• 한국재료학회지
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• 제28권5호
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• pp.295-300
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• 2018

Effects of annealing temperature on the microstructure and mechanical properties through thickness of a Cu-3.0Ni-0.7Si alloy processed by differential speed rolling are investigated in detail. The copper alloy with a thickness of 3 mm is rolled to a 50 % reduction at ambient temperature without lubricant and subsequently annealed for 0.5 h at $200-900^{\circ}C$. The microstructure of the copper alloy after annealing is different in the thickness direction depending on the amount of the shear and compressive strain introduced by the rolling; the recrystallization occurs first in the upper roll side and center regions which are largely shear-deformed. The complete recrystallization occurs at an annealing temperature of $800^{\circ}C$. The grain size after the complete recrystallization is finer than that of the conventional rolling. The hardness distribution of the specimens annealed at $500-700^{\circ}C$ is not uniform in the thickness direction due to partial recrystallization. This ununiformity of hardness corresponds well to the amount of shear strain in the thickness direction. The average hardness and ultimate tensile strength has the maximum values of 250 Hv and 450 Mpa, respectively, in the specimen annealed at $400^{\circ}C$. It is considered that the complex mode of strain introduced by rolling directly affects the microstructure and the mechanical properties of the annealed specimens.

• Macromolecular Research
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• 제14권5호
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• pp.552-558
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• 2006

Biodegradable nanofibrous poly(L-lactic acid) (PLLA) scaffold was prepared by an electrospinning process for use in tissue regeneration. The nanofiber scaffold was treated with oxygen plasma and then simultaneously in situ grafted with hydrophilic acrylic acid (AA) to obtain PLLA-g-PAA. The fiber diameter, pore size, and porosity of the electrospun nanofibrous PLLA scaffold were estimated as $250\sim750nm,\;\sim30{\mu}m$, and 95%, respectively. The ultimate tensile strength was 1.7 MPa and the percent elongation at break was 120%. Although the physical and mechanical properties of the PLLA-g-PAA scaffold were comparable to those of the PLLA control, a significantly lower contact angle and significantly higher ratio of oxygen to carbon were notable on the PLLA-g-PAA surface. After the fibroblasts were cultured for up to 6 days, cell adhesion and proliferation were much improved on the nanofibrous PLLA-g-PAA scaffold than on either PLLA film or unmodified nanofibrous PLLA scaffold. The present work demonstrated that the applications of plasma treatment and hydrophilic AA grafting were effective to modify the surface of electrospun nanofibrous polymer scaffolds and that the altered surface characteristics significantly improved cell adhesion and proliferation.

• Journal of Welding and Joining
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• 제31권2호
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• pp.16-20
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• 2013

Titanium and its alloys have been widely using in the various field of industry application due to high corrosion resistant properties and mechanical properties. Titanium is highly reactive in the high temperature state and the formation of titanium oxide and porosities in the nuggets of fusion welding will results in the degradation of the mechanical properties. For this reason the studies of friction stir welding for titanium have been investigated recently. The FSW zones of titanium were classified by the weld nugget (WN), the linear transition boundary (TB) and the heat affected zone (HAZ). The WN along with titanium parent was characterized by the presence of twins and dislocations. The average grain size and hardness of WN has been changed according to heat input. The grain refinement resulted from the FSW increased the hardness in the stir zone. Sound dissimilar joints between SUS 304 and CP-Ti were achieved using an advancing speed of 50 mm/min and rotation speeds in the range of 700-1100 rpm. Aluminum 1060 and titanium alloy Ti-6Al-4V plates were lap joined by friction stir welding, hence the ultimate tensile shear strength of joint reached 100% of Al 1060. Mg alloy and Ti were successfully butt joined by inserting a probe into the Mg alloy plate with slightly offsetting. But Ti-Al intermetallic compound layers formed at the interface of these joints.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 2008년도 춘계 학술발표회 제20권1호
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• pp.49-52
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• 2008

