• Title/Summary/Keyword: Tensile Adhesion Test

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Performance Test Method on the Influence Waterproofing as Behavior of Concrete Structure (지하 콘크리트 구조물의 거동에 대한 방수층의 대응성 평가에 관한 실험적 연구)

  • Noh Jong-Soo;Kwon Shi-Won;Kwak Kyu-Sung;Kwon Kee-Joo;Oh Sang-Keun
    • Proceedings of the Korean Institute of Building Construction Conference
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    • v.y2004m10
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    • pp.77-81
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    • 2004
  • The massive structures are not free to move with vibration, differential settlement, thermal stresses because, construction and expansion joint, crack etc., can be large enough to cause leakage as deformation of waterproofing. It has been depended on the test method of tensile/tear strength which is waterproofing performance as behavior of concrete structure crack. However, not to practically confirm the creep applied to concrete surface, even waterproofing membrane have more performance than definite strength and elasticity. Therefore, in this study will focus on the test method to consider a resistance performance about loose adhesion and deformation of waterproofing and behavior of concrete structure as construction/expansion joint, crack. Performance test method on the influence as behavior of concrete structure crack is to choose waterproofing materials and construction method which possible to confront with behavior of 50mm crack in the atmosphere and low temperature. Examine the deformation of waterproofing membrane and loose adhesion which can occur to structure in general job site, suggest standard testing method to analyze correlation waterproofing membrane and structure with 5-types of materials used in this study, such as Adhesion membrane and sheet complex, sheet and urethane complex, self-adhesive sheet, spray poly-urea, spray membrane of rubberized Asphalt.

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Influence of ozone and paracetic acid disinfection on adhesion of resilient liners to acrylic resin

  • Ekren, Orhun;Ozkomur, Ahmet
    • The Journal of Advanced Prosthodontics
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    • v.8 no.4
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    • pp.290-295
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    • 2016
  • PURPOSE. The aim of this study was to evaluate the effect of paracetic acid (PAA) and ozone disinfection on the tensile bond strength (TBS) of silicone-based resilient liners to acrylic resins. MATERIALS AND METHODS. One hundred and twenty dumbbell shaped heat-polymerized acrylic resins were prepared. From the mid segment of the specimens, 3 mm of acrylic were grinded off and separated parts were reattached by resilient liners. The specimens were divided into 2 control (control1, control7) and 4 test groups of PAA and ozone disinfection (PAA1, PAA7, ozone1 and ozone7; n=10). While control groups were immersed in distilled water for 10 min (control1) and 7 days (control7), test groups were subjected to PAA (16 g/L) or ozone rich water (4 mg/L) for 1 cycle (10 min for PAA and 60 min for ozone) per day for 7 days prior to tensile tests. Measurements of the TBS were analyzed using 3-way ANOVA and Tukey's HSD test. RESULTS. Adhesive strength of Mollosil decreased significantly by application of ozone disinfection. PAA disinfection had no negative effect on the TBS values of Mollosil and Molloplast B to acrylic resin. Single application of ozone disinfection did not have any negative effect on TBS values of Molloplast B, but prolonged exposure to ozone decreased its adhesive strength. CONCLUSION. The adhesion of resilient liners to acrylic was not adversely affected by PAA disinfection. Immersion in ozonated water significantly decreased TBS of Mollosil. Prolonged exposure to ozone negatively affects adhesion of Molloplast B to denture base materials.

Evaluation of Mechanical Performance and Flame Retardant Characteristics of Biomass-based EVA Composites using Intumescent Flame Retardant Technology

  • Park, Ji-Won;Kim, Hoon;Lee, Jung-Hun;Jang, Seong-Wook;Kim, Hyun-Joong
    • Journal of the Korean Wood Science and Technology
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    • v.46 no.2
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    • pp.189-201
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    • 2018
  • Intumescent system is a highly effective flame retardant technology that takes advantage of the mechanism of foaming and carbonization. In order to materialize Intumescent system, it is necessary to use reinforcement material to improve the strength of the material. In this study, we used kenaf as a natural fiber to manufacture intumescent/EVA (ethylene vinyl acetate) composites to improve mechanical and flame retardant performance. Finally two materials with different particle shape are applied to one system. Therefore, the influence factors of the particles with different shapes on the composite material were analyzed based on the tensile test. For this purpose, we have used the tensile strength analysis model and confirmed that it can only act as a partial strength reinforcement due to weak binding force between the matrix and particles. In the combustion characteristics analysis using cone calorimeter and UL 94, the combustion characteristics were enhanced as the content of Intuemscent was increased. As the content of kenaf increased, combustion characteristics were strengthened and carbonization characteristics were weakened. Through the application of kenaf, it can be confirmed that elastic modulus improvement and combustion characteristics can be strengthened, which confirmed the possibility of development of environmentally friendly flame retardant materials.

