• Title/Summary/Keyword: Thermal Treatment

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Numerical study of direct contact membrane distillation process: Effects of operating parameters on TPC and thermal efficiency

  • Zamaniasl, Mohammadmehdi
    • Membrane and Water Treatment
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    • v.10 no.5
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    • pp.387-394
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    • 2019
  • Membrane distillation (MD) is one of the water treatment processes which involves the momentum, heat and mass transfer through channels and membrane. In this study, CFD modeling has been used to simulate the heat and mass transfer in the direct contact membrane distillation (DCMD). Also, the effect of operating parameters on the water flux is investigated. The result shows a good agreement with the experimental result. Results indicated that, while feed temperature is increasing in the feed side, water flux improves in the permeate side. Since higher velocity leads to the higher mixing and turbulence in the feed channel, water flux rises due to this increase in the feed velocity. Moreover, results revealed that temperature polarization coefficient is rising as flow rate (velocity) increases and it is decreasing while the feed temperature increases. Lastly, the thermal efficiency of direct contact membrane distillation is defined, and results confirm that thermal efficiency improves while feed temperature increases. Also, flow rate increment results in enhancement of thermal efficiency.

Evaluation of the bond strength between aged composite cores and luting agent

  • Polat, Serdar;Cebe, Fatma;Tuncdemir, Aliriza;Ozturk, Caner;Usumez, Aslihan
    • The Journal of Advanced Prosthodontics
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    • v.7 no.2
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    • pp.108-114
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    • 2015
  • PURPOSE. The aim of this study was to evaluate effect of different surface treatment methods on the bond strength between aged composite-resin core and luting agent. MATERIALS AND METHODS. Seventy-five resin composites and also seventy-five zirconia ceramic discs were prepared. 60 composite samples were exposed to thermal aging (10,000 cycles, 5 to $55^{\circ}C$) and different surface treatment. All specimens were separated into 5 groups (n=15): 1) Intact specimens 2) Thermal aging-air polishing 3) Thermal aging- Er:YAG laser irradiation 4) Thermal aging- acid etching 5) Thermal-aging. All specimens were bonded to the zirconia discs with resin cement and fixed to universal testing machine and bond strength testing loaded to failure with a crosshead speed of 0.5 mm/min. The fractured surface was classified as adhesive failure, cohesive failure and adhesive-cohesive failure. The bond strength data was statistically compared by the Kruskal-Wallis method complemented by the Bonferroni correction Mann-Whitney U test. The probability level for statistical significance was set at ${\alpha}$=.05. RESULTS. Thermal aging and different surface treatment methods have significant effect on the bond strength between composite-resin cores and luting-agent (P<.05). The mean baseline bond strength values ranged between $7.07{\pm}2.11$ and $26.05{\pm}6.53$ N. The highest bond strength of $26.05{\pm}6.53$ N was obtained with Group 3. Group 5 showed the lowest value of bond strength. CONCLUSION. Appropriate surface treatment method should be applied to aged composite resin cores or aged-composites restorations should be replaced for the optimal bond strength and the clinical success.

Effect of non-thermal plasma on the shear bond strength of resin cements to Polyetherketoneketone (PEKK)

  • Labriaga, Wilmart;Song, So-Yeon;Park, Jin-Hong;Ryu, Jae-Jun;Lee, Jeong-Yol;Shin, Sang-Wan
    • The Journal of Advanced Prosthodontics
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    • v.10 no.6
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    • pp.408-414
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    • 2018
  • PURPOSE. This study aimed to assess the effect of non-thermal plasma on the shear bond strength of resin cements to polyetherketoneketone (PEKK) in comparison to other surface treatment methods. MATERIALS AND METHODS. Eighty PEKK discs were subjected to different surface treatments: (1) Untreated (UT); (2) Non-thermal plasma (NTP); (3) Sandblasting with $50{\mu}m$ $Al_2O_3$ particles (SB); and (4) Sandblasting + Non-thermal plasma (SB+NTP). After each surface treatment, the contact angle was measured. Surface conditioning with Visio.Link was applied in all groups after pre-treatment. RelyX Unicem resin cement was bonded onto the PEKK specimens. After fabrication of the specimens, half of each group (n=10) was initially tested, while the other half was subjected to thermocycling ($5^{\circ}C$ to $55^{\circ}C$ at 10,000 cycles). Shear bond strength (SBS) testing was performed using a universal testing machine, and failure modes were assessed using stereomicroscopy. The SBS results were analyzed statistically using one-way ANOVA followed by Tukey's post hoc test. Independent t-test was used to examine the effect of thermocycling (P<.05). RESULTS. The highest SBS values with or without thermocycling were observed with PEKK specimens that were treated with SB+NTP followed by the SB group. The lowest SBS results were observed in the UT groups. CONCLUSION. The shear bond strength between PEKK and resin cements was improved using non-thermal plasma treatment in combination with sandblasting.

