• Title/Summary/Keyword: Thin Layer Chromatography

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Screening Test on the Constituents from the Stems of the Genus Thalictrum in Korea (국산 Thalictrum 속 식물 지상부의 성분검색)

  • Lee, In-Ran
    • Korean Journal of Pharmacognosy
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    • v.3 no.1
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    • pp.23-25
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    • 1972
  • Preliminary investigations were carried out to isolate the constituents from the stems of genus Thalictrum. Methanol extracts of eight species from the genus were examined by thin layer chromatography. The author observed three different spots with Dragendorff's reagent in Thalictrum actaefolium, whereas none was detected in Thalictrum tuberiferum and Thalictrum simplex. Various fluorescent colors with different Rf values were detected in all species by UV ray, suggesting that each species may have different components.

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A Study on the Microdetermination of Nicotine in Contaminated Beverage by Thin-Layer Chromatography (커피음료중(飮料中)에 위화(僞和)된 Nicotine의 미량분석(微量分析)에 관(關)한 연구(硏究))

  • Lee, Duk-Heng;Lee, Yong-Joo
    • Korean Journal of Pharmacognosy
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    • v.10 no.1
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    • pp.23-25
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    • 1979
  • A trace amount of nicotine, main constituent in tobacco, contaminated in coffee, was identified by the T.L.C method. The Eastman chromagram plate was used and determined with the linear scanning by transmission method. It was possible to identify nicotine in coffee beverage regardless of types of tobacco. Ten micrograms of nicotine could be determined in a cup of coffee (75ml), which was acidified with hydrochloric acid.

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Analytical Method of additive in Polyester (I) (폴리에스테르의 첨가제 분석법(I))

  • Jung, Jong Hwa;Lee, Kyeong Hee
    • Analytical Science and Technology
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    • v.12 no.1
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    • pp.84-88
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    • 1999
  • A method to analyze additives in a polyester resin has been studied by utilizing a centrifuge and a thin layer chromatography. Identification of the separated organic and inorganic compounds were carried out by spectrophotometers, such as NMR, UV-VIS, IR and XRD. For the polyester resin studied in this research contained organic and inorganic compounds which were found to be a dimer form of 2-phenylbenzoazole and an anatase form of $TiO_2$, respectively.

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Isolation of Solanesol from Korean Native Tobacco (한국산 재래종 잎담배중의 Solanesol의 분리)

  • Park, Oee-Sook
    • Korean Journal of Pharmacognosy
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    • v.12 no.4
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    • pp.211-214
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    • 1981
  • Solanesol has been isolated from aged Korean native tobacco leaf(Hyangcho and Sohyang) by water pretreatment, hexane extraction and column chromatography on Florisil in yields of 0.41% and 0.31% dry wt., respectively. Thin-layer densitometric analysis of the hexane extracts of samples(Hyangcho Sohyang) has shown that the amounts of solanesol present are 0.74% and 0.52% dry wt., respectively.

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Studies on the Flavonoid Constituents of Leaves of Lespedeza maximowiczii(I) (Lespedeza maximowiczii엽(葉)의 풀라보노이드 성분(成分) 연구(硏究)(I))

  • Han, Seong-Sun
    • Korean Journal of Pharmacognosy
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    • v.7 no.3
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    • pp.209-210
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    • 1976
  • To identify eriodictyol from the leaves of Lespedeza maximowiczii C.K. $S_{CHNEIDER}$, growing in Korea, the fresh leaves collected at Mt. Chil Bo, Geong Gi Province were used in the investigation. A white crystal was isolated from the water extract and it was identified as eriodictyol by its melting point, physico-chemical properties, thin layer chromatography and infrared absorption spectrum patterns.

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Studies on the Lipid Classes of Nicotiana tabacum L. Seed Oil

  • Waheed, Amran;Mahmud, Shahid;Javed, Muhammad Akhtar;Saleem, Muhammad
    • Natural Product Sciences
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    • v.7 no.4
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    • pp.110-113
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    • 2001
  • The lipid classes constituents; hydrocarbons, wax esters, sterol esters, triacylglycerols, free fatty acids, 1,3-diacylglycerols, 1,2-diacylglycerols, free sterols, 2-monoacylglycerols, 1-monoacylglycerols, phosphatidylethanolamines, phosphatidylcholines, lysophosphatidylethanolamines and phosphatidylinositols of Nicotiana tabacum L. seeds oil were investigated by thin layer and gas chromatography. Palmitic, oleic and linoleic acids were the major components in all lipid classes studied.

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The Darkening Effect of Phytosterylferulate on the Rice Bran Oil (Phytosterylferulate가 米糠油 暗色化에 미치는 影響에 關한 硏究)

  • Jum Sik Kim
    • Journal of the Korean Chemical Society
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    • v.13 no.4
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    • pp.325-332
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    • 1969
  • An attempt has been made to investigate the nature of the characteristic darkening reaction occurring in the rice bran oil during the storage. Several pigments were separated by using column and thin layer chromatography of the pigments was made in the light of the knowledge of absorption spectral behavior. The presence of trace amount of iron and phytosteryl esters of ferulic acid (3-methoxy-4-hydroxy-cinnamic acid) was found to be responsible for the development of the characteristic color in rice bran oil. The model reactions with the ferulate, iron and fatty acids could be suggested the mechanism.

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PHYTOCHEMICAL SURVEY OF HERB DURGS (VII) (국산생약의 식물화학 조사연구 VII)

  • 우린근;도상학;장정자
    • YAKHAK HOEJI
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    • v.13 no.4
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    • pp.147-148
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    • 1969
  • As one of projects of this Institute, 330 species of plants which are currently used as herb drugs in Korea were screened for the presence of alkaloids, phenolic compounds, flavonoids, chalcones, lactones, glycosides, carbohydrates, terpenoids, steroids, proteins, polypeptides, saponins, and organic acids. The most reliable presence of alkaloids detected by thin layer chromatography is presented by screening of 52 species.

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