• Bulletin of the Korean Chemical Society
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• 제32권11호
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• pp.3923-3927
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• 2011

A noble method for pre-concentration and speciation of ultra trace As (III) and As (V) in urine and whole blood samples based on dispersive liquid-liquid microextraction (DLLME) has been developed. In this method, As (III) was complexed with ammonium pyrrolidine dithiocarbamate at pH = 4 and Then, As (III) was extracted into the ionic liquid (IL). Finally, As (III) was back-extracted from the IL with hydrochloric acid (HCl) and its concentration was determined by flow injection coupled with hydride generation atomic absorption spectrometry (FI-HGAAS). Total amount of arsenic was determined by reducing As (V) to As (III) with potassium iodide (KI) and ascorbic acid in HCl solution and then, As (V) was calculated by the subtracting the total arsenic and As (III) content. Under the optimum conditions, for 5-15 mL of blood and urine samples, the detection limit ($3{\sigma}$) and linear range were achieved 5 ng $L^{-1}$ and 0.02-10 ${\mu}g\;L^{-1}$, respectively. The method was applied successfully to the speciation and determination of As (III) and As (V) in biological samples of multiple sclerosis patients with suitable precision results (RSD < 5%). Validation of the methodology was performed by the standard reference material (CRM).

• 대한전기학회논문지:전기물성ㆍ응용부문C
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• 제53권10호
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• pp.515-522
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• 2004

In this study, we tried to investigate that the advantages of SOM(Self Organizing Map) algorithm such as data accumulation ability and the degradation trend trace ability would be adaptable to the analysis of partial discharge pattern recognition. For the purpose, we analyzed partial discharge data obtained from the typical artificial defects in GIS and XLPE power cable system through SOM algorithm. As a result, partial discharge pattern recognition could be well carried out with an acceptable error by use of Kohonen map in SOM algorithm. Also, it was clarified that the additional data could be accumulated during the operation of the algorithm. Especially, we found out that the data accumulation ability of Kohonen map could make it possible to suggest new patterns, which is impossible through the conventional BP(Back Propagation) algorithm. In addition, it is confirmed that the degradation trend could be easily traced in accordance with the degradation process. Therefore, it is expected to improve on-site applicability and to trace real-time degradation trends using SOM algorithm in the partial discharge pattern recognition

• 한국세라믹학회지
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• 제43권2호
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• pp.69-73
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• 2006

A full retention of the tetragonal phase with coarse grains $(50\~60\;{\mu}m)$ was possible with the specimen $ZrO_2-1.9\;mol\%\;Y_2O_3$. In these coarse grains, $\{101\}_t$ annealing twins were frequently observed, although they do not exist in the usual fine grained specimens. The morphology and growth rate of the isothermally formed individual products are studied at an optical microscopic level. The habit planes of both products are also identified by performing two-surface trace analysis on the grains whose orientations are determined by the Electron Back Scattering Pattern (EBSP) method. The morphologies of isothermal martensite were well-defined thin plates and lenticular types. The growth rate in their longitudinal directions was quite slow and temperature-dependent. A two-surface trace analysis, incorporated with the EBSP method, identified the habit planes near $\{013\}_c$, in agreement with previous reports obtained from TEM works.

• 한국실내디자인학회논문집
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• 제15권4호
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• pp.3-11
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• 2006

The vocabulary of modern grand hotels' interior designs reflects western design patterns, showing its nostalgia for modern architecture. And it also contains the trace of past designs implanted by others then, expressing the hardships of Korean history. Like this, the past architectural style distorted under the Japanese imperialistic rule has continued to exist until now without any significant changes, because there has been little effort to figure out the history of modern interior designs. And also there has been the lack of data and aesthetic descriptions about the modern interior designs that contain the historical nature of society. Therefore, this study will review the interior design of modern buildings, which trace back to the fawning of the Korean Interior Design. And it aims to understand the hotel interior's expressive characteristics and historical meanings by paying a particular attention to its lost parts. And it also alms to have a significant meaning in taking the first step toward a clue of the history of Korean modern interiors by systematically putting in order the ever-disappearing materials of modern hotel interiors.

