• Title/Summary/Keyword: Synchrotron X-ray

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X-ray PIV Measurements of Velocity Field of Blood Flows

  • Lee, Sang-Joon;Kim, Guk-Bae
    • International Journal of Vascular Biomedical Engineering
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    • v.4 no.1
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    • pp.1-8
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    • 2006
  • The x-ray PIV method was improved for measuring quantitative velocity fields of real blood flows using a coherent synchrotron x-ray source. Without using any contrast media or seeding particles, this method can visualize flow pattern of blood by enhancing the phase-contrast and interference characteristics of blood cells based on a synchrotron x-ray imaging mechanism. The enhanced x-ray images were achieved by optimizing the sample-to-scintillator distance, the sample thickness, and hematocrit. The quantitative velocity fields of blood flows inside opaque tubes were obtained by applying a 2-frame PIV algorithm to the x-ray images of the blood flows. The measured velocity field data show typical features of blood flows such as the yield stress effect. The non-Newtonian flow characteristics of blood flows were analyzed using the x-ray PIV method and the experimental results were compared with hemodynamic models.

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CHARACTERIZATION OF METALLIC CONTAMINATION OF SILICON WAFER SURFACES FOR 1G DRAM USING SYNCHROTRON ACCELERATOR

  • Kim, Heung-Rak;Kun-Kul, Ryoo
    • Journal of the Korean institute of surface engineering
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    • v.32 no.3
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    • pp.239-243
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    • 1999
  • At Present, 200mm wafer technology is being applied for commercial fabrications of 64, 128, and 256 M DRAM devices, and 300mm technology will be evolved for 1G DRAM devices in the early 21th century, recognizing limitations of several process technologies. In particular recognition has been realized in harmful effects of surface contamination of trace metals introduced during devicing processes. Such a guide line for surface metal contamination has been proposed as 1E9 and 1E10 atoms/$\textrm{cm}^2$ of individual metal contamination for wafering and devicing of 1G DRAM, respectively, and so its measurement limit should be at least 1E8 atoms/$\textrm{cm}^2$. The detection limit of present measurement systems is 2E9 atoms/$\textrm{cm}^2$ obtainable with TRXFA(Total Reflection X-Ray Fluorescence Analysis). TRXFA is nondestructive and the simplest in terms of operation, and it maps the whole wafer surfaces but needs detection improvement. X-Ray intensity produced with synchrotron accelerator is much higher than that of conventional X-ray sources by order of 4-5 magnitudes. Hence theoretically its reactivity with silicon surfaces is expected to be much higher than the conventional one, realizing improvement of detection limit. X-ray produced with synchrotron accelerator is illuminated at a very low angle with silicon wafer surfaces such as 0.1 degree and reflects totally. Hence informations only from surface can be collected and utilized without overlapping with bulk informations. This study shows the total reflection phenomenon and quantitative improvement of detection limit for metallic contamination. It is confirmed that synchrotron X-ray can be a very promising alternative for realizing improvement of detection limit for the next generation devices.

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High Pressure X-Ray Diffraction Study on a Goethite using Synchrotron Radiation (방사광을 이용한 괴타이트에 대한 고압 X-선 회절연구)

  • 김영호;이지은
    • Journal of the Mineralogical Society of Korea
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    • v.10 no.2
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    • pp.75-81
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    • 1997
  • High pressure X-ray diffraction study was carried out on a natural FeO(OH)-goethite to investigate its compressibility at room temperature. Energy dispersive X-ray diffraction method was employed using Mao-Bell type diamond anvil cell with Synchrotron Radiation. MgO powder was compressed together with goethite for the high pressure determinations. Bulk modullus was determined to be 147.9 GPa by the Birch-Murnaghan equation of state under assumption of K0' of 4. This value was subjected to compare with its structural analogs and related materials.

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Survey on ultrafast time resolved X-ray diffraction measurements of crystal structure (X선의 초고속 결정구조 측정법)

  • Koo, Y.D.;Kim, Y.C.;Oh, C.S.
    • Journal of Energy Engineering
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    • v.23 no.3
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    • pp.13-16
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    • 2014
  • We have surveyed on significant progress in recent developments of accelerator-based pulsed X-ray sources has offered the opportunity for time-resolved studies on fast structure dynamics on the nanometer scale. The required and currently available techniques for time resolved X-ray diffraction measurements using the third-generation synchrotron radiation sources are summarized. Ultrafast X-ray experimental techniques are discussed for femtosecond studies at future synchrotron radiation sources.

Synchrotron X-ray Micro-imaging Technique for Simultaneous Measurement of Size and Velocity of Micro-bubbles (X-ray 미세 영상기법을 이용한 미세기포의 크기 및 속도 동시측정)

  • Kim, Seok;Lee, Sang-Joon
    • Proceedings of the KSME Conference
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    • 2004.04a
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    • pp.1744-1748
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    • 2004
  • It is important to measure precisely the size and velocity of micro-bubbles used in various field. The synchrotron X-ray micro-imaging technique was employed to measure the size and velocity of micro-bubbles moving in an opaque tube simultaneously. Phase contrast images were obtained at interfaces of micro-bubbles between water and air due to their different refractive indices. The X-ray micro-imaging technique was found to measure an optical fiber with an accuracy of 0.2%. Micro-bubbles of $10{\sim}60{\mu}m$ diameter moving upward in an opaque tube (${\phi}=2.7mm$) were tested to measure bubble size and up-rising velocity. For DI water, the measured velocity of micro-bubbles is nearly proportional to the square of bubble size, agreed well with the theoretical result. In addition, the synchrotron X-ray micro-imaging technique can measure accurately the size and velocity of several overlapped micro-bubbles.

