• Title/Summary/Keyword: Surface treatment.

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Effect of surface and heat treatment on the bond strength of veneering ceramics to zirconia(Y-TZP) (표면처리와 열처리가 전장도재와 지르코니아의 결합력에 미치는 영향)

  • Lee, Jung-Hwan;Ahn, Jae-Seok
    • Journal of Technologic Dentistry
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    • v.35 no.4
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    • pp.271-280
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    • 2013
  • Purpose: This study was to assess the effect of surface and heat treatment on the bond strength of veneering ceramics to zirconia. Methods: The specimens were divided into 7 groups according to surface treatment and heat treatment conditions prior to porcelain application. ten specimens from each group were subjected to a 3-point flexural test. In addition the influence of surface and heat treatment on surface roughness values and phase transformation of zirconia was evaluated. Statistical analysis was performed with one-way ANOVA and post hoc Tukey's test. Results: Bond strength ranged from $20.67{\pm}3.13MPa$ to $32.69{\pm}4.52$. Bond strength of surface treatment group was lower than that of control group but only $Al_2O_3$ sandblasting group was significant difference. Bond strength of heat treatment group was higher than that of surface treatment group but there was no statistical significance. Conclusion: Bond strength of veneering ceramics to zirconia was affected by surface and heat treatment.

Effect of Heat Treatment on the Surface Machined by W-EDM (고온 열처리가 와이어 컷 가공면에 미치는 영향)

  • Choi, K.K.;Lee, Y.S.
    • Transactions of Materials Processing
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    • v.15 no.8 s.89
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    • pp.539-543
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    • 2006
  • Experimental studies are carried out in order to investigate the effects of heat treatment on the surface machined by W-EDM. In this work, two ways of heat treatment after W-EDM are considered. As a comparison, the machined surface by a traditional method such as milling/grinding is also considered. Thereby, specimens are prepared by four different machining methods. Those are (1) milling and then grinding, (2) wire-cut electric discharge machining (W-EDM), and (3) low temperature heat treatment or (4) high temperature heat treatment after W-EDM. The resulting surface roughness are measured and the changes of surface microstructures are investigated using the scanning electron microscope (SEM) with energy dispersive X-ray spectrometer (EDS). In general, heat treatment after W-EDM result in smoother surface and better chemical composition at the machined surface. Especially, high temperature tempering could remove defects in the thermally affected zone, which cause an overall deterioration of the surface machined by W-EDM.

Plasma Surface Treatment of the Polymeric Film with Low Temperature Process (저온프로세스를 이용한 고분자필름의 플라즈마 표면처리)

  • Cho, Wook;Yang, Sung-Chae
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.21 no.5
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    • pp.486-491
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    • 2008
  • The plasma processing is applied to many industrial fields as thin film deposition or surface treatment technique. In this study, we investigated large-area uniformed surface treatment of PET film at low temperature by using Scanning Plasma Method(SPM). Then, we measured difference and distribution of temperature on film's surface by setting up a thermometer. We studied the condition of plasma for surface treatment by examining intensity of irradiation of uniformed plasma. And we compared contact angles of treated PET film by using Ar and $O_2$ plasma based low temperature. In our result, surface temperature of 3-point of treating is low temperature about $22^{\circ}C$, in other hands, there is scarcely any variation of temperature on film's surface. And by using Ar plasma treatment, contact angle is lower than untreatment or $O_2$ plasma treatment. In case of PET film having thermal weak point, low temperature processing using SPM is undamaged method in film's surface and uniformly treated film's surface. As a result, Ar plasma surface treatment using SPM is suitable surface treatment method of PET film.