• 한국정보전자통신기술학회논문지
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• 제8권4호
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• pp.270-274
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• 2015

본 논문에서는 HSV 색 공간을 이용한 야간 차량의 검출 시스템을 제안한다. 주정차 감시등 도로변에서 자동차를 감시하는 경우 자동차 번호판 추출하는 것이 중요하다. 일반적으로 번호판 추출을 위해서는 원거리에서 자동차 검출후 Pan-Tilt-Zoom 카메라로 자동차를 일정한 크기로 확대한 영상을 획득하여 번호판을 추출한다. 그리고 자동차 검출 및 추적을 위해 Mean-Shift 혹은 Optical Flow 알고리듬이 많이 이용되고 있다. 그러나 이러한 알고리즘은 주간에는 성공적으로 자동차를 검출 및 추적 할수 있었으나 야간에는 검출 및 추적에 어려움이 있었다. 그래서 본 논문에서는 입력 영상을 HSV 색 공간으로 변환하면 자동차의 전조등 혹은 후미등의 위치가 두드러지게 나타나는 것을 이용하여 자동차의 위치를 검출하였다. 실험 결과 정면 차량의 경우 93.9%, 후면 차량의 경우 97.7%의 차량을 검출하여 제안된 방법이 야간 차량 검출에 효율적임을 증명하였다.

• 대한화학회지
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• 제40권7호
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• pp.492-500
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• 1996

Ammonium pyrrolidine dithiocarbamate(APDC)를 착화제로 사용하여 해수중 흔적량 비스무트, 카드뮴, 인듐을 동시에 용매추출하여 정량하는 방법을 연구하였다. 최적조건을 찾기위하여, 시료용액의 pH, 착화제의 양, 흔들어주는 시간, 유기용매의 종류 등에 대하여 조사하였고 역추출효율도 검토하였다. 해수시료 200mL를 취하여, pH를 4.0으로 조정하고 1% APDC 5.0mL를 첨가하고, MIBK 10.0mL로 35분 동안 흔들어 추출한다. 그리고 0.05M 수산화나트륨용액 10mL로 유기층의 HPDC를 세척한다. 유기층을 150.mu.g/mL Pd(II)를 포함하는 4M 질산으로 5분동안 흔들어 분석원소를 역추출한다. 팔라윰이 포함된 4M질산은 역추출효율을 증가시키고 흡광도 측정에서 매트릭스를 개선하여 감도를 증가시켰다. 바탕 흡광도에 대한 표준편차의 3배에 해당하는 농도로서의 검출한계는 Bi(III) :0.038, Cd(II) : 0.0057, In(III) : 0.023 ng/mL이었다. 동해 시료2 가지를 취하여 본방법으로 정량한 결과 Bi(III), In(III)은 검출한계 이하였고, Cd(II)는 0.018과 0.016 ng/mL이었다. 해수시료에 일정량 원소를 가해서 구한 회수율은 모두 90% 이상으로 아칼리금속 매트릭스에서 흔적량 원소의 동시분석에 이 방법이 응용될수 있음을 알 수 있었다.

• 한국도시환경학회지
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• 제18권4호
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• pp.523-530
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• 2018

오존층의 파괴물질인 CFCs의 대체물로써 $SF_6$의 사용량이 늘어나면서 대기 중의 $SF_6$의 농도가 높아지고 있다. $SF_6$은 지구온난화가스중의 하나로써 대기 중에서 3,200년 이상 머무를 뿐만 아니라 온난화지수도 매우 높아 무려 22,800이나 된다. 그러나, 대기 중에서의 $SF_6$ 농도는 낮은 수준이어서 검출한계이하인 경우가 많다. 본 연구에서는 이러한 극미량 $SF_6$ 농도를 정확하게 분석하기 위해서 $GC-{\mu}ECD$를 이용한 12가지 분석방법을 실험적으로 고찰하였다. 극미량 $SF_6$ 농도를 가장 정확하게 분석할 수 있는 방법은 Carboxen-1000 물질을 사용한 흡착관과 저온농축 고온탈착 방식의 농축장치에 역추출방식의 분석법을 사용할 경우가 최상의 효율을 나타냈다.