Disintegration of sewage sludge using combined pre-treatment thermal hydrolysis and separation (열가수분해-고액분리 결합 공정을 적용한 하수슬러지의 가용화)

  • Lee, See-Young;Han, Ihn-Sup
    • Journal of the Korea Organic Resources Recycling Association
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    • v.29 no.4
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    • pp.107-114
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    • 2021
  • This study applied with pre-treatment combined with thermal hydrolysis and seperation for disintegration of sludge. As results of particle size distribution D10, D50 and D90 of thermal hydrolyzed and centrifuged sludge was 8.6, 59.2 and 425.1 ㎛, which are lower than those of thermal hydrolyzed. The molecular weight distribution results showed that the thermal hydrolyzed sludge showed the highest proportion in the 10-100kDa range. But, Sludge, treated with combined pre-treatment, showed the highest proportion <1kDa range. Results of DOC and UVA254 found that the organic matters of hydrolyzed sludge composed high molecular weight component above 10kDa. While, the organic matters of sludge, treated by combined pre-treatment, composed relarively low molecular weight below 1kDa. The specific methane yield of hydrolyzed and centrifuged sludge was higher 1.7 times than that of only hydrolyzed sludge.

Effects of hairline treatment on surface blackening and thermal diffusion of Zn-Al-Mg alloy-coated steel sheet (Zn-Al-Mg 합금도금강판의 헤어라인 처리가 표면흑색화 및 열확산도에 미치는 영향)

  • Jin Sung Park;Duck Bin Yun;Sang Heon Kim;Tae Yeob Kim;Sung Jin Kim
    • Journal of the Korean institute of surface engineering
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    • v.56 no.1
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    • pp.69-76
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    • 2023
  • The effects of hairline treatment on surface blackening and thermal diffusion behaviors of Zn-Al-Mg alloy coated steel sheet were evaluated by the three-dimensional surface profiler and laser-flash technique. The metallographic observation of coating damages by hairline treatments showed that several cracks were initiated and propagated along the interface between primary Zn/eutectic phases. As the hairline processing became more severe, the crack occurrence frequency in eutectic phase of coating layer and the surface roughness increased, which had a proportional relationship with the level of blackening on the coating surface. In addition, the higher interfacial areas of the blackened coating surface, caused by the hairline process, led to an increase in thermal diffusivity and conductivity of the coated steel sheet. On the other hand, when the coating damage by hairline treatment was excessive and the steel substrate was exposed, there was little difference between the thermal diffusivity/conductivity of the untreated sample though the blackening degree was higher than that of untreated sample. This work suggests that the increase in the surface areas of the coating layer without exposure to steel substrate through hairline treatment can be one of the effective technical strategies for the development of Zn-Al-Mg alloy coated steel sheets with higher blackening level and thermal diffusivity.

Effect of Thermal Cycle and Aging Heat Treatment on Transformation Characteristics of Cu-Zn-Al Shape Memory Alloys (Cu-Zn-Al계 형상기억합금의 변태특성에 미치는 열 Cycle 및 시효열처리의 영향)

  • Park, Pyeongyeol;Kim, Ickjun;Park, Seyun;Kim, Inbae;Park, Ikmin
    • Journal of the Korean Society for Heat Treatment
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    • v.2 no.4
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    • pp.47-55
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    • 1989
  • The effects of thermal cycle, aging heat treatment and Boron addition on the phase transformation characteristics and mechanical properties of the shape memory alloys of Cu-Zn-Al system, which was designed to operate about $80^{\circ}C$ by this research group, were studied. From the view point of the effects of thermal cycle on the phase transformation temperature change, it was found that up to 100 cycles Ms and Af points increased by $3-7^{\circ}C$ and Mf decreased a little bit and after that all of them were remain constant, and As point was not affected. All of the phase transformation temperatures were decreased $5-7^{\circ}C$ by aging heat treatment, at $140^{\circ}C$ for 24h however the effects of thermal cycle on aged alloys were same as on unaged alloys. As the thermal cycle increased the shape memory ability decreased a little up to 20 cycles, but above that it kept almost same ability. By Boron addition, grain size was refined from $1500{\mu}m$ to about $330{\mu}m$ and the hardness, fatigue property were improved but shape memory ability was lowered.

