• Korean Journal of Materials Research
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• v.23 no.9
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• pp.489-494
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• 2013

In this study, by using nickel chloride solution as a raw material, a nano-sized nickel oxide powder with an average particle size below 50 nm was produced by spray pyrolysis reaction. A spray pyrolysis system was specially designed and built for this study. The influence of nozzle tip size on the properties of the produced powder was examined. When the nozzle tip size was 1 mm, the particle size distribution was more uniform than when other nozzle tip sizes were used and the average particle size of the powder was about 15 nm. When the nozzle tip size increases to 2 mm, the average particle size increases to roughly 20 nm, and the particle size distribution becomes more uneven. When the tip size increases to 3 mm, particles with an average size of 25 nm and equal to or less than 10 nm coexist and the particle size distribution becomes much more uneven. When the tip size increases to 5 mm, large particles with average size of 50 nm partially exist, mostly consisting of minute particles with average sizes in the range of 15~25 nm. When the tip size increases from 1 mm to 2 mm, the XRD peak intensities greatly increase while the specific surface area decreases. When the tip size increases to 3 mm, the XRD peak intensities decrease while the specific surface area increases. When the tip size increases to 5 mm, the XRD peak intensities increase again while the specific surface area decreases.

• Korean Journal of Materials Research
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• v.23 no.2
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• pp.81-88
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• 2013

In this study, using a tin chloride solution as the raw material, a nano-sized tin oxide powder with an average particle size below 50 nm is generated by a spray pyrolysis process. The properties of the tin oxide powder according to the nozzle tip size are examined. Along with an increase in the nozzle tip size from 1 mm to 5 mm, the generated particles that appear in the shape of droplets maintain an average particle size of 30 nm. When the nozzle tip size increases from 1 mm to 2 mm, the average size of the generated particles is around 80-100 nm, and the ratio of the independent particles with a compact surface structure increases significantly. When the nozzle tip size is at 3 mm, the majority of the generated particles maintain the droplet shape, the average size of the droplet-shaped particles increases remarkably compared to the cases of other nozzle tip sizes, and the particle size distribution also becomes extremely irregular. When the nozzle tip size is at 5 mm, the ratio of droplet-shaped particles decreases significantly and most of the generated particles are independent ones with incompact surface structures. Along with an increase in the nozzle tip size from 1 mm to 3 mm, the XRD peak intensity increases, whereas the specific surface area decreases greatly. When the nozzle tip size increases up to 5 mm, the XRD peak intensity decreases significantly, while the specific surface area increases remarkably.

• Resources Recycling
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• v.25 no.6
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• pp.41-49
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• 2016

The present study was intended to prepare cobalt oxide ($Co_3O_4$) powder of average particle size 50 nm or less by spray pyrolysis reaction using the raw cobalt chloride ($CoCl_2$) solution, in order to identify the change in the nature of the particles according to the change in the nozzle tip size. When the nozzle tip was 1 mm, it turned out that most of the droplets were spherical and the surface showed very tight structure. The average particle size of the finally formed particles was 20-30 nm. When the nozzle tip size was 2 mm, some of the droplets formed were spherical, but a considerable part of them showed severely disrupted form. particles formed showed an average particle size of 30 - 40 nm. For the nozzle tip size of 5 mm, spherical droplets were almost non-existent and most were in badly fragmented state. The tightness of surface structure of the droplets has greatly been reduced compared with other nozzle tip sizes. Average size of the formed particles was about 25 nm. As the nozzle tip size increased from 1 mm to 2 mm and 3 mm, the intensities of the XRD peaks have changed little, but significantly been reduced when the nozzle tip size increased to 5mm. As the nozzle tip size increased from 1 mm to 2 mm, the specific surface area of the particles decreased, but the nozzle tip size increased to 5mm, the specific surface area remarkably increased.

• Journal of Powder Materials
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• v.10 no.4
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• pp.262-269
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• 2003

Nano-sized Ni-ferrite powder was fabricated by spray pyrolysis process using the waste solution resulting from shadow mask processing. The average particle size of the powder was below 100 nm. The effects of the concentration of raw material solution, the nozzle tip size and air pressure on the properties of powder were studied. As the concentration increased, the average particle size of the powder gradually increased and its specific surface area decreased, but size distribution was much wider and the fraction of the Ni-ferrite phase greatly increased as the concentration increasing. As the nozzle tip size increased from 1 mm to 2 mm, the average particle size of the powder decreased. In case of 3 mm nozzle tip size, the average particle size of the powder increased slightly. On the other hand, in case of 5 mm nozzle tip size, average particle size of the powder decreased. Size distribution of the powder was unhomogeneous, and the fraction of the Ni-ferrite phase decreased as the nozzle tip size increasing. As air pressure increased up to 1 kg/$cm^2$, the average particle size of the powder decreased slightly, on the other hand, the fraction of the Ni-ferrite phase was almost constant. In case of 3kg/$cm^2$ air pressure, average particle size of the powder and the fraction of the Ni-ferrite phase remarkably decreased, but size distribution was narrow.