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Synchrotron X-ray Powder Diffraction Study of CFC-13 Loaded Zeolite LSX (제올라이트 LSX에서의 CFC-13 분자체 흡착에 관한 결정학적 연구)

  • Lee, Yong-Jae;Lee, Jong-Won;Yoon, Ji-Ho
    • Journal of the Mineralogical Society of Korea
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    • v.21 no.3
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    • pp.307-312
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    • 2008
  • Rietveld analysis using synchrotron X-ray powder diffraction data collected at 15 K reveals that CFC-13 ($CF_{3}Cl;$ chlorotrifluoromethane) sorbed on Na,K-LSX binds through fluorine to sodium ions around the single 6-ring aperture in the supcrgage.

최근의 X-ray 리소그래피 기술개발 현황

  • Yu, Hyeong-Jun;Hwang, Ho-Jun;Lee, Byeng-Chul;Yun, Chang-Joo
    • Electronics and Telecommunications Trends
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    • v.5 no.3
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    • pp.14-31
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    • 1990
  • 반도체기술의 발전에 따라 보다 정교한 리소그래피 기술이 요구되고 있으며, x-ray 리소그래피 기술이 다음 세대 리소그래피 기술로 활발히 연구되고 있다. 특히 최근 리소그래피 전용 compact synchrotron 등 관련분야 기술발전에 힘입어 x-ray 리소그래피는 막대한 초기투자에도 불구하고, 전체적으로는 경쟁력을 확보하는 수준에 이르렀으며, 실용화 가능성이 한층 높아졌다. 그러나 아직도 마스크 및 resist 등 해결하여야 할 문제가 많이 남아 있다. 본 고에서는 주로 '80년대 후반에 이루어진 x-ray 리소그래피 기술의 연구개발 현황을 정리하였다. 특히 미국, 일본, 유럽에서의 개괄적인 연구개발 현황과, 고출력 x-ray 광원으로서 실용화에 성큼 다가선 compact synchrotron의 개발현황, x-ray 리소그래피 기술의 핵심중의 하나인 x-ray 마스크 기술개발 현황 등을 중심으로 기술하였다.

In Situ Observation of Initial Rusting Process of Steel Containing Al Using Synchrotron Radiation X-Rays

  • Morimoto, J.;Yamashita, M.;Uchida, H.;Doi, T.;Kamimura, T.;Miyuki, H.;Konishi, H.;Mizuki, J.
    • Corrosion Science and Technology
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    • v.7 no.2
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    • pp.112-118
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    • 2008
  • We observed initial rusting process of steel containing Al under wet/dry cyclic condition with NaCl solution film using in situ X-ray diffraction spectroscopy at SPring-8 synchrotron radiation facility. It was found that mass fraction of iron oxides such as ${\alpha}-FeOOH$, ${\beta}-FeOOH$ and ${\gamma}-FeOOH$ varied with Al content. Some kinds of Al oxides were also found at the initial stage of corrosion. Those corrosion products might affect the corrosion process and corrosion rate of the steel.

Micrometer Spatial Resolution Imaging System Using Synchrotron X-ray (Synchrotron X-선을 이용한 Micrometer 공간 분해능 영상시스템)

  • 홍진오;정해조;정하규;제정호;김은경;유형식;김희중
    • Journal of Biomedical Engineering Research
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    • v.22 no.2
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    • pp.165-169
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    • 2001
  • 최근 포항 방사광 가속기 연구소에 미세구조 X-선 영상 실험을 위한 5C1 방사광(Synchrtoron Radiation) 빔라인이 건설되었다. 광대역의 에너지 스펙트럼을 가진 방사광 X-선이 물체를 투과한 후 CdWO$_{4}$ scintillator에 의해 가시광선으로 바뀌고, 그 빛을 CCD 카메라로 받아들여 영상을 획득하게 된다. 방사광 X-선은 일반 의료진단용 X-선에 비하여 위상이 일치하고, 평행하며, 그 양이 풍부한 특성들을 갖고 있다. 방사광 영상시스템과 X-선 유방촬영 시스템에서 영상을 획득하여 영상특성들을 비교, 분석하였다. 고-분해능 X-선 시험 패턴(20 line pairs mm$^{-1}$), 유방촬영 팬텀, 파라핀에 고정한 인체 유방암조직과 포르말린에 고정한 인체 유방암조직, 그리고 capillary tube내 micro-bubbles등의 방사광 영상은 기존의 X-선 유방촬영시스템에서 얻은 영상보다 분해능이 뛰어나고 영상질도 우수하였다. 방사광 X-선 영상시스템은 micrometer 공간 분해능 영상을 획득할 수 있어 많은 기초분야의 영상연구와 의료영상분야에서도 활발하게 활용될 것으로 기대된다.

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Phase Transition Study on Graphite at Room Temperature (고압하에서 방사광을 이용한 흑연에 대한 연구)

  • Kim, Young-Ho;Na, Ki-Chang
    • The Journal of the Petrological Society of Korea
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    • v.6 no.2
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    • pp.88-95
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    • 1997
  • High pressure X-ray diffraction study was carried out on a polycrystalline graphite to investigate the phase transition(s) at room temperature. Energy dispersive X-ray diffraction method was employed using a Mao-Bell type diamond anvil cell with an Wiggler synchrotron Radiation at the National Synchrotron Light Source. Sodium chloride power was used as the internal pressure sensor for the high pressure determinations as well as the pressure medium for quasihydrostatic pressure environment. Graphite transforms into a hexagonal didose not agree with the previously reported observations and this phase persists when pressure is released down to 0.1 MPa. This result dose not agree with the previously reported observations and this discrepancy would be due to the kinetics in phase transition as well as the uniaxially oriented pressure field in the diamond anvil cell.

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