• Geomechanics and Engineering
• /
• v.17 no.6
• /
• pp.527-534
• /
• 2019

There have been developed a number of methods to assess the abrasivity of rock materials with the increased use of mechanized rock excavation. These methods range from determination of abrasive and hard mineral content using petrographic thin section analysis to weight loss or development of wear flat on a specified cutting tool. The Cerchar abrasivity index (CAI) test has been widely accepted for the assessment of rock abrasiveness. This test has been considered to provide a reliable indication of rock abrasiveness for isotropic rocks. However, a great amount of rocks in nature are anisotropic. Hence, viability assessment of Cerchar abrasivity test for the anisotropic rocks is investigated in this research. The relationship between CAI value and quartz content for the isotropic rocks is well known in literature. However, a correlation between EQ, F-Schimazek value, Rock Abrasivity Index (RAI) and CAI of anisotropic rocks such as phyllite was done first time in literature with this research. The results obtained with this research show F-Schimazek values and RAI values should be considered when determination of the abrasivity of anisotropic rocks instead of just using Cerchar scratch test.

• Bulletin of the Korean Chemical Society
• /
• v.22 no.2
• /
• pp.205-209
• /
• 2001

Uniformly-doped silicon thin films were fabricated by ion beam sputter deposition. The thin films had four levels of copper dopant concentration ranging between 1 ${\times}$1019 and 1 ${\times}$ 1021 atoms/cm3 . Concentrations of Copper dopants were determined by the isotope dilution inductively coupled plasma mass spectrometry (ICP-MS) to provide certified reference data for the quantitative surface analysis by secondary ion mass spectrometry (SIMS). The copper-doped thin films were dissolved in a mixture of 1 M HF and 3 M HNO3 spiked with appropriate amounts of 65 Cu. For an accurate isotope ratio determination, both the detector dead time and the mass discrimination were appropriately corrected and isobaric interference from SiAr molecular ions was avoided by a careful sample pretreatment. An analyte recovery efficiency was obtained for the Cu spiked samples to evaluate accuracy of the method. Uncertainty of the determined copper concentrations, estimated following the EURACHEM Guide, was less than 4%, and detection limit of this method was 5.58 ${\times}$ 1016 atoms/cm3.

• Bulletin of the Korean Chemical Society
• /
• v.17 no.4
• /
• pp.342-347
• /
• 1996

Voltammetric determination of phenol derivatives, such as phenol, o-, m-, and p-cresols was studied with a β-Cyclodextrin (β-CD) modified-carbon paste electrode composing of the graphite powder and Nujol oil. Phenol derivatives were chemically deposited via the complex formation with β-CD by immersing the CME into a sample solution. The resulting surfaces were characterized with cyclic and differential pulse voltammetry. Treating the CME with 1 M nitric acid for five sec after a measurement could regenerate the electrode surface. Linear sweep and differential pulse voltammograms were recorded for the above system to optimize the experimental parameters for analysing the phenol derivatives. In this case, the detection limit for phenols was 5.0×10-7M for 25 min of the deposition time with differential pulse voltammetry. The relative standard deviation was ±5.2% of 3.0×10-6M (four repetitions). The interference effect of the following organic compounds was also investigated; Bezoic acid, hippuric acid, o-, m-, and p-methylhippuric acid. Adding the organic compounds into the sample solution reduces the peak current of the phenols to about 25%.

• International conference on construction engineering and project management
• /
• 2015.10a
• /
• pp.618-619
• /
• 2015

The costs due to the maintenance and its method of national road have increased every year, and the maintenance costs have become higher due to the maintenance method without considering the characteristics of each region. This study is a preliminary study regarding the determination of maintenance method according to the characteristics of each region by applying variables (e.g. serviced time, traffic volume, average temperature, maximum temperature, minimum temperature, rainfall, and snowfall) to decide the maintenance and its method through the correlation analysis of road maintenance and repair period for each regional agency using the maintenance history data of national road management agency.

• International conference on construction engineering and project management
• /
• 2011.02a
• /
• pp.376-381
• /
• 2011

In Korea Water Resources Corporation (K-Water) has seen four problems rising in four aspects of property management of approximately 1,300 buildings scattered through put to country. To solve these, ground data for repair and replacement works to be conducted for prevention will be prepared and building maintenance system (hereinafter referred to as PBMS) intended to record related repair and replacement work histories and calculate LCC of the related these items will be developed. PBMS, a web-based system, will be developed for users' convenience and data monitoring in real time. To sum up, PBMS are expected to maximize efficiency in four aspects including the establishment of repair and replacement work plans for prevention, history management, DB for predicting future work to be occurred and enable the determination of priorities by being developing into facility condition assessment systems through the results of analysis of repair and replacement histories and LCC.

