• Journal of the Korean institute of surface engineering
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• v.56 no.5
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• pp.299-308
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• 2023

In this study, phosphorus (P)-doped nickel cobaltite (P-NiCo₂O₄) and nickel-cobalt layered double hydroxide (P-NiCo-LDH) were synthesized on nickel (Ni) foam as a conductive support using hydrothermal synthesis. The thermal properties, crystal structure, microscopic surface morphology, chemical distribution, electronic state of the constituent elements on the sample surface, and electrical properties of the synthesized P-NiCo₂O₄ and P-NiCo-LDH samples were analyzed using thermogravimetric analysis-differential scanning calorimetry (TGA-DSC), X-ray diffraction (XRD), field-emission scanning electron microscopy (FE-SEM), energy dispersive X-ray spectroscopy (EDS), X-ray photoelectron spectroscopy (XPS), cyclic voltammetry (CV), galvanostatic charge-discharge (GCD), and electrochemical impedance spectroscopy (EIS). The P-NiCo₂O₄ electrode exhibited a specific capacitance of 1,129 Fg^-1 at a current density of 1 Ag^-1, while the P-NiCo-LDH electrode displayed a specific capacitance of 1,012 Fg^-1 at a current density of 1 Ag-1. When assessing capacity changes for 3,000 cycles, the P-NiCo₂O₄ electrode exhibited a capacity retention rate of 54%, whereas the P-NiCo-LDH electrode showed a capacity retention rate of 57%.

• Korean Journal of Applied Biomechanics
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• v.31 no.1
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• pp.72-78
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• 2021

Objective: The purpose of this study was to investigate relations and effectiveness about mountain climbling exercise with different level of support surfaces by analyzing heart rate and EMG data. A total of 10 male college students with no musculoskeltal disorder were recruited for this study. Method: The biomechanical analysis was performed using heart rate monitor (Polar V800, Polar Electro Oy, Finland), step-box, exercise mat, and EMG device (QEMG8, Laxtha Inc. Korea, sampling frequency = 1,024 Hz, gain = 1,000, input impedance > 1012 Ω, CMRR > 100 dB). In this research, step-box were used to create different surface levels on the upper body (flat surface, 10% of subject's height, 20% of subject's height, and 30% of subject's hight). Based on these different conditions, data was collected by performing mountain climbing exercise during 30 seconds. Subjects were given 5 minutes of break to prevent muscular fatigue after each exercise. For each dependent variable, a one-way analysis of variance with repeated measures was conducted to find significant differences and Bonferroni post-hoc test was performed. Results: The results of this study showed that exercise intensity was reduced statistically as increased surface level on the upper body. Muscle activity of the upper rectus abdominis and biceps femoris for 30% of surface level was significantly higher than the corresponding values for flat surface. However, the opposite was found in the rectus femoris. In general, muscle activity of the lower rectus abdominis, erector spinae, external oblique abdominis, and gluteus maximus increased when surface level increased, but the differences were not significant. Conclusion: As a result, the increase in surface level of the body would change muscle activity of the upper body, indicating that different surface level of the upper body may cause significant effect on particular muscles to be more active during mountain climbing exercise. Based on results of this study, it is suggested to set up an appropriate surface level to target particular muscle to expect an effective training. It is also important to set adequate surface levels to create an effective training condition for preventing exercise injuries.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.15 no.1
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• pp.32-38
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• 2014

In the present study, immersion corrosion characteristics of Zn and Al thermal spray coating with sealer for the seawater heat exchanger are experimentally investigated. Total 8 coating types of Zn and Al thermal spray coating with silicone and epoxy sealer were tested with immersion corrosion testing in $80^{\circ}C$ 3.5%w NaCl solution and compared the corrosion characteristics between each coatings. To investigate the corrosion characteristics of the specimens, AC impedance, SEM, and thermal diffusivity were acquired and analyzed. As a result, on the surface of the specimens with silicone and epoxy sealer, blister did not occurred, so the sealers might be effective at increasing the corrosion resistance of the specimens immersed in the NaCl solution.

• Plant Journal
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• v.16 no.3
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• pp.47-52
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• 2020

This study investigated the methodologies to enhance the corrosion resistance and the ways to measure for subsea equipment made of aluminum. The methodologies for the anticorrosion were cathodic protection, conversion coating, anodizing and organic coating. The simply analyzed ways to measure the corrosion resistance were Scanning Electron Microscope (SEM), Electrochemical Impedance Spectroscopy (EIS), Glow discharge optical emission spectrum spectroscopy (GD-OES), Fourier Transform Infrared Spectroscopy (FT-IR), Transmission Electron Microscopy (TEM), X-ray Photoelectron Spectroscopy (XPS), Scanning Vibrating Electrode Technique (SVET), contact angle and interfacial tension. The most widely used tools for increasing the corrosion resistance were the anodizing and the organic coating. Many ways were evenly used to measure corrosion. The methods more frequently utilized were SEM for the surface investigation and the contact angle to evaluate the corrosion resistance.

