more difficult release vapor pressure at rapid rising temperature compared to HSC. Therefore, in this study, an experiment was conducted to evaluate spalling properties of UHSC using ${\Box}$ $100mm{\times}100{\times}H200mm$ rectangular specimen according to ISO-834 standard fire curve. With respect melting point of fiber, three fiber types of Polyethylene, Polypropylene, and Nylon fibers with melting temperature of $110^{\circ}C$, $165^{\circ}C$, and $225^{\circ}C$, respectively, were considered. Mixed fiber of 0.15% and 0.25% of concrete volume was used to consider spalling properties based on water vapor pressure release. Then, TGDTA test on fiber and FEM analysis were performed. The results showed that it is difficult to prevent initial spalling without loss of fiber mass even if fiber melting temperature is low. Also, in preventing thermal spalling, fiber that melts to rapidly create porosity within 10 minutes of fire is more effective than that of low melting temperature property of fiber.

Control and Design of a Arc Power Supply for KSTAR's the Neutral Beam Injection

  • Ryu, Dong-Kyun;Lee, Hee-Jun;Lee, Jung-Hyo;Won, Chung-Yuen
    • Journal of Electrical Engineering and Technology
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    • v.10 no.1
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    • pp.216-226
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    • 2015
  • The neutral beam injection generate ultra-high temperature energy in the tokamak of nuclear fusion. The neutral beam injection make up arc power supply, filament power supply and acceleration & deceleration power supply. The arc power supply has characteristics of low voltage and high current. Arc power supply generate arc through constant output of voltage and current. So this paper proposed suitable buck converter for low voltage and high current. The proposed buck converter used parallel switch because it can be increased capacity and decrease conduction loss. When an arc generated, the neutral beam injection chamber occur high voltage. And it will break output capacitor of buck converter. Therefore the output capacitor was removed in the proposed converter. Thus the proposed converter should be designed for the characteristics of low voltage and high current. Also, the arc power supply should be guaranteed for system stability. The proposed parallel buck converter enables the system stability of the divided low output voltage and high current. The proposed converter with constant output be the most important design of the output inductor. In this paper, designed arc power supply verified operation of system and stability through simulation and prototype. After it is applied to the 288[kW] arc power supply for neutral beam injection.