Properties of Blood Compatible Crosslinked Blends of $Pellethene^{(R)}$/Multiblock Polyurethanes Containing Phospholipid Moiety/C-18 Alkyl Chain

  • Yoo, Hye-Jin;Kim, Han-Do
    • Macromolecular Research
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    • v.16 no.7
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    • pp.596-603
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    • 2008
  • To improve the mechanical properties, dimensional stability and blood compatibility, the biomedical material $Pellethene^{(R)}$ was blended with multiblock polyurethane (MPU) containing phospopholipid/long alkyl chain (C-18) at the various MPU contents and crosslinked using dicumyl peroxide as a crosslinking agent. The maximum MPU content for stable $Pellethene^{(R)}$/MPU blended films was approximately 30 wt%. The optimum crosslinking agent content and crosslinking time with respect to the mechanical properties were 4 wt% and 3 h, respectively. The mechanical properties (tensile strength and elongation at break) and water absorption of the crosslinked blend film increased with increasing MPU content. The test of platelet adhesion on the surfaces of the crosslinked blend film showed a decrease in the level of platelet adhesion from 70% to 6% with increasing MPU content from 0 to 30 wt%. These results suggest that the crosslinked $Pellethene^{(R)}$/MPU-30 (MPU content: 30 wt%) sample has strong potential as a novel material for blood compatible material applications.

Synthesis and Characteristics of Unsaturated Polyester Modified with Rosin Containing 2-Hydroxyethylmethacrylate (2-Hydroxyethylmethacrylate가 도입된 로진 변성 불포화 폴리에스테르의 합성과 그 특성)

  • Kang, D.W.;Yoon, D.K.;Kweon, D.K..
    • Applied Chemistry for Engineering
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    • v.10 no.3
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    • pp.450-455
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    • 1999
  • Unsaturated diol (UD) was prepared from the esterification of maleic anhydride with diethylene glycol (DEG). Unsaturated polyesters modified with rosin (UPMR) or with rosin maleic anhydride adduct (RMA) from 2-hydroxyethylmethacrylate (HEMA) and rosin (UPMRH) were prepared by the reaction of UD with RMA or RMA-HEMA. After crosslinking of UPMR and UPMRH with styrene and methylmethacrylate (MMA), respectively, solvent resistance, tensile strength, and adhesion property of the resins were measured. UPMR crosslinked with styrene or MMA shows an excellent resistance to water and acid. Solvents resistance and tensile strength of UPMR using styrene as crosslinking agent were increased compared with those of UPMR using MMA as crosslinking agent. UPMRH showed better solvents resistance and tensile strength than UPMR. Adhesion strengths of UPMR crosslinked with styrene and MMA were 1.61 and 3.02 MPa, and those of UPMRH were 2.32 and 3.89 MPa, respectively.

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Bonding Properties of PMMA Mortars Using EPS with Silane Coupling Agent (실란 커플링제를 첨가한 발포폴리스티렌 혼입 폴리메타크릴산 메틸 모르타르의 부착특성)

  • Lee, Chol-Woong;Mun, Kyoung-Ju;Choi, Nak-Woon;Jeon, Seong-Hwan;Soh, Yang-Seob
    • Proceedings of the Korea Concrete Institute Conference
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    • 2006.05b
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    • pp.301-304
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    • 2006
  • The purpose of this study is to evaluate bonding properties of PMMA mortars using EPS with silane coupling agent. PMMA mortars are prepared with various silane coupling agent, and tested for flexural strength test, adhesion test in flexure and tensile strength in underwater and air. It is estimated that the application of silane coupling agent to PMMA mortar is more effective in underwater than air.

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Effect of Ultrasound on the Properties of Biodegradable Polymer Blends of Poly(lactic acid) with Poly(butylene adipate-co-terephthalate)