• Journal of the Korean Chemical Society
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• v.55 no.3
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• pp.495-501
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• 2011

The corrosion inhibitive nature of a flavonoid compound, 3-Hydroxy-7-methoxy-2-phenylchromen-4-one (HMPC), the synergistic effect between HMPC and n-Tetrabutylammonium bromide (TBAB) and their adsorption behavior on mild steel in hydrochloric acid solution were studied by weight loss, potentiodynamic polarization and electrochemical impedance spectroscopy (EIS) measurements. The results of weight loss study at different temperatures revealed that the inhibition efficiency increases with inhibitor concentration and decreases with increase in the temperature of the system. The electrochemical studies showed that the inhibitor acts through mixed mode of inhibition and the inhibitor molecules adsorb on the metal - solution interface forming a protective layer. The adsorption of the inhibitor molecules over the metal surface was supported by the obeyed Langmuir's adsorption isotherm, Scanning Electron Microscopic analysis (SEM) and Fourier Transform Infrared (FT-IR) spectroscopic studies.

• Journal of Biomedical Engineering Research
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• v.25 no.3
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• pp.165-169
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• 2004

In Magnetic Resonance Electrical Impedance Tomography (MREIT), we inject current through electrodes placed on the surface of a subject and measure the induced magnetic flux density distribution using an MRI scanner. This requires a constant current source whose output pulses are synchronized with MR pulse sequences. In this paper, we present a design and performance analysis of a current source used in a 3.0T MREIT system. The developed current source was tested using a saline phantom. We found that its performance is satisfactory for the current MREIT system. We suggest future improvements for better SNR(signal-to-noise ratio).

• Journal of Biomedical Engineering Research
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• v.29 no.6
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• pp.436-442
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• 2008

Magnetic resonance electrical impedance tomography(MREIT) has been suggested to produce cross-sectional conductivity images of an electrically conducting object such as the human body. In most previous studies, recessed electrodes have been used to inject imaging currents into the object. An MRI scanner was used to capture induced magnetic flux density data inside the object and a conductivity image reconstruction algorithm was applied to the data. This paper reports the performance of a thin and flexible carbon-hydrogel electrode that replaces the bulky and rigid recessed electrode in previous studies. The new carbon-hydrogel electrode produces a negligible amount of artifacts in MR and conductivity images and significantly simplifies the experimental procedure. We can fabricate the electrode in different shapes and sizes. Adding a layer of conductive adhesive, we can easily attach the electrode on an irregular surface with an excellent contact. Using a pair of carbon-hydrogel electrodes with a large contact area, we may inject an imaging current with increased amplitude primarily due to a reduced average current density underneath the electrodes. Before we apply the new electrode to a human subject, we evaluated its performance by conducting MREIT imaging experiments of five swine legs. Reconstructed conductivity images of the swine legs show a good contrast among different muscles and bones. We suggest a future study of human experiments using the carbon-hydrogel electrode following the guideline proposed in this paper.

• Proceedings of the Materials Research Society of Korea Conference
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• 2011.05a
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• pp.42.2-42.2
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• 2011

$TiO_2$ films were modified by adding a glass frit as a light scattering particle and applied to an anode electrode in dye-sensitized solar cells (DSSCs) to enhance the adhesion between $TiO_2$ and fluorine doped transparent oxide (FTO). Low melting point glass frits at contents of (3 to 7wt%) were added to the nano crystalline $TiO_2$ films. The light scattering properties, photovoltaic properties and microstructures of the photo electrodes were examined to determine the role of the low glass transition temperature ($T_g$) glass frit. Electrochemical impedance spectroscopy, Brunauer-Emmett-Teller method and scratch test were conducted to support the results. The DSSC with the $TiO_2$ film containing 3wt% low Tg glass frit showed optimal performance (5.1%, energy conversion efficiency) compared to the $TiO_2$-based one. The photocurrent density slightly decreased by adding 3wt% of the frit due to its large size and non conductivity. However, the decrease of current density followed by the decrease of electron transfer due to the large frit in $TiO_2$ electrode was compensated by the scattering effect, high surface area and reduced the electron transfer impedance at the electrolyte-dye-$TiO_2$ interface. The stability of the photo electrodes was improved by the frit, which chemically promoted the sintering of $TiO_2$ at relatively low temperature ($450^{\circ}C$).

• Journal of the Institute of Electronics Engineers of Korea SC
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• v.38 no.5
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• pp.23-32
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• 2001

Electrical impedance tomography (EIT) is a relatively new imaging modality in which the resistivity (conductivity) distribution of the unknown object is estimated based on the known sets of injected currents and measured voltages on the surface of the object. In this paper, we propose a dynamical EIT reconstruction algorithm based on the regularized extended Kalman filter(EKF). The EIT inverse problem is formulated as dynamic equation which consists of the slate equation and the observation equation, and the unknown state(resistivity) is estimated recursively with the aid of the EKF. In doing so, the generalized Tikhonov regularization technique is employed in the cost functional to mitigate the ill-posedness characteristics of the inverse problem. Computer simulations for the 16-channel synthetic data are provided to illustrate the reconstruction performance of the proposed algorithm.

• Journal of IKEEE
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• v.5 no.2 s.9
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• pp.153-163
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• 2001

Electrical impedance tomography(EIT) is a relatively new imaging modality in which the internal impedivity distribution is reconstructed based on the known sets of injected currents and measured voltages on the surface of the object. We describe a dynamic EIT imaging technique for the case where the resistivity distribution inside the object changes rapidly within the time taken to acquire a full set of independent measurement data. In doing so, the inverse problem is treated as the state estimation problem and the unknown state (resistivity) is estimated with the aid of extended Kalman filter in a minimum mean square error sense. In particular, additional electrodes are attached to the known internal structure of the object to enhance the reconstruction performance and modified Tikhonov regularization technique is employed to mitigate the ill-posedness of the inverse problem. Computer simulations are provided to illustrate the reconstruction performance of the proposed algorithm.