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Quality Deterioration Suppressing Effects of pH Regulators during Heat Treatment of Concentrated Blueberry Puree (농축 블루베리 퓌레 열처리 시 pH 조절제의 품질 저하 억제 효과)

  • Lee, In Gyeong;Min, Seo Cheol;Kim, Hee Sun;Han, Gwi Jung;Kim, Myung Hwan
    • Korean journal of food and cookery science
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    • v.32 no.5
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    • pp.549-558
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    • 2016
  • Purpose: In this study, we aimed to minimize quality degradation of concentrated blueberry puree by thermal treatment at $90^{\circ}C$ for 5 min, with citric acid (CA) and acidic sodium metaphosphate (ASM) as pH modifiers. Methods: The color values, redness a, anthocyanin contents, DPPH radical scavenging, elastase inhibition and tyrosinase inhibition activities were evaluated for quality parameters of concentrated blueberry puree. Results: The highest values of color value, redness a, anthocyanin contents, DPPH radical scavenging, elastase inhibition and tyrosinase inhibition activities were 1% CA+0.5% ASM followed by 1% CA and control. The quality parameters of concentrated blueberry puree were significantly different between control and 1% CA+0.5% ASM treatment (p<0.05). Conclusion: During thermal treatment, quality degradation of concentrated blueberry puree was reduced by 1% CA+0.5% ASM treatment, which is expected for new acidulants.

A study of DSC using Ultrasonic and Thermal treatment on nano-crystalline $TiO_{2}$ surface (염료감응형 태양전지 $TiO_{2}$ 광전극 표면의 초음파 열처리에 관한 연구)

  • Hong, Ji-Tae;Choi, Jin-Young;Seo, Hyun-Woong;Kim, Jong-Lak;Kim, Hee-Je
    • 한국신재생에너지학회:학술대회논문집
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    • 2007.06a
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    • pp.317-319
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    • 2007
  • Recently, there were many researches for efficiency improvement of DSC. Among of these works, research of surface treatment is still a prerequisite for electron diffusion, light-harvesting and surface state of $DSC^{4)}$. Using of the surface treatment, it can be raise up porosity of $TiO_{2}$ nano-crystalline structure on $photo-electrode^{5)}$. There are chemical, physical, electrical and optical methods which raise up its porosity. In this paper, we have designed and manufactured MOPA-type ultrasonic circuit (100W, frequency and duty variable). Manufactured ultrasonic circuit to use to force cavity density and power into $TiO_{2}$ paste. Then, we have optimized forcing time, frequency and duty of ultrasonic irradiation for surface treatment of photo-electrode of DSC. In I-V characteristic test of DSC, ultrasonic and thermal treated DSC shows 19% improved its efficiency against established DSC.

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Effect of Vacuum Heat Treatment on the Properties in Thermal Sprayed Ceramics Coating (세라믹스 용사 코팅 특성에 미치는 진공열처리의 영향)

  • Lee, J.I.;Ur, S.C.;Lee, Y.G.
    • Journal of the Korean Society for Heat Treatment
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    • v.13 no.2
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    • pp.98-102
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    • 2000
  • The effect of vacuum heat treatment in the thermal sprayed ceramics coating on a capstan by either high velocity oxygen fuel(HVOF) or plasma thermal spray process was investigated. The coating materials applied on the capstan were tungsten and chrome carbides. In order to characterize the interface between coating layer and bare materials, hardness, adhesion strength, X-ray diffraction(XRD) and microstructural analysis are conducted. The adhesion strength of the carbide coated materials by HVOF process is over 500MPa compared to those of plasma coating process is 230MPa. In case of the carbide coated materials by HVOF process, the adhesion strength is increased to 15MPa and the porosity is reduced under 5% by vacuum heat treatment for 5 hrs at $1000^{\circ}C$. The XRD results reveal that the increasement is believed due to the phase stabilization of metastable $Cr_3C_2$ phase to stable $Cr_{23}C_6$ phase.

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Coercivity Enhancement of Nd23Dy10Fe64TM2B1 Sintered Magnet by Convergent Heat Treatment (Convergent 열처리를 통한Nd23Dy10Fe64TM2B1 소결자석의 보자력 향상)

  • Kim, Hoon-Sup;Kim, Se-Hoon;Kim, Jin-Woo;Kim, Young-Do
    • Journal of Powder Materials
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    • v.17 no.1
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    • pp.1-6
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    • 2010
  • In this study, a convergent heat treatment was performed in certain temperature regions in order to control the microstructures of Nd-rich phases and to reduce thermal stress on grain boundaries which could be caused during expansion and shrinkage of Nd-rich and $Nd_2Fe_{14}B$ phases. The difference of thermal expansion coefficient between $Nd_2Fe_{14}B$ and Nd-rich phases is the mechanism for convergent heat treatment. The Nd-rich phases which were located in junctions could penetrate into the grain boundaries between $Nd_2Fe_{14}B$ phases due to the difference of thermal expansion coefficient. Through the convergent heat treatment, the microcracks that were observed in cyclic heat treatment were not observed and coercivity was increased to 34.05 kOe at 8 cycles.