• Computers and Concrete
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• v.17 no.1
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• pp.107-127
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• 2016

Concrete is a heterogeneous material containing many weaknesses such as micro-cracks, pores and grain boundaries. The crack growth mechanism and failure behavior of concrete structures depend on the plastic deformation created by these weaknesses. In this article the non-linear finite element method is used to analyze the effect of presence of micro pore near a crack tip on both of the characteristics of crack tip plastic zone (its shape and size) and crack growth properties (such as crack growth length and crack initiation angle) under pure shear loading. The FE Code Franc2D/L is used to carry out these objectives. The effects of the crack-pore configurations and the spacing between micro pore and pre-excising crack tip on the characteristics of crack tip plastic zone and crack growth properties is highlighted. Based on the obtained results, the relative distance between the crack tip and the micro pore affects in very significant way the shape and the size of the crack tip plastic zone. Furthermore, crack growth length and crack initiation angle are mostly influenced by size and shape of plastic zone ahead of crack tip. Also the effects of pore decrease on the crack tip by variation of pore situation from linear to perpendicular configuration. The critical position for a micro pore is in front of the crack tip.

• International Journal of Naval Architecture and Ocean Engineering
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• v.8 no.3
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• pp.219-227
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• 2016

Numerical simulation based on the Reynolds Averaged Naviere-Stokes (RANS) Computational Fluid Dynamics (CFD) method had been carried out with the commercial code ANSYS CFX. The structured grid and SST $k-{\omega}$ turbulence model had been adopted. The impact of non-condensable gas (NCG) on cavitation performance had been introduced into the Schnerr and Sauer cavitation model. The numerical investigation of cavitating flow of marine propeller E779A was carried out with different advance ratios and cavitation numbers to verify the numerical simulation method. Tip clearance effects on the performance of pumpjet propulsor had been investigated. Results showed that the structure and characteristics of the tip leakage vortex and the efficiency of the propulsor dropped more sharply with the increase of the tip clearance size. Furthermore, the numerical simulation of tip clearance cavitation of pumpjet propulsor had been presented with different rotational speed and tip clearance size. The mechanism of tip clearance cavitation causing a further loss of the efficiency had been studied. The influence of rotational speed and tip clearance size on tip clearance cavitation had been investigated.

• 유체기계공업학회:학술대회논문집
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• 1998.12a
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• pp.240-247
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• 1998

Leakage vortices formed near blade tip causes an increase of total pressure loss near casing endwall region and as a result, the efficiency of rotor decreases. The reduction of rotor efficiency is related to the size of tip clearance. In this study, the three-dimensional flowfields in an axial flow rotor were calculated with varying tip clearance under various flow rates, and the numerical results were compared with experimental ones. The effects of tip clearance and attack angle on the leakage vortex and overall performance, and the less distributions were investigated through numerical calculations. In this study, tip leakage flow rate and total pressure loss by tip clearance were evaluated using numerical results and aprroximate equations were presented to evaluate the reduction of rotor efficiency by tip leakage flow.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.30 no.11 s.254
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• pp.1455-1460
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• 2006

The relationship between fatigue crack growth behavior and cyclic crack tip opening displacement is studied. An elastic-plastic finite element analysis (FEA) is performed to examine the growth behavior of fatigue crack, where the contact elements are used in the mesh of the crack tip area. We investigate the relationship between the reversed plastic zone size and the changes of the cyclic crack tip opening displacement along the crack growth. We investigate the effect of the element size when predict fatigue crack opening behavior using the cyclic crack tip opening displacement obtained from FEA. The cyclic crack tip opening displacement is related to fatigue crack opening behavior.

• The KSFM Journal of Fluid Machinery
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• v.2 no.1 s.2
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• pp.73-80
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• 1999

Leakage vortices formed new blade tip causes an increase of total pressure loss near the casing endwall region and as a result, the efficiency of rotor decreases. The reduction of rotor efficiency is related to the size of the tip clearance. In this study, the three-dimensional flowfields in an axial flow rotor were calculated by varying the tip clearance under various flow rates, and the numerical results were compared with experimental ones. The effects of tip clearance and attack angle on the leakage vortex and overall performance, and the loss distributions were investigated through numerical calculations. In this study, tip leakage flow rate and total pressure loss by tip clearance were evaluated using numerical results and approximate equations were presented to evaluate the reduction of rotor efficiency by tip leakage flow.

• International Journal of Naval Architecture and Ocean Engineering
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• v.10 no.3
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• pp.307-317
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• 2018

In this study, numerical investigations of the tip clearance flow characteristics of a pumpjet propulsor based on Computational Fluid Dynamics (CFD) method have been presented. The Zwart-Gerber-Belamri (Z-G-B) cavitation model based on Reynolds Averaged Navier-Stokes (RANS) method is employed. The structured gird is applied. The formation and development of the tip clearance flows has been investigated and presented. The structure of the tip leakage vortex has been shown. The radial distributions of different velocity components with different Span along the axial direction have been carried out to present the influence of the tip clearance flow on the main flow. In addition, the influences of the tip clearance size on the pumpjet propulsor performance, including the impact on the velocity flow fields and the cavitation characteristic, have been presented.