유리섬유를 사용한 섬유강화복합체(Glass Fiber Reinforced Polymer, GFRP) 보강근의 인장강도 및 부착성능 등은 철근과 다르기 때문에 GFRP 보강근을 콘크리트 구조물에 적용하기 위해서는 GFRP 보강근으로 보강된 콘크리트 부재의 거동에 관한 연구가 선행되어야 한다. GFRP는 높은 비강도, 경량성, 비부식성 등의 장점을 가지고 있으나 탄성계수가 철근보다 작아 상대적으로 큰 처짐이 발생하는 단점이 있다. 교량 바닥판은 아칭효과 등에 의해 휨성능이 증가하므로 FRP 보강근을 우선 적용할 수 있는 대상 중 하나이다. 본 논문은 국내에서 개발된 철근 대체재용 GFRP 보강근의 콘크리트 구조물로의 적용 가능성을 관찰하기 위한 실험연구에 관한 것으로 폭과 길이가 3,000 mm, 4,000 mm이고 두께가 240 mm인 실제 크기의 콘크리트 바닥판을 제작하여 GFRP 보강근의 보강비에 따른 거동을 관찰하였다. 정적실험을 수행하였으며 DB-24 하중등급의 축하중을 모사한 재하면적을 가진 직사각형 강재로 바닥판이 파괴될 때까지 집중하중을 가하였다. 철근 보강 바닥판과 GFRP 보강 바닥판의 거동차이를 최대성능 및 처짐 거동 등에 대해 비교 검토하였다.

• 설비공학논문집
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• 제21권11호
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• pp.613-620
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• 2009

The thermal stresses of a ceramic heat exchanger were analyzed numerically since the ceramic material is good in heat resistance but weak in the thermal stress. The analysis of thermal stress was conducted in the ceramic core with two boundary conditions depending on bolt jointing. The thermal stresses were computed by applying temperature and pressure distributions obtained from the numerical results of conjugate heat transfer to ANSYS WORKRBENCH. When number of bolt joining halls was reduced from $8\times2$ to $4\times2$, the maximum principal stresses decrease by 47.6~50.5% and increase in safety factors by 2.18~2.5 for ultimate tensile strength. Thus, it can be said that bolt joining halls should be minimized in ceramic heat exchanger to be efficient in reducing thermal stress. In addition, the width of particular gas flow passages were revised from 52 mm to 42 mm to reduce maximum thermal stresses since certain passages experienced high thermal stresses. From the revision, safety factors were increased by 13.8~14.1% for the boundary condition of $4\times2$ bolt joining halls. Therefore, it is suggested that thermal stress can be reduced by changing local geometry of a ceramic heat exchanger.

• Elastomers and Composites
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• 제6권1호
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• pp.71-81
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• 1971

The intention of this study is to investigate the properties of polymer blend, NBR/PVC vulcanizates and blending procedures such as roll-mixing temperatures and sequences for polymer blending of NBR and PVC(resin type). The results obtained are as follows: 1. The roll temperature applied for polymer blending is around $150^{\circ}C$. At this temperature region, the degradation of rubber stock, which may be caused by heat, can be minimized and mill processing in practical application in industries can also be facilitated. 2. It is obviously necessary that a small amount of plasticizers should be added to the stock for improving processibility of roll mixing and physical properties. 3. On roll-mixing sequence, it is more effective that PVC compounded with plasticizer is added to NBR milled on hot roll. 4. The vulcanizates of the blends with different degree of polymerization of PVC ale similar to one another in properties. 5. NBR/PVC(70/30) blends shows the better physical characters than eve,-made foreign latex blend except abrasion-resistance. 6. As PVC addition ratio is increased, the physical properties such as resistance to ozone, tear, heat and oil and tensile strength, modulus, hardness have also improved, on the other hand, tension set and rebound character decreased. 7. The curve of ultimate elongation have point of inflection at the ratio of $30\sim40$ part of PVC. 8. While CR is blended, the physical properties such as brittle point, rebound and resistance to oil in high temperature have improved. 9. Polymer blend of NBR and domestic PVC is applied for the industrial utility such as rubber sole and heel, electric wire cover and oil-resistant packing, coating and gasket, printing roll, film for food packing etc.

• 폴리머
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• 제32권6호
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• pp.580-586
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• 2008

