• Title/Summary/Keyword: TraceBack

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Ultra-trace Arsenic Determination in Urine and Whole Blood Samples by Flow Injection-Hydride Generation Atomic Absorption Spectrometry after Preconcentration and Speciation Based on Dispersive Liquid-Liquid Microextraction

  • Shirkhanloo, Hamid;Rouhollahi, Ahmad;Mousavi, Hassan Zavvar
    • Bulletin of the Korean Chemical Society
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    • v.32 no.11
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    • pp.3923-3927
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    • 2011
  • A noble method for pre-concentration and speciation of ultra trace As (III) and As (V) in urine and whole blood samples based on dispersive liquid-liquid microextraction (DLLME) has been developed. In this method, As (III) was complexed with ammonium pyrrolidine dithiocarbamate at pH = 4 and Then, As (III) was extracted into the ionic liquid (IL). Finally, As (III) was back-extracted from the IL with hydrochloric acid (HCl) and its concentration was determined by flow injection coupled with hydride generation atomic absorption spectrometry (FI-HGAAS). Total amount of arsenic was determined by reducing As (V) to As (III) with potassium iodide (KI) and ascorbic acid in HCl solution and then, As (V) was calculated by the subtracting the total arsenic and As (III) content. Under the optimum conditions, for 5-15 mL of blood and urine samples, the detection limit ($3{\sigma}$) and linear range were achieved 5 ng $L^{-1}$ and 0.02-10 ${\mu}g\;L^{-1}$, respectively. The method was applied successfully to the speciation and determination of As (III) and As (V) in biological samples of multiple sclerosis patients with suitable precision results (RSD < 5%). Validation of the methodology was performed by the standard reference material (CRM).

A Study on the Partial Discharge Pattern Recognition by Use of SOM Algorithm (SOM 알고리즘을 이용한 부분방전 패턴인식에 대한 연구)

  • Kim Jeong-Tae;Lee Ho-Keun;Lim Yoon Seok;Kim Ji-Hong;Koo Ja-Yoon
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.53 no.10
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    • pp.515-522
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    • 2004
  • In this study, we tried to investigate that the advantages of SOM(Self Organizing Map) algorithm such as data accumulation ability and the degradation trend trace ability would be adaptable to the analysis of partial discharge pattern recognition. For the purpose, we analyzed partial discharge data obtained from the typical artificial defects in GIS and XLPE power cable system through SOM algorithm. As a result, partial discharge pattern recognition could be well carried out with an acceptable error by use of Kohonen map in SOM algorithm. Also, it was clarified that the additional data could be accumulated during the operation of the algorithm. Especially, we found out that the data accumulation ability of Kohonen map could make it possible to suggest new patterns, which is impossible through the conventional BP(Back Propagation) algorithm. In addition, it is confirmed that the degradation trend could be easily traced in accordance with the degradation process. Therefore, it is expected to improve on-site applicability and to trace real-time degradation trends using SOM algorithm in the partial discharge pattern recognition

The Morphology and Crystallography of Isothermal Martensite in Yttria Stabilized Zirconia

  • Pee, Jae-Hwan;Choi, Eui-Seok;Hayakawa, Motozo
    • Journal of the Korean Ceramic Society
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    • v.43 no.2 s.285
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    • pp.69-73
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    • 2006
  • A full retention of the tetragonal phase with coarse grains $(50\~60\;{\mu}m)$ was possible with the specimen $ZrO_2-1.9\;mol\%\;Y_2O_3$. In these coarse grains, $\{101\}_t$ annealing twins were frequently observed, although they do not exist in the usual fine grained specimens. The morphology and growth rate of the isothermally formed individual products are studied at an optical microscopic level. The habit planes of both products are also identified by performing two-surface trace analysis on the grains whose orientations are determined by the Electron Back Scattering Pattern (EBSP) method. The morphologies of isothermal martensite were well-defined thin plates and lenticular types. The growth rate in their longitudinal directions was quite slow and temperature-dependent. A two-surface trace analysis, incorporated with the EBSP method, identified the habit planes near $\{013\}_c$, in agreement with previous reports obtained from TEM works.

