• Title/Summary/Keyword: Structural Synthesis

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Synthesis of SiC by Self-Propagating High Temperature Synthesis Chemical Furnace (SHS화학로에 의한 SiC의 합성)

  • Kim, Do-Kyung;Park, Sung;Cho, Kurn;Lee, Hyung-Bock
    • Journal of the Korean Ceramic Society
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    • v.31 no.11
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    • pp.1283-1292
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    • 1994
  • Ultra-fine $\beta$-SiC powders were fabricated by self-propagating high temperature synthesis process (SHS) using chemical furnace. The dependences of the C powders with different surface areas, the molar ratios of C/Si, the weight ratios of chemical fuel content, and pellet diameter-size on synthesis were investigated. Compositional and structural characterization of these powders was carried out by scanning electron micrograph and X-ray diffraction. The $\beta$-SiC powders which had C/Si mole ratio=1.05, 3 times chemical fuel contents, and pellet diameter=20 mm were optimum for synthesis efficiency. By optimizing process-variables, it is possible to fabricate $\beta$-SiC powders which have little secondary phases ($\alpha$-SiC).

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Structural Dynamic Analysis using Multi-FRF Synthesis Method (다중전달 함수합성법을 이용한 구조물의 동특성 해석)

  • 정재훈;지태한;박영필
    • Journal of KSNVE
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    • v.8 no.1
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    • pp.139-145
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    • 1998
  • A great deal of effort has been invested in upgrading the performance and the efficiency of dynamic analysis of mechanical structures. Using experimental modal analysis(EMA) or finite element analysis(FEA) data of mechanical structures, the performance and efficiency can be effectively evaluated. In order to analyze complex structures such as automobiles and aircrafts, for the sake of computing efficiency, the dynamic substructuring techniques that allow to predict the dynamic behavior of a structure are widely used. Through linking a modal model obtained from EMA and an analytical model obtained from FEA, the best conditioned strucutres can be proposed. In this study, a new algorithm of substructre synthesis method, Multi-FRF synthesis method, is proposed to analyze a structure composed of many substructures.

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Synthesis and Structural Properties of YBa2Cu3O7-x Films/ZnO Nanorods on SrTiO3 Substrates

  • Jin, Zhenlan;Park, C.I.;Song, K.J.;Han, S.W.
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.08a
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    • pp.169-169
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    • 2012
  • The high-temperature superconductor YBa2Cu3O7-x (YBCO) have attached attentions because of a high superconducting transition temperature, low surface resistance, high superconducting critical current density (Jc), and superior superconducting capability under magnetic field. Moreover, the Jc of YBCO superconductors can be enhanced by adding impurities to the YBCO films for vortex-pinning. Understanding and controlling pinning centers are key factors to realize high Jc superconductors. We synthesized vertically-aligned ZnO nanorods on SrTiO3 (STO) substrates by catalyst-free metal-organic chemical vapor deposition (MOCVD), and subsequently, deposited YBCO films on the ZnO nanorods/STO templates using pulsed laser deposition (PLD). The various techniques were used to analyze the structural and interfacial properties of the YBCO/ZnO nanorods/STO hybrid structures. SEM, TEM, and XRD measurements demonstrated that YBCO films on ZnO nanorods/STO were well crystallized with the (001) orientation. EXAFS measurements from YBCO/ZnO nanorods/STO at Cu K edge demonstrated that the local structural properties around Cu atoms in YBCO were quite similar to those of YBCO/STO.

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Frequency Window Method for the Vibration of Secondary Structural Systems (Frequency Window Method에 의한 Secondary 구조 시스템의 진동특성)

  • ;Igusa, Takeru;Achenbach, Jan D.
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 1991.04a
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    • pp.153-158
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    • 1991
  • Recently, demands on light weight, high strength, and low noise or vibration have led to the design of complicated structural systems. Although finite elements [1], mode synthesis [2], and statistical energy analysis [3] can be used to compute the dynamic response of such systems, the structural complexity has made the interpretation of the results of such analysis difficult. Many researchers in dynamic analysis have sought to further develop existing theories or develop alternate methods to obtain greater insight in the behavior of large massive primary systems (P systems) with connected light secondary systems (S systems). Some recent research includes work by Sackman and Kelly [4], Sackman et al.[5], Der Kiureghian et al.[6], and Igusa and Der Kiureghian [7-9] who have combined mode synthesis concepts, matrix algebraic theory, and perturbation methods for characterizing weakly-coupled structural systems. A major limitation of these works are that they are limited to lumped mass S systems. In this paper, the general ideas in the Refs.[4-9] are used to study continuous S systems and the method to reduce the complexity, studied in the works by Igusa, Achenbach, and Min [10,11], is developed into the frequency window method.

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Low-temperature Synthesis of (TiC+Al2O3) Reinforced Al Matrix Composite Based on Self-combustion Reaction (자발연소반응을 이용한 (TiC+Al2O3)/Al 복합재료의 저온합성)

  • Lee, Jung-Moo;Kim, Su-Hyeon;Cho, Young-Hee;Kim, Je-Woo;Lee, Jae-Chul
    • Korean Journal of Metals and Materials
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    • v.49 no.12
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    • pp.1001-1004
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    • 2011
  • The formation of TiC and $Al_2O_3$ particles based on the self-combustion reaction of the $Al-TiO_2-C-CuO$ system in an Al alloy melt was investigated. With an adequate amount of CuO in the system, a spontaneous reaction occurred within the Al alloy melt at $850^{\circ}C$ and thereafter was self-maintained, producing an Al matrix composite reinforced with thermodynamically stable TiC and $Al_2O_3$ particles. TiC and $Al_2O_3$ particles contributed to a considerable increase in the strength and stiffness, demonstrating the feasibility of this method as a practical application for structural parts.

Partitioned structural eigenvalue analysis (부분 구조물 합성으로 이루어진 고유치 문제 해석)

  • Jung, Eui-Il;Na, Hye-Joong;No, Suk-Hong;Chun, Du-Hwan
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2005.05a
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    • pp.117-119
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    • 2005
  • For large structural eigen-analysis, the whole structure is divided into some partitioned structures and through synthesis of partitioned structural model the eigen-data of structure can be obtained. In that case, eigenvalue problem consists of semidefinite mass matrix form because of displacement constraint condition. In this work the eigenvalue problem is considered by means of several method, determinant search and null space reduction method.

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