  • Lee, Sang-Mook;Lee, Young-Joo;Lee, Jae-Wook
    • Macromolecular Research
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    • v.15 no.1
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    • pp.44-50
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    • 2007
  • This study investigated the effect of ultrasound irradiation on the blend of poly(lactic acid) (PLA) and poly(butylene adipate-co-terephthalate) (PBAT). The blends of PLA/PBAT(50/50) (PBAT50) were prepared in a melt mixer with an ultrasonic device attached. Thermal, rheological, and mechanical properties, morphology, and biodegradability of the sonicated blends were analysed. The viscosity of the sonicated blends was increased by the ultrasound irradiation owing to the strong interaction. The morphology of the sonicated blends was significantly dependent on the duration o the ultrasound irradiation. For PBAT50, the phase size reduction was maximized when the blends were ultrasonically irradiated for 30 sec. At longer duration of ultrasound irradiation, the PBAT phase underwent flocculation. Measurement of the tensile properties showed an increased breakage tensile stress and an enhanced Young's modulus when the blends were properly irradiated. This improvement was ascribed to better adhesion between the PLA matrix and the PBAT domain and to better dispersion of the PBAT phase. However, the tensile properties were maximized after excessive energy irradiation, which was ascribed to an emulsifying effect leading to coalescence of the PBAT phase. Impact strength was increased to reach a peak with the ultrasound irradiation, and was higher than the untreated sample for all sonicated samples due to the difference of failure mechanism between the tensile test and the impact test.

Bond Strength Properties of Latex Modified Concrete (라텍스 개질 콘크리트의 부착강도 특성)

  • 윤경구;이주형;최상릉;김기헌
    • Journal of the Korea Concrete Institute
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    • v.13 no.5
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    • pp.507-515
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    • 2001
  • Significant improvements in bond strength between new and existing concrete can be achieved through the modification of the new concrete by latex. This study focuses on the investigation of bond strength of latex modified concrete. Pull-out bond test and uniaxial direct tensile bond test are adopted for evaluating the adhesion characteristics of latex modified concrete to conventional concrete substrate. The main experimental variables are test methods, latex-cement ratio, surface preparations and moisture levels. The results are as follows; The increase of latex-cement ratio substantially improves the adhesion between latex modified concrete and substrate. The effects of surface preparation at substrate into the bonding of latex modified concrete are quite different according to the conditions of surfaces. Thus, an adequate surface preparations are essential for good bond strength. Because the moisture level of the substrate may be critical to achieving bond, optimum moisture condition for a conventional concrete has evaluated in this study. The saturated condition of surface is the most appropriate moisture level among the considered, followed by dry condition and wet condition.

Effect of Coupling Agent and Fiber Loading on Mechanical Behavior of Chopped Jute Fiber Reinforced Polypropylene Composites (황마 단섬유 강화 폴리프로필렌 복합재료의 기계적 거동에 미치는 결합제 및 섬유 Loading의 영향)

  • Rasel, S.M.;Nam, G.B.;Byeon, J.M.;Kim, B.S.;Song, J.I.
    • Elastomers and Composites
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    • v.46 no.3
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    • pp.204-210
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    • 2011
  • In this study, Jute fibers reinforced polypropylene (JFRP) composites were manufactured by injection molding technique. In order to improve the affinity and adhesion between fibers and thermoplastic matrices during manufacturing, Maleic anhydride (MA) as a coupling agent have been employed. Untreated and treated surfaces of jute fibers were characterized using SEM and Fourier transform infrared (FTIR). Physical properties like water absorption rate were studied. Tensile and flexural tests were carried out to evaluate the composite mechanical properties. Tensile test and bending test indicated that JFRP composites show higher strength and modulus than pure PP. In addition, strength and modulus were found to be influenced by the variation of MAPP content (1%, 2%, and 3%). Tensile fracture surfaces were examined using scanning electron microscope. It ensures better interfacial adhesion between fibers and matrix by increasing the percentage of MAPP.

Synthesis and Characterization of Polyimide/silica Hybrid Films Derived from Silane Oligomer Containing Epoxy Group (에폭시 그룹을 함유한 실란 올리고머의 합성과 그로부터 유도된 폴리이미드/실리카 혼성 필름의 특성)

  • Lee, Jun Hyuk;Park, Yun Jun;Choi, Jong-Ho;Nam, Sang Yong;Kim, Sung Won;Hong, Young Taik
    • Journal of Adhesion and Interface
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    • v.10 no.2
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    • pp.98-105
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    • 2009
  • Poly(amic acid) was synthesized from the reaction of p-PDA/ODA and PMDA/BPDA and silane oligomer containing epoxy group was also synthesized from the reaction of tetramethylorthosilicate (TMOS) and glycidol. After hybridizing poly (amic acid) and silane oligomer, they were effectively converted into polyimide/silica hybrid films by thermal imidization process. As the silica contents in hybrid films increased, CTE values decreased from 17 ppm/K to 10 ppm/K and the tensile modulus increased, in spite of decreasing tensile strength. In addition, the peel test showed that the adhesion strength of hybrid film was enhanced from $0.43kg_f/cm$ to $1.02kg_f/cm$. Therefore, it could be concluded that the polyimide/silica hybrid film is effective to enhance adhesion strength for FCCL films.

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