A Study on Surface Treatment for Rubber Materials with Low Friction Factor

  • Li, Xiang-Xu;Cho, Ur Ryong
    • Elastomers and Composites
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    • v.51 no.1
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    • pp.43-48
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    • 2016
  • Multi-Surface (MS) treatment is a new technique of surface treatment to reduce the static friction factor on the surface of rubber. MS treatments include 4 methods which names are MS-V (UV-irradiation on the rubber surface), MS-M (doing the chemical reaction with double bond of rubber), MS-Q (dilution of rubber surface by silicone surfactant), and MS-P (coating and heating of rubber surface). The experiment and test of every MS-treatment had been carried out using acrylonitrile-butadiene rubber (NBR), ethylene-propylene-diene rubber (EPDM), and chlorosulphonated rubber (CSM) as rubber materials. It had introduced the steps of every MS-treatment process and the result of the properties test. From the research, it was found that the best method was MS-V treatment because it suited all the samples and the effect was obviously.

A study on the Polymer surface treatment of GF-filter bag for collection of fine Particle like carbon black (카본블랙류 미세입자 포집을 위한 유리섬유 필터백의 고분자 표면처리에 관한 연구)

  • Lee, B.;Choi, H.L.;Moon, C.K.
    • Journal of Power System Engineering
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    • v.12 no.3
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    • pp.55-59
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    • 2008
  • In this paper, we have investigated on collection efficiency of fine particle of glass fiber-filter bag according to the surface treatment. The solution consisted of polytetrafluoroethylene(teflon), graphite powder, silicon resin and water was used as a basic surface treatment agent. Tensile strength of glass filter-bag increased with up to 3hrs and then decreased with surface treatment time. Tensile strength and initial modulus of the glass fiber-filter bag treated by iodine after basic surface treatment for 3hrs were lower than those of basic surface treatment for 3hrs, however collection efficiency and fracture strain were higher than those of basic surface treatment for 3hrs. Glass fiber-filter bag with lower initial modulus and more strain will be extend the durable period and the one treated by iodine after basic surface treatment 3or 3hrs is expected high collection efficiency of fine particle. This method makes it possible to manufacture glass fiber-filter bag of the optimum condition.

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The Improvement of Surface Roughness of Poly-$Si_{1-x}Ge_x$Thin Film Using Ar Plasma Treatment (아르곤 플라즈마처리에 의한 다결정 $Si_{1-x}Ge_x$박막의 표면거칠기 개선)

  • 이승호;소명기
    • Journal of the Korean Ceramic Society
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    • v.34 no.11
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    • pp.1121-1128
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    • 1997
  • In this study, the Ar plasma treatment was used to improve the surface roughness of Poly-Si1-xGex thin film deposited by RTCVD. The surface roughness and the resistivity of Si1-xGex thin film were investigated with variation of Ar plasma treatment parameters (electrode distance, working pressure, time, substrate temperature and R.F power). When the Ar plasma treatment was used, the cluster size decreased by the surface etching effect due to the increasing surface collision energy of particles (ion, neutral atom) in plasma under the conditions of decreasing electrode distance and increasing pressure, time, temperature, and R. F power. Although the surface roughness value decreased by the reduction of the cluster size due to surface etching effect, however, the resistivity increased. This may be due to the surface damage caused by the increasing surface collision energy. It was concluded that the surface roughness could be improved by the Ar plasma treatment, while the resistivity was increased by the surface damage on the substrate.

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An Experimental Study of the Surface Treatment Effect on the Frosting/Defrosting Behavior of a Fin-Tube Heat Exchanger (휜-관 열교환기의 착.제상 거동에 대한 표면처리의 영향에 관한 실험적 연구)

  • Jhee, Sung;Lee, Kwan-Soo
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.24 no.8
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    • pp.1062-1068
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    • 2000
  • The effect of heat exchanger surface treatment on the frosting/defrosting behavior in a fin-tube heat exchanger is investigated experimentally. It is found that the hydrophilic surface mainly influences on the frosting behavior, however, the hydrophobic surface gives some influence on the defrosting behavior. In view of frosting performance, surface-treated heat exchanger with either hydrophilic or hydrophobic characteristic shows a little improvement in the thermal performance than the aluminium heat exchanger with no surface treatment. The result reveals that the heat exchanger with hydrophobic surface treatment is more effective in view of the defrosting efficiency and time. The amounts of residual water on the surface-treated heat exchangers are shown to be smaller than those of the bare heat exchanger, therefore further improvements on the performance of re-operations are expected.