• 대한토목학회논문집
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• 제10권2호
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• pp.11-22
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• 1990

본(本) 논문(論文)에서는 보존력(保存力) 및 비보존력(非保存力)을 받는 구조물(構造物)의 비선형(非線形) 유한요소해석(有限要素解析)을 수행(遂行)하기 위하여 기존의 하중증분법(荷重增分法)과 변위증분법(變位增分法)을 효율적(效率的)으로 결합(結合)시킨 수치적(數値的)인 해석(解析)알고리즘을 제시(提示)하였다. 제안(提案)한 알고리즘은 하중증분(荷重增分)과 변위증분(變位增分)이 자동(自動) 생성되도록 하므로써 Snap-Through, Turning-Back과 같은 비선형(非線形) 거동(擧動)을 포함(包含)하는 다양(多樣)한 평형경로(平衡經路)들을 추적(追跡)할 수 있었다.

• 대한가정학회지
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• 제30권3호
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• pp.15-32
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• 1992

The purpose of this study was to detect the effect of the lower body type on the shape of flare skirts. The subjects for the wearing test were 50 female students, who were controlled in their hip and waist shapes. The skirts used for wearing test were six types(three flar angles $\times$ two fabric types). The effect of lower body type on the shape of flare skirts was determind by the hemline trace method and the silhouette photography. The data were then analyzed by the repeated measures of analysis of variance and the SNK multiple range test. The results obtained from this study were as follows : 1) When a flare skirt made with larger flare angle and better drapable fabric was worn, the numeric of the nodes increased as the drop value(hip - waist) increased. When a flare skirt made with smaller flare angle was worn, the width of horizontal sectio of hemline increased as the drop value increased. The hemline uneveness decreased on the sides and back as the drop value increased. When a flare skirt made with worse drapable fabric was worn, the sides angle of the flarskirt increased as the drop value increased. 2) When a flare skirt made with larger flare angle was worn, the numeric of nodes increased as the ratio of dropped hip increased. The wave-height increased and the back variation ratio of wave-height was higher than the front variation ratio of wave-height as the ratio of dropped hip increased. The hemiline uneveness decreased on the back as the ratio of dropped hip increased. When a flare skirt made with larger flare angle was worn, the sides angle of the flare skirt increased as the ratio of dropped hip increased.

• 대한수의학회지
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• 제57권1호
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• pp.23-29
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• 2017

This study investigated the effects of gonadotropin-releasing hormone (GnRH) vaccine on pig growth, carcass quality, and sensory perceptions of pork meat by Thai consumers. Male crossbred pigs (n = 30) were separated into three groups of 10 pigs each: boars, immunocastrated pigs, and surgically castrated pigs. The immunocastrated group was immunized at 13 and 19 weeks of age with GnRH vaccine ($400{\mu}g/dose$). All pigs were slaughtered at 24 weeks of age. Blood samples were collected and testes size determined. Testes weight and back fat thickness were recorded at the time of slaughter, and meat samples were collected for sensory assessment by Thai consumers. Testosterone and progesterone concentration levels decreased significantly two weeks after the second dose of GnRH (p < 0.05), and the GnRH antibody titer of the immunocastrated pigs was significantly high two weeks after the second dose of GnRH (p < 0.05). GnRH vaccine significantly reduced the weight and size of testes. Thai consumers reported no significant differences in odor or flavor among meat samples from the three groups. In conclusion, immunocastration improved growth performance, removed the need for castration surgery, and avoided "boar taint" in the meat. It has also no distinct trace of the boar taint same as pork that is currently produced from physically castrated pig which is making it acceptable to consumers.