• 제목/요약/키워드: Surface Properties Test

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Mechanical Properties and Surface Characteristics of Ti-25Ta-xHf Alloys

  • Park, Seon-Yeong;Kim, Jeong-Jae;Choe, Han-Cheol
    • 한국표면공학회:학술대회논문집
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    • 한국표면공학회 2014년도 추계학술대회 논문집
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    • pp.187-187
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    • 2014
  • In this study, we investigated mechanical properties and surface characteristics of Ti-25Ta-xHf alloys. The samples were manufactured for composition of Ti-25Ta-xHf(x=0 to 15 wt. %) alloys. Each alloy was melted twenty times in an arc-melting vacuum furnace. The microstructural phases and phase transformation of Ti-25Ta-xHf alloys were identified with the aid of an XRF, XRD and DSC. And mechanical properties were investigated using Vickers hardness, nanoindentation, and tensile test.

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비대칭 마크네트론 스퍼터링을 이용한 이리듐 산화물 박막의 합성과 전기 화학적 특성분석 (Electro-Chemical Properties of Iridium Oxide Coated Ti Electrode Synthesized by Unbalanced Magnetron Sputtering Process)

  • 김성대;김상식;송진호
    • 한국표면공학회지
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    • 제40권5호
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    • pp.203-208
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    • 2007
  • Preliminary studies were conducted to develop a dimensionally stable anode (DSA)electrode prepared by reactive sputtering method. The microstructure, surface morphology and electrochemical properties of iridium oxide $(IrO_2)$ coatings synthesized by unbalanced magnetron sputtering (UBMS) and conventional DSA electrode were compared. In addition, the possibilities of $IrO_2$ films synthesized by UMB on a real DSA electrode were investigated by electro-chemical application test. The degree of non-stoichiometry and surface area were closely related to the electro-chemical activity of the $IrO_2$ electrode. The feasibility of making a DSA electrode prepared by PVD technique was demonstrated through the present work.

준설매립된 해성점성토에서 시멘트계 고화재를 이용한 표층개량 (The Improvement of Surface Layer Using Cement-hardening Agents in Dredged and Reclaimed Marine Clay)

  • 남정만;윤중만
    • 한국해양공학회지
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    • 제18권4호
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    • pp.46-51
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    • 2004
  • The surface layer in dredged and reclaimed marine clay is improved by mixing of shallow soils and hardening agents, which is made of cement, containing some other special admixtures. Tests in both laboratory and field settings are performed to investigate the improvement effect and strength properties of cement-stabilized soils. The test results show that the hardening agent sufficiently improves the soil properties of the surface layer, while increasing the load-carrying capacity. The strength of cement-stabilized soils depends, primarily, on water-to-cement ratio and curing temperature. That is, the higher curing temperature and the longer curing time, the higher the strength in cement-stabilized soils. The high ratio of water-ta-cement results in a lower strength.

비대칭 스퍼터링에 의한 TiAIN/CrN 나노 다층 박막의 합성 및 특성 분석에 관한 연구 (Studies on the Development of TiAIN/CrN Multi-layered Thin Films by Unbalanced Magnetron Sputtering Process)

  • 김광석;김범석;이상율
    • 한국표면공학회지
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    • 제38권6호
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    • pp.207-211
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    • 2005
  • In this work a multi-layered nanostructured TiAIN/CrN superlattice coatings was synthesized using closed-field unbalanced magnetron sputtering method and the relationships between their superlattice period (1), micro-structure, hardness and elastic modulus were investigated. In addition, wear test at $500^{\circ}C$ and oxidation resistance test at $900^{\circ}C$ were performed to investigate high temperature properties of these thin films. The coatings were characterized in terms of microstructure and mechanical properties by transmission electron microscopy (TEM) and nano-indentation test. Results from TEM analysis showed that superlattice periods was inversely proportional to the jig rotation speed. The maximum hardness and elastic modulus of 37 GPa and 375 GPa were observed at superalttice period of 6.1 nm and 4.4 nm, respectively. An higher value of microhardness from TiAIN/CrN thin films than either TiAIN (30 GPa) or CrN (26 GPa) was noted while the elastic modulus was approximately an average of TiAIN and CrN films. These enhancement effects in superlattice films could be attributed to the resistance to dislocation glide across interface between the CrN and TiAIN layers. Much improved plastic deformation resistance ($H^3/E^2$) of 0.36 from TiAIN/CrN coatings was observed, compared with 0.15 and 0.16 from TiAIN and CrN, respectively. Also the wear resistance at $500^{\circ}C$ was largely increased than those of single TiAIN and CrN coatings and TiAIN/CrN coatings showed much reduced weight gain after exposure at $900^{\circ}C$ for 20 hours.

수분열화에 의한 에폭시절연재료의 표면특성에 관한 연구 (A Study on the Surface Properties of Epoxy Insulator by Water Degradation)

  • 임경범;이백수;김종택;정무영;황명환;이덕출
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1998년도 춘계학술대회 논문집
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    • pp.199-202
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    • 1998
  • In examining application of polymer as electrical insulators, it is very important to perform accelerated aging test substituted the process which polymer insulator is degraded for long-time by the process of short-time. The purpose of this paper is to examine the properties of water degradation which affect on the efficiency of epoxy insulator. To do this, the surface properties on epoxy insulating material have been investigated after long-time accelerated degradation in boiling water condition. The experimental results showed the contact angle and surface resistivity after treatment to decrease the sample of water treatment. In dielectric properties, dielectric constant was increased by the aging development with water treatments.