The Effect of Coloring Condition on the Surface Characteristic of 304 Stainless Steel (304 스테인리스강의 착색 처리 조건이 표면 특성에 미치는 영향)

  • Kim, Ki-Ho
    • Journal of Surface Science and Engineering
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    • v.44 no.5
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    • pp.220-225
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    • 2011
  • 304 stainless steel plate was colored by hot dip and electrochemical treatment in a solution containing sulphuric and chromic acids. In the process, treatment variables such as operating time and methode were changed. The surface characteristics that changed by the treatment of the samples such as surface composition, oxide film thickness, color, surface roughness and reflectivity were studied. Surface composition was varied as follows. Fe was decreased, but Cr and O were increased. Ni was increased until 20 min, but reveals decreasing tendency as time passed after that. These means the surface film becomes chrome rich oxide phase as the treatment times increase. The thickness of film was about 220 nm at 30 min by dip treatment and it reduced as the treatment times increased. On the other hand, the thickness was about 150 nm at 10 min by electrochemical method and it doesn't increased with time. Surface color changed from metallic white of the base plate to gray, black, red, and green-blue, gradually, as the treating time increased. The reflectivity of colored surface measured by UVVIS-NIR spectrophotometer was reduced from max 38% of basis metal to min 3.5%.

A Study on the Characteristics and Surface Modification of the Zeocarbon for Water Treatment

  • Kim, Seo-A;Hong, Ji-Sook;Suh, Jeong-Kwon;Lee, Jung-Min
    • Carbon letters
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    • v.6 no.3
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    • pp.166-172
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    • 2005
  • The objective of this study was to investigate the possibility of application for water treatment using the zeocarbon. The zeocarbon was mixture of zeolite and activated carbon. In general, the application of commercial zeocarbon to water treatment is difficult because of weak strength in water and the high pH value of effluents after water treatment. Therefore, we have modified the surface of zeocarbon. For the surface modification, we used the acid treatment to make surface functional group. As a result of modification, was created functional group on zeocarbon surface and was formed mesopore in zeocarbon. The surface modified zeocarbon was applied to removal of nitrogen. In removal experiments of nitrogen, removal efficiency was very high. And, strength of zeocarbon after water treatment and pH of effluents were stabilized. This indicates that the surface modified zeocarbon was easy to recover and reuse. Consequently, our results were shown the possibility of application for water treatment using the surface modified zeocarbon.

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Effect of Surface Condition on the Bonding Characteristics of 3Y-$ZrO_2$-Metal Bracket System (3Y-$ZrO_2$ 세라믹과 교정용 브라켓계에서 세라믹의 표면 조건에 따른 접착 거동의 변화)

  • O, Seon-Mi;Kim, Jin-Seong;Lee, Chae-Hyun
    • Journal of Technologic Dentistry
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    • v.33 no.1
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    • pp.47-54
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    • 2011
  • Purpose: To investigate shear bonding strength between dental zirconia ceramics with different surface treatment and metal bracket. Methods: Zirconia ceramics(LAVA, 3M ESPE, USA) were divided to 4 groups according to their surface treatment; no surface treatment(G1), sand blasting(G2), silane coating(G3), and sand blasting+silane coating(G4). Specimens were bonded to metal bracket using resin bond($Transbond^{TM}XT$, 3M Unitek, USA). Shear bond strength was measured using universal test machine(3366 INSTRON. U.S.A) with cross head speed of 1 mm/min. Microstructural investigation for fracture surface was performed after shear test. Results: Shear bonding strengths of single surface treatment groups (G2 and G3) were higher than no treatment group(G1). Combined Treatment Group (G4) showed the highest shear bond strength of 9.15MPa. Microstructural observation shows that higher shear bonding strength was obtained when debonding was occurred at metal bracket/resin interface rather than zirconia ceramic/resin interface. Conclusion: Surface treatment of zirconia is necessary to obtain higher bonding strength. Combined treatment can be more effective when surface the surfaces are kept clean and homogeneous.