• 비파괴검사학회지
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• 제20권6호
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• pp.562-567
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• 2000

발전 및 산업설비에 사용되는 많은 압력용기는 저합금강을 사용하여 제작되고 있다. 압력용기의 내면은 부식이 미치는 영향을 최소화하기 위하여 오스테나이트계 스테인리스강으로 덧살용접을 하고 있으나, 용접층간의 계면에서 발생하고 있는 박리균열은 압력용기의 신뢰성에 중요한 변수가 되고 있다. 본 연구에서는 DSP를 사용하여 오버레이 용접부를 고속으로 검사할 수 있는 C-scan 시스템을 개발하였다. 본 시스템은 신호 처리부 (오실로스코프, 펄서/리시버, 디지타이저, DSP), 스캐너, 프로그램 및 위치 제어부로 구성되어 있다. 개발된 시스템을 사용하여 실제 오버레이 용접부에 대한 초음파검사를 실시한 결과 고속으로 신뢰성 높은 검사결과를 얻을 수 있었다.

• Corrosion Science and Technology
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• 제18권4호
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• pp.148-153
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• 2019

Pure nickel with a thickness of 1 mm was plated on type 304 stainless steels and low alloy steels (JIS G3131 SPHC) by electrolytic plating method in a circulating plating bath. Plating performance, mechanical properties, and surface characteristics were evaluated in terms of pretreatment process, anode material, pH, current density, and flow rate of the plating solution. Addition of hydrochloric acid during pre-treatment process improved the adhesion performance of plating. To improve plating efficiency, it is desirable to use S-nickel rather than electrolytic nickel. The use of S-nickel was also confirmed to be desirable for maintaining the pH and concentration of the plated solution. The defect of the plating using S-nickel anode produced pit on the surface. However, it is believed that proper control can be obtained by increasing the flow rate. Internal stress and hardness values of electrolytic nickel plating according to current density need to be carried out with further studies.

• 대한금속재료학회지
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• 제46권11호
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• pp.708-712
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• 2008

The influence of high temperature gas nitriding (HTGN) in STS347 and STS310S steels was experimentally investigated. The HTGN was carried out at $1,050^{\circ}C{\sim}1,150^{\circ}C$ for 10 hrs in a gaseous atmosphere containing $1kg/mm^2$ of nitrogen. After HTGN, fine precipitates of $Cr_2N$ and NbN appeared in austenite on the surface of STS 347, while nitrogen pearlite, which was layeredof $Cr_2N$ and austenite alternatively, appeared in austenite on the surface of STS 310S. The surface hardness of HTGN-treated, STS 347 and STS 310S specimens was 250~360 Hv and 270~400 Hv, respectively, depending on the temperature of HTGN. The nitrogen content was analyzed 1.4 wt% and 1.6 wt% at the surface layer of STS 347 and STS 310S steels, respectively. In addition, an improvement in the corrosion resistance of HTGN treated specimens was observed.

• Journal of Welding and Joining
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• 제28권3호
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• pp.92-98
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• 2010

Ferritic stainless steels, which have relatively small thermal expansion coefficient and excellent corrosion resistance, are increasingly being used in vehicle manufacturing, in order to increase the lifetime of exhaust manifold parts. But, there are limits on use because of the problem related to cosmetic resistance, corrosions of condensation and high temperature salt etc. So, Aluminum-coated stainless steel instead of ferritic stainless steel are utilized in these parts due to the improved properties. In this investigation, Al-8wt% Si alloy coated 409L ferritic stainless steel was used as the base metal during Gas Tungsten Arc(GTA) welding. The effects of coated layer on the microstructure and hardness were investigated. Full penetration was obtained, when the welding current was higher than 90A and the welding speed was lower than 0.52m/min. Grain size was the largest in fusion zone and decreased from near HAZ to base metal. As welding speed increased, grain size of fusion zone decreased, and there was no big change in HAZ. Hardness had a peak value in the fusion zone and decreased from the bond line to the base metal. The highest hardness in the fusion zone resulted from the fine re-precipitation of the coarse TiN and Ti(C, N) existed in the base metal during melting and solidification process and the presence of fine $Al_2O_3$ and $SiO_2$ formed by the migration of the elements, Al and Si, from the melted coating layer into the fusion zone.

• 열처리공학회지
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• 제20권2호
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• pp.84-93
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• 2007

Microstructural changes during tempering at the temperature range of $300^{\circ}C{\sim}700^{\circ}C$ for the nitrogen-permeated STS 410 and 410L martensitic stainless steels has been investigated. After nitrogen permeation at temperature between 1050 and $1150^{\circ}C$, the surface layer appeared fine $Cr_2N$ of square and rod types in the martensite matrices. Hardness of the nitrogen-permeated surface layer represented 680Hv and 625Hv, respectively, for 410 and 410L steels. It is considered that the fine homogeneously dispersive effect of precipitates by nitrogen caused the increased hardness. Due to the counter current effect of carbon from interior to surface during nitrogen diffusion from surface to interior, the 0.1%C alloyed 410 steel showed the low nitrogen content of 0.025% compared with 0.045% of 410L steel at the distance of $100{\mu}m$ from the surface. Tempering of nitrogen-alloyed 410 and 410L showed the maximum hardness at $450^{\circ}C$. This maximum hardness was considered to be the secondary hardening effect of very fine carbide and nitride. The decrease in hardness at $700^{\circ}C$ was the softening effect of the matrix due to the precipitation of many needle-shaped $Cr_2N$ for 410 steel and the precipitation of coarse nitride of $Cr_2N$ in line with the spherical precipitates with directionality for 410L steel. For 410 steel, the corrosion resistance of nitrogen permeated surface in the solution of 1 N $H_2SO_4$ were nearly unchanged, however the superior corrosion resistance was obtained for nitrogen permeated 410L steel compared to the solution annealed condition.