Study on the Characteristics of Modern Hotel Interior Decorations and the Historical Meaning of Interior Design (근대 호텔 실내공간의 표현 특성과 실내디자인 사적의미에 관한 연구)

  • Oh In-Wook
    • Korean Institute of Interior Design Journal
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    • v.15 no.4 s.57
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    • pp.3-11
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    • 2006
  • The vocabulary of modern grand hotels' interior designs reflects western design patterns, showing its nostalgia for modern architecture. And it also contains the trace of past designs implanted by others then, expressing the hardships of Korean history. Like this, the past architectural style distorted under the Japanese imperialistic rule has continued to exist until now without any significant changes, because there has been little effort to figure out the history of modern interior designs. And also there has been the lack of data and aesthetic descriptions about the modern interior designs that contain the historical nature of society. Therefore, this study will review the interior design of modern buildings, which trace back to the fawning of the Korean Interior Design. And it aims to understand the hotel interior's expressive characteristics and historical meanings by paying a particular attention to its lost parts. And it also alms to have a significant meaning in taking the first step toward a clue of the history of Korean modern interiors by systematically putting in order the ever-disappearing materials of modern hotel interiors.

Vehicle Tracking System using HSV Color Space at nighttime (HSV 색 공간을 이용한 야간 차량 검출시스템)

  • Park, Ho-Sik
    • The Journal of Korea Institute of Information, Electronics, and Communication Technology
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    • v.8 no.4
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    • pp.270-274
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    • 2015
  • We suggest that HSV Color Space may be used to detect a vehicle detecting system at nighttime. It is essential that a licence plate should be extracted when a vehicle is under surveillance. To do so, a licence plate may be enlarged to certain size after the aimed vehicle is taken picture from a distance by using Pan-Tilt-Zoom Camera. Either Mean-Shift or Optical Flow Algorithm is generally used for the purpose of a vehicle detection and trace, even though those algorithms have tendency to have difficulty in detection and trace a vehicle at night. By utilizing the fact that a headlight or taillight of a vehicle stands out when an input image is converted in to HSV Color Space, we are able to achieve improvement on those algorithms for the vehicle detection and trace. In this paper, we have shown that at night, the suggested method is efficient enough to detect a vehicle 93.9% from the front and 97.7% from the back.

Studies on Solvent Extraction and Analytical Applications of Metal-Dithiocarbamate Complexes(Ⅰ). Extraction and Determination of Trace Bismuth, Cadmium and Indium in Sea Water (Dithiocarbamate 금속착물의 용매추출 및 분석적 응용(제 1 보). 해수중 흔적량 비스무트, 카드뮴, 인듐의 용매추출 및 정량)

  • Jeon, Moon Kyo;Choi, Jong Moon;Choi, Hee Seon;Kim, Young Sang
    • Journal of the Korean Chemical Society
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    • v.40 no.7
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    • pp.492-500
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    • 1996
  • The solvent extraction of trace Bi, Cd and In in seawater samples using ammonium pyrrolidine dithiocarbamate(APDC) as a complexing agent was studied. The pH of sample solution, the amount of APDC, the type of solvent and the shaking time were investigated together with back-extraction conditions. After the pH of 200 mL seawater was adjusted to 4.0 and 5.0 mL of 1% APDC was added, analytes were extracted with 10.0 mL of MIBK by shaking for 35 minutes. The organic phase seperated was washed with a 0.05 M NaOH 10.0 mL to remove HPDC. The analytes were stripped by the back-extraction of 5 minute shaking with 5 mL of 4 M HNO3 containing 150 ㎍/mL Pd(Ⅱ). Detection limits of Bi, Cd and In were 0.038, 0.0057 and 0.023 ng/mL, respectively. Both of Bi(Ⅲ) and In(Ⅲ) were not detected in two kinds of water samples of the East Sea and the contents of Cd(Ⅱ) were 0.018 and 0.016 ng/mL. The recoveries of over 90% showed that this procedure was applicable to the determination of such trace elements in seawater samples.

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A Study on the Improvement Repeatability and Accuracy of the Analysis Method for SF6 of Trace Level (극미량 수준의 SF6 측정법에 따른 재현성 및 정확도 향상에 관한 연구)

  • Yoo, Heejung;Choe, Hongwoo;Lee, Sepyo;Kim, Jongho;Han, Sangok;Ryoo, Sangboom
    • Journal of the Korean Society of Urban Environment
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    • v.18 no.4
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    • pp.523-530
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    • 2018
  • Kyoto Protocol, adopted in 1997, set the obligation to reduce $CO_2$, $CH_4$, $N_2O$, HFCs, PFCs, and $SF_6$ in developed countries during 1st promised period. $SF_6$ has been drawing a lot of attention since the Kyoto Protocol because once it is released into the atmosphere, it not only stays in the atmosphere for more than 3,200 years but also emits 22,800 times stronger global warming potential at the same concentrations as $CO_2$ if remains in the atmosphere for 100 years. This study introduces 12 methods for $SF_6$ of measuring trace. $SF_6$ of trace level in the atmosphere correctly, the measurement method was changed and as a result, when the back flush method was applied to the pre-concentration system that used low-temperature concentration and high-temperature desorption system, which used Carboxen-1000 adsorption trap, the effect was the best.