• ETRI Journal
• /
• v.46 no.3
• /
• pp.421-431
• /
• 2024

In this study, a direct position tracking method for non-circular (NC) signals using distributed passive arrays is proposed. First, we calculate the initial positions of sources using a direct position determination (DPD) approach; next, we transform the tracking into a compensation problem. The offsets of the adjacent time positions are calculated using a first-order Taylor expansion. The fusion calculation of the noise subspace is performed according to the NC characteristics. Because the proposed method uses the signal information from the previous iteration, it can realize automatic data associations. Compared with traditional DPD and two-step localization methods, our novel process has lower computational complexity and provides higher accuracy. Moreover, its performance is better than that of the traditional tracking methods. Numerous simulation results support the superiority of our proposed method.

• Biomolecules & Therapeutics
• /
• v.15 no.2
• /
• pp.123-126
• /
• 2007

A sensitive, simple and highly selective liquid chromatography method of determination for extraction of pseudoephedrine hydrochloride from Allegra D tablet was developed. The chief benefit of the present method is the minimal sample preparation, as the procedure is only filtering through pore syringe filter. Two drugs (pseudoephedrine hydrochloride, fexofenadine) were separated on a C$_{18}$ column and analyzed by high performance liquid chromatography (HPLC). The method had a chromatographic run time of 8.0 min. 1 ml of pseudoephedrine hydrochloride solution (1 mg/ml) was filtered through 0.22 um pore syringe filter. 50 ul of filtering solution was injected to HPLC pump and we knew the retention time (1.85 min) of separating of pseudoephedrine hydrochloride using UV detector at 280 nm. We used C$_{18}$ column (4.6 mm${\times}$250 mm), mobile phase solution (<0.05 mol/L NaH$_2$PO$_4$, 2 ml/L H$_3$PO$_4$>/CH$_3$CN / sodium dodesyl sulfate = 60 ml / 40 ml / 1 g). We separated psedoephedrine hydrochloride at run time of 1.85 min from Allegra D tablet solution (1 mg/ml) filtered through 0.22 um pore syringe filter using UV detector at 280 nm. Flow rate was set at 1.0 ml/min and the column temperature was set at 40$^{\circ}C$. Psedoephedrine hydrochloride solution (1 mg/ml) separated from Allegra D tablet was filtered through 0.22 um pore syringe filter and injected 50 ul. We confirmed the peak of psedoephedrine hydrochloride at same retention time and the separating solution was freeze-dried. In conclusion, A simple isocratic reverse-phase HPLC method has been developed that provides excellent separation of pseudoephedrine from Allegra D tablet.

• Journal of the Korean Chemical Society
• /
• v.22 no.5
• /
• pp.340-355
• /
• 1978

Model reactions were often applied in the measuring of the mass transfer coefficient and interfacial area between gas and liquid, which are the most important factors in the design of equipment for gas absorption accompanied with chemical reaction this study, wetted wall column was applied to the sulfite-system among the known model reactions. It was found that one could not ignore the effect of contact time on the determination of mass transfer coefficient and interfacial area. When the reaction rate is very high or very low, the differences of absorption rate would be very large in according to the length of column, that is to the contact time. But the effect of contact time was free about the rate constant $k_2=5.5{\times}10^6m^3/kmol{\cdot}s$, that means the rate of gas absorption become independent upon the hydrodynamics of the equipment. It has shown that instead of steel column could be applied the fine grain-graphite column.

• Journal of Navigation and Port Research
• /
• v.32 no.3
• /
• pp.207-213
• /
• 2008

Ship-handling simulation system has been used for maritime traffic safety assessment for harbor and fairway. There exist various environmental conditions under which ship may navigate along a fairway or in harbor. Due to the time and budget limitations, however, ship-handling simulations are usually carried out for very limited number of environmental conditions. In this paper, statistical method for effective and systematic determination of real time simulation conditions is suggested and applied to the maritime traffic safety assessment problems. In the empirical study, the principal component analysis method and the concept of empirical cumulative distribution function are suggested to estimate synthetic navigational difficulty and to select simulation conditions which would impose high difficulty on shiphandling.

• The KIPS Transactions:PartD
• /
• v.10D no.1
• /
• pp.45-56
• /
• 2003

In the wireless environment, according to the development of technology, which is able to obtain location information of spatiotemporal moving object, the various application systems are developed such as vehicle tracking system, forest fire management system and digital battle field system. These application systems need the data model, which is able to represent and process the continuous change of moving object. However, if moving objects are expressed by a relational model, there is a problem which is not able to store all location information that changed per every time. Also, existing data models of moving object have a week point, which constrain the query time to the time that is managed in the database such as past or current and near future. Therefore, in this paper, we propose a data model, which is able to not only express the continuous movement of moving point and moving region but also process the operation at all query time by using shape-change process and location determination functions for past and future. In addition, we apply the proposed model to forest fire management system and evaluate the validity through the implementation result.