4,4'-(Hexafluoroisopropylidene) diphthalic anhydride (6FDA) 와 1,3-bis (3-aminophenoxy) benzene(BAPB)의 조성에 2,2-bis [4-(4-aminophenoxy)phenyl] hexafluoropropane (BAPP)를 다양한 몰 비에 따른 폴리이미드(PI) 공중합체를 합성하였다. PI 공중합체 필름들은 여러 열처리 과정을 통하여 용액 캐스팅 (solution casting)된 폴리아믹산(PAA)으로부터 얻었다. 퓨리에 변환 적외선 분광기(FT-IR), 넓은 각 X-선 회절(XRD), 전계 방사형 주사 전자 현미경(FE-SEM) 시차 주사 열량계(DSC)와 열 중량 분석기(TGA), 만능 인장 시험기 (UTM) 그리고 자외선-가시광선 흡광도기 (UV-Vis. spectrometer) 등을 사용하여 PI 공중합체 필름의 열적 기계적 성질, 모폴로지 및 광학 투명도를 측정하였다. PI 공중합체 필름의 유리전이온도 및 최종 강도와 초기 탄성률은 BAPP의 몰 비가 증가할수록 증가하였으나, 초기분해온도는 BAPP의 몰 비 증가에 무관하게 일정하였다. BAPP가 charge transfer complex를 형성하는 이유로 BAPP 농도가 증가함에 따라 PI 공중합체 필름의 투명도는 약간씩 감소하였다.

• 한국지반환경공학회 논문집
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• 제15권2호
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• pp.59-66
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• 2014

본 논문에서는 석션파일의 인발거동을 조사하기 위해 유한차분법 상용 프로그램인 FLAC3D를 이용하여 수치해석을 수행하였다. 석션파일의 인발지지력을 전통적인 지지력 식을 이용하여 구하고, 이 값을 파일의 직경, 길이, 그리고 주변 점토의 비배수 전단강도를 변수로 하는 수치해석을 통한 해석 값과 비교하였다. 총 24개의 수치해석 결과를 바탕으로 석션파일의 인발파괴는 석션파일의 배수조건뿐만 아니라 파일의 제원과 주변 지반의 물성값에 의해 형태가 결정되는 것으로 밝혀졌다. 수치해석 결과로부터 석션파일 내부 주면에 발현되는 전단응력을 구하여 활동파괴와 인장파괴 중 어떤 파괴가 발생할 것인지를 결정하는데 사용하였다. 외부주면의 전단응력과 관계없이 높은 내부 전단응력을 얻은 경우 수치해석 내에서 활동파괴가 발생하는 경우가 많았으며, 이는 전통적인 지지력 공식으로부터 얻은 예측과 잘 맞았다.

• Steel and Composite Structures
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• 제35권2호
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• pp.261-278
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• 2020

In steel-concrete composite beams, to improve the cracking resistance of the concrete slab in the hogging moment region, a new type of connector in the interface, named uplift-restricted and slip-permitted screw-type (URSP-S) connector has been proposed. This paper focuses on the behavior of steel-concrete composite beams with URSP-S connectors. A total of three beam specimens including a simply supported beam with URSP-S connectors and two continuous composite beams with different connectors arrangements were designed and tested. More specifically, one continuous composite beam was equipped with URSP-S connectors in negative moment region and traditional shear studs in other regions. For comparison, the other one was designed with only traditional shear studs. The failure modes, crack evolution process, ultimate capacities, strain responses at different locations as well as the interface slip of the three tested specimens were measured and evaluated in-depth. Based on the experimental study, the research findings indicate that the larger slip deformation is allowed while using URSP-S connectors. Meanwhile, the tensile stress reduces and the cracking resistance of the concrete slab improves accordingly. In addition, the overall stiffness and strength of the composite beam become slightly lower than those of the composite beam using traditional shear studs. Moreover, the arrangement suggestion of URSP-S connectors in the composite beam is discussed in this paper for its practical design and application.

• Steel and Composite Structures
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• 제36권1호
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• pp.1-16
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• 2020

In steel-concrete composite beams, to improve the cracking resistance of the concrete slab in the hogging moment region, a new type of connector in the interface, named uplift-restricted and slip-permitted screw-type (URSP-S) connector has been proposed. This paper focuses on the behavior of steel-concrete composite beams with URSP-S connectors. A total of three beam specimens including a simply supported beam with URSP-S connectors and two continuous composite beams with different connectors arrangements were designed and tested. More specifically, one continuous composite beam was equipped with URSP-S connectors in negative moment region and traditional shear studs in other regions. For comparison, the other one was designed with only traditional shear studs. The failure modes, crack evolution process, ultimate capacities, strain responses at different locations as well as the interface slip of the three tested specimens were measured and evaluated in-depth. Based on the experimental study, the research findings indicate that the larger slip deformation is allowed while using URSP-S connectors. Meanwhile, the tensile stress reduces and the cracking resistance of the concrete slab improves accordingly. In addition, the overall stiffness and strength of the composite beam become slightly lower than those of the composite beam using traditional shear studs. Moreover, the arrangement suggestion of URSP-S connectors in the composite beam is discussed in this paper for its practical design and application.