Automatic Load and Displacement Incremental Algorithm for Geometric Non-Linear Finite Element Analysis of the Structure subjected to Conservative and Non-conservative Forces (보존력(保存力) 및 비보존력(非保存力)을 받는 구조물(構造物)의 기하적(幾何的) 비선형(非線形) 유한요소해석(有限要素解析)을 위한 하중(荷重) 및 변위증분(變位增分) 알고리즘의 개발(開發))

  • Kim, Moon Young;Chang, Sung Pil
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.10 no.2
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    • pp.11-22
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    • 1990
  • An automatic incremental algorithm for geometric non-linear finite element analysis of the structures subjected to the conservative and non-conservative forces is presented. By making efficient combination of the load incremental method and the displacement incremental method, this scheme can trace various post-buckling equilibrium path such as snap-through and turning-back. Several numerical examples to demonstrate the feasibility of the present algorithm, over ranges of deformation that are well beyond those likely to occur in practical structures, are given and discussed.

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Analysis of Lower body on Korean Young Women and the Effect of the Lower body Type on the Shape of Flare Skirt (II) (한국 미혼 여성의 하반신체형 분석과 체형변인이 플레어스커트 입체성능에 미치는 영향(II))

  • 조정미
    • Journal of the Korean Home Economics Association
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    • v.30 no.3
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    • pp.15-32
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    • 1992
  • The purpose of this study was to detect the effect of the lower body type on the shape of flare skirts. The subjects for the wearing test were 50 female students, who were controlled in their hip and waist shapes. The skirts used for wearing test were six types(three flar angles $\times$ two fabric types). The effect of lower body type on the shape of flare skirts was determind by the hemline trace method and the silhouette photography. The data were then analyzed by the repeated measures of analysis of variance and the SNK multiple range test. The results obtained from this study were as follows : 1) When a flare skirt made with larger flare angle and better drapable fabric was worn, the numeric of the nodes increased as the drop value(hip - waist) increased. When a flare skirt made with smaller flare angle was worn, the width of horizontal sectio of hemline increased as the drop value increased. The hemline uneveness decreased on the sides and back as the drop value increased. When a flare skirt made with worse drapable fabric was worn, the sides angle of the flarskirt increased as the drop value increased. 2) When a flare skirt made with larger flare angle was worn, the numeric of nodes increased as the ratio of dropped hip increased. The wave-height increased and the back variation ratio of wave-height was higher than the front variation ratio of wave-height as the ratio of dropped hip increased. The hemiline uneveness decreased on the back as the ratio of dropped hip increased. When a flare skirt made with larger flare angle was worn, the sides angle of the flare skirt increased as the ratio of dropped hip increased.

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Gonadotropin-releasing hormone immunization and castration in male pigs: effects on growth, hormonal levels, antibody titer response, testicular function, back fat, and consumers' sensory perceptions

  • Yamsakul, Panuwat;Patchanee, Prapas;Yano, Terdsak;Boonma, Thanawish;Somkert, Chalermchart;Sathanawongs, Anucha
    • Korean Journal of Veterinary Research
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    • v.57 no.1
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    • pp.23-29
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    • 2017
  • This study investigated the effects of gonadotropin-releasing hormone (GnRH) vaccine on pig growth, carcass quality, and sensory perceptions of pork meat by Thai consumers. Male crossbred pigs (n = 30) were separated into three groups of 10 pigs each: boars, immunocastrated pigs, and surgically castrated pigs. The immunocastrated group was immunized at 13 and 19 weeks of age with GnRH vaccine ($400{\mu}g/dose$). All pigs were slaughtered at 24 weeks of age. Blood samples were collected and testes size determined. Testes weight and back fat thickness were recorded at the time of slaughter, and meat samples were collected for sensory assessment by Thai consumers. Testosterone and progesterone concentration levels decreased significantly two weeks after the second dose of GnRH (p < 0.05), and the GnRH antibody titer of the immunocastrated pigs was significantly high two weeks after the second dose of GnRH (p < 0.05). GnRH vaccine significantly reduced the weight and size of testes. Thai consumers reported no significant differences in odor or flavor among meat samples from the three groups. In conclusion, immunocastration improved growth performance, removed the need for castration surgery, and avoided "boar taint" in the meat. It has also no distinct trace of the boar taint same as pork that is currently produced from physically castrated pig which is making it acceptable to consumers.