• 한국신재생에너지학회:학술대회논문집
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• 한국신재생에너지학회 2010년도 춘계학술대회 초록집
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• pp.137.2-137.2
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• 2010

본 연구는 스테인리스 스틸(STS)을 직접메탄올 연료전지(DMFC)용 바이폴라 플레이트에 적용하기 위한 것이다. 약산성의 연료전지 환경에서 부식저항성을 향상시키고자 오스테나이트계 STS 316L과 페라이트계 STS 430에 UBM(unbalanced magnetron) DC sputter로 CrN 코팅막을 제작하였다. CrN이 코팅된 스테인리스 스틸은 부식특성, 접촉 저항 및 접촉각 등을 측정하여 무 코팅의 스테인리스 스틸과 특성을 비교하였다. 그리고 이들 재료의 연료전지(DMFC) 적용 가능성을 알아보기 위하여 단위전지로 제작하여 연료전지 성능 등을 측정하고 평가하였다. 무 코팅 스테인리스 스틸(STS 316L, STS 430)과 CrN 코팅 스테인리스 스틸의 부식저항 특성은 동전위와 정전위 실험으로 조사하였다. 동전위 부식 실험은 -0.4~1.0 V로 0.001 M의 황산용액 또는 메탄올을 첨가하여 질소 또는 공기의 환경에서 실험을 실시하였으며, 정전위 부식 실험은 0.4 V 또는 0.6 V에서 진행하였다. 연료전지의 단전지 측정은 실제 DMFC의 운전조건에서 실시하였다. 부식실험과 단전지 실험 전/후 메탈 바이폴라 플레이트의 조직 변화는 SEM을 통해 관찰하였고, 부식산화물의 화학적 조성과 메탈 바이폴라의 표면은 EDS를 이용하여 측정하였다.

• 동력기계공학회지
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• 제8권3호
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• pp.30-35
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• 2004

In the steel making industries, the continuous casting process has been applied to the number of company because of its economical benefit. Casting rolls are utilized for frictional drive and transport of solidifying slap. Dimensional tolerances, mechanical stability and surface condition of the cast roll can affect both the surface and internal quality of the product being cast. To overcome these problems, the industry is accelerating on the rate of technology improvements. Samples were overlaid on the S45C steel by submerged arc welding process. And the hardness, wear, electrochemical corrosion and oxidation tests were carried out. Test results were that all these materials were satisfying basic requirements of caster rolls. By these results, the addition of 0.1%Nb and 0.15%V increase mechanical properties and tempering resistance by its superior carbide forming characteristics in low carbon $12{\sim}13%Cr$ martensitic stainless steels.

• Journal of Welding and Joining
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• 제14권5호
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• pp.122-133
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• 1996

In order to evaluate the cryogenic fracture characteristics of structural steels for superconducting magnets of fusion reactor, small punch (SP) testing was performed on austenitic stainless steel (JN1 base metal) and its TIG weldments at 293K, 77K and 4K. The mechanical properties with respect to the extracted location of the weld metal, on the effects of welding heat cycle about base metal near fusion line in TIG weldments were investigated. The mechanical property of the weld metal in TIG weldments depends on distance from welding root, root region of weldments having the lowest mechanical property. The base metal near fusion line showed degradation of mechanical property caused by cyclic heating during the TIG welding. Based on the test results, HAZ was found to be up to 5mm from the fusion line. It is shown that SP testing is a useful tool to evaluate the mechanical properties with respect to the microstructures changes such as HAZ as well as weld metal in TIG weldments at cryogenic temperature.

• Journal of Welding and Joining
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• 제15권4호
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• pp.136-142
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• 1997

In this study, the amorphous foil filler, thickness of 20 - $20~30\mu\textrm{m}$ was made to develop Cu-7.5wt%Mn-7.5wt%Si insert alloy(melting point temperature : solidus line 1003K, liquidus line 1070K). Liquid phase diffusion bonding of 304 stainless steels (STS304), is carried out successfully by using developed Cu-7.5Mn-7.5Si insert alloy. Bonding conditions are taken from bonding pressure of 5MPa, bonding temperatures from 1073K to 1423K varied within 50K and brazing holding times of 0, 30, 60 and 240 minutes. As the results, the tensile strength in the liquid phase diffusion bonding is a little bit lower than that in the solid phase diffusion bonding. The authors find out that the liquid phase diffusion bonding needs lower bonding pressure than the others. Therefore, the liquid phase diffusion bonding had an excellent brazability in which the bonding process showed the typical mechanism of diffusion bonding. In corresponding, the new developed insert alloy of low melting pointed Cu-7.5Mn-7.5Si makes possible brazing between the STS304.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 2005년도 춘계학술대회 논문집
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• pp.1560-1565
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• 2005

Laser beam welding is increasingly being used in welding of structural steels. The laser welding process is one of the most advanced manufacturing technologies owing to its high speed and deep penetration. The thermal cycles associated with laser welding are generally much faster than those involved in conventional arc welding processes, leading to a rather small weld zone. Experiments are performed for 304 stainless steel plates changing several process parameters such as laser power, welding speed, shielding gas flow rate, presence of surface pollution, with fixed or variable gap and misalignment between the similar and dissimilar plates, etc. The following conclusions can be drawn that laser power and welding speed have a pronounced effect on size and shape of the fusion zone. Increase in welding speed resulted in an increase in weld depth/ aspect ratio and hence a decrease in the fusion zone size. The penetration depth increased with the increase in laser power.