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Surface Integrity and Tribological Properties of Machined Surfaces

  • Kim, Dae-Eun;Hwang, Dong-Hwan
    • Tribology and Lubricants
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    • 제11권5호
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    • pp.31-39
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    • 1995
  • The surface integrity of a machined surface is an important factor that dictates several performance characteristics of a metal part. In this paper, the surface integrity aspects are presented specifically with respect to the tribological properties of steel. Test specimens were prepared under varying conditions to induce different levels of surface deformation and hardness. Sliding and rolling experiments were performed to assess the friction and wear characteristics of these specimens using a pinon-disk type tribotester and a plate-on-ball type set-up. It is reaffirmed that heat treated steels possess superior sliding and rolling fatigue resistance than raw steel. However, for the case of raw steels machined under varying conditions, the harder specimen resulted in higher wear. This result is attributed to the presence of surface cracks that were induced during machining. The results of such findings will aid in the optimization of surface preparation process for tribological applications of steel.

반도전성 실리콘 고무의 플라즈마 표면처리에 따른 접착특성과 절연성능 (Adhesion and Electrical Performance by Plasma Treatment of Semiconductive Silicone Rubber)

  • 황선묵;이기택;홍주일;허창수
    • 한국전기전자재료학회논문지
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    • 제18권5호
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    • pp.450-456
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    • 2005
  • In this paper, the effect of adhesion properties of semiconductive-insulating interface layer of silicone rubber on electrical properties was investigated. The modifications produced on the silicone surface by oxygen plasma were accessed using ATR-FTIR, contact angle and Surface Roughness Tester. Adhesion was obtained from T-peel tests of semiconductive layer haying different treatment durations. In addition, ac breakdown test was carried out for elucidating the change of electrical property with duration of plasma treatment. From the results, the treatment in the oxygen plasma produced a noticeable increase in surface energy, which can be mainly ascribed to the creation of O-H and C=O. It is observed that adhesion performance was determined by surface energy and roughness level of silicone surface. It is found that at dielectric strength was increased with improving the adhesion between the semiconductive and insulating interface.

Study on Hygrothermal Degradation and Corrosion Protection of Epoxy Coatings Cured by Different Amine Based Curing Agents

  • Shon, Min-Young;Kwon, Huck-Sang
    • Corrosion Science and Technology
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    • 제9권5호
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    • pp.201-208
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    • 2010
  • Epoxy coatings cured by different amine based curing agents have been prepared. Atomic force microscopy (AFM) has been used to monitor the surface topology changes of epoxy coatings before and after hygrothermal cyclic test. The glass transition temperature ($T_g$) and coefficient of thermal expansion (CTE) of the epoxy coating were measured by Thermo-mechanical Analysis (TMA). The Electrochemical impedance spectroscopy (EIS) with hygrothermal cyclic test has been introduced to evaluate the corrosion protection of the epoxy coatings. In conclusion, thermal properties of epoxy coatings were in good agreement with the results of corrosion protection of epoxy coated carbon steel obtained result by EIS with hygrothermal cyclic test. The relationship between thermal properties, surface roughness changes and corrosion protection of epoxy coatings are discussed in this study.

SCMH2 고속회전축재의 표면처리조건에 따른 VHCF 피로특성에 관한 연구 (VHCF Characteristics of SCMH2 Steel Depending on the Surface Treatment Conditions)

  • 서창민;서창희;서민수
    • Journal of Welding and Joining
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    • 제31권4호
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    • pp.47-53
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    • 2013
  • SCMH2 steel is widely used in the industrial members of car and tractor. This study focused on material properties and evaluation technology of the SCMH2 steel regarding the surface treatment followed by carburizing and nitriding, by means of impact test, hardness test. and fatigue test including HCF (high cycle fatigue) and VHCF (very high cycle fatigue). Drop weight impact tester (Instron, 9250 Hv) and Cantilever type rotating-bending fatigue tester (YRB200, 3150 rpm) were used to characterize the SCMH2 standard specimen before and after carburizing/nitriding. In order to understand those effects on fatigue characteristics and material properties, the fractured surfaces were carefully observed and analyzed by SEM (scanning electron microscope) and EDS (energy-dispersive X-ray spectroscopy).

A Study on Surface Treatment for Rubber Materials with Low Friction Factor

  • Li, Xiang-Xu;Cho, Ur Ryong
    • Elastomers and Composites
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    • 제51권1호
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    • pp.43-48
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    • 2016
  • Multi-Surface (MS) treatment is a new technique of surface treatment to reduce the static friction factor on the surface of rubber. MS treatments include 4 methods which names are MS-V (UV-irradiation on the rubber surface), MS-M (doing the chemical reaction with double bond of rubber), MS-Q (dilution of rubber surface by silicone surfactant), and MS-P (coating and heating of rubber surface). The experiment and test of every MS-treatment had been carried out using acrylonitrile-butadiene rubber (NBR), ethylene-propylene-diene rubber (EPDM), and chlorosulphonated rubber (CSM) as rubber materials. It had introduced the steps of every MS-treatment process and the result of the properties test. From the research, it was found that the best method was MS-V treatment because it suited all the samples and the effect was obviously.