• Title/Summary/Keyword: Shrinkage solution

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Properties of Bentwood for Esthetic Designing by Microwave and Ammonia Solution Treatment

  • Lee, Won-Hee;Bae, Hyun-Mi
    • Journal of the Korea Furniture Society
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    • v.18 no.4
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    • pp.275-281
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    • 2007
  • This study was carried out to know bending process property of bentwood by treatment methods such as microwave and ammonia solution treatment. Bentwood processing was operated on bending-jig form with 60mm and 100mm radius of curvature (ROC). The species was used to Korean red pine (Pinus densiflora). No significant difference was shown in bentwood processing method on ROC. In treatment method, ammonia solution treatment for bentwood was better in dimensional stability and working ability than that of microwave treatment. However, bentwood stress was reduced with ammonia solution treatment. Color of bentwood surface appearance has a dark tendency in ammonia solution treatment. But it seems to beautiful effect of apparent annual ring is rising esthetically by ammonia solution treatment. To utilize wood as a exterior material for living amenity, it has to be closely examined from various angles including surface property, degree of swelling and shrinkage, drying state, retaining strength, durability, safety, and insect damage.

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Sintering Behavior of Ultra-fine Hydroxyapatite Powders Synthesized by Hydrothermal Reaction (수열반응으로 합성한 Hydroxyapatite 초미분말의 소결특성)

  • 최재웅;조성원;최상홀
    • Journal of the Korean Ceramic Society
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    • v.31 no.11
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    • pp.1265-1270
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    • 1994
  • Ultra-fine hydroxyapatite powder were synthesized by the hydrothermal reaction at 10 atm, 3 hrs of Ca(OH)2 suspension with (NH4)2HPO4 solution, and were characterized sintering behavior. Sintered bodies of hydroxyapatite powders which synthesized by hydrothermal reaction method has less weight loss, less sintering shrinkage and superior mechanical property, and was more dense than sintered bodies of hydroxyapatite powder which synthesized by wet method. Sintered bodies were hydroxyapatite single phase. When soack in Ringer's solution for 2 weeks, hydroxyapatite powders preserved hydroxyapatite and sintered body absorbed trace of Ca2+ ion with soaked time.

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Preparation of Silica Glass using TMOS Solution (TMOS 용액을 이용한 실리카 유리의 제조)

  • 서정민;신대용;한상목
    • Journal of the Korean Ceramic Society
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    • v.28 no.4
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    • pp.324-328
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    • 1991
  • Monolithic silica gel and glass were prepared from TMOS solution with high concentration of HCl. Appearance of the dried gels and gelation time varied with content of HCl and H2O were observed in the TMOS-CH3OH-HCl-H2O system. The conversion from gel to glass during heat treatment stage was investigated using TG-DTA, XRD, IR and SEM and characteristics of the gel were examined by measuring bulk density, linear shrinkage and Vicker's hardness. A transparent silica glass was prepared from the gel after heat treatment at 1050℃.

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Vitrification solution without sucrose for cryopreservation in mouse blastocysts

  • Joo, Jong Kil;Lee, Young Ju;Jeong, Ju Eun;Kim, Seung Chul;Ko, Gyoung Rae;Lee, Kyu Sup
    • Clinical and Experimental Reproductive Medicine
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    • v.41 no.3
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    • pp.115-119
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    • 2014
  • Objective: This study was designed to investigate the survival rate of vitrified mouse blastocysts depending on the presence or absence of sucrose in vitrification solution. Methods: Mouse two-cell embryos were collected and cultured to blastocysts. Two vitrification solutions were prepared. The control solution was composed of 25% glycerol, 25% ethylene glycol, and 0.5 M sucrose (G25E250.5S) containing 2.5 mL glycerol, 2.5 mL ethylene glycol, 2 mL SSS, and 0.855 g sucrose in 5 mL PB1. The experimental solution was composed of 25% glycerol and 25% ethylene glycol (G25E25) and contained 2.5 mL glycerol and 2.5 mL ethylene glycol in 5 mL PB1. Artificial shrinkage was conducted by aspirating the blastocoelic fluid using an ICSI pipette. To examine the effect of sucrose in the vitrification solution on the survival rate of mouse blastocysts, the shrunken-equilibrated blastocysts were rehydrated or vitrified after being exposed to one of the two vitrification solutions. After exposure and the vitrification-thawing process, the re-expansion rate and hatching rate were evaluated after 6 hours of in vitro culture. Results: The re-expansion rate of mouse blastocysts exposed to vitrification solution with and without sucrose were not different in the experimental solution (without sucrose) (98%) and the control solution (with sucrose) (92%) (p>0.05). The hatching rate was higher in the experimental solution (95%) than in the control solution (88%), but did not differ across two treatments (p>0.05). The re-expansion rate of mouse blastocysts vitrified in the control solution was 92% and 94%, respectively (p>0.05), and the hatching rate was higher in the experimental solution (90%) than in the control solution (74%) (p<0.05). Conclusion: Sucrose need not be added in vitrification solution for freezing of artificially shrunken mouse blastocysts.

Effect of Ti, B, Zr Elements on Grain Refinement and Castability of Al-4wt%Mg-0.9wt%Si-0.3wt%Mn-0.15wt%Fe Casting Alloy (주조용 Al-4wt%Mg-0.9wt%Si-0.3wt%Mn-0.15wt%Fe 합금의 결정립 미세화와 주조특성에 미치는 Ti, B, Zr 첨가원소의 영향)

  • Kim, Heon-Joo;Park, Su-Min
    • Journal of Korea Foundry Society
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    • v.35 no.5
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    • pp.120-127
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    • 2015
  • The effects of Ti, B and Zr on grain refinement and castability were investigated in Al-4wt%Mg-0.9wt%Si-0.3wt%Mn-0.15wt%Fe alloy. Measurement of cooling curve and micro-structure observation were performed to analyze the effects of the addition of minor elements Ti, B and Zr during solidification. The prominence of effect on grain refinement was in increasing order for Ti, Zr and B element. Fine grain size and an increase of the crystallization temperature for ${\alpha}$-Al solution were evident as the amount of addition elements increased in this study. Addition of 0.15wt% Ti was most effective for grain refinement, and the resulting grain size of ${\alpha}$-Al solution for shell mold and steel mold were $72.3{\mu}m$ and $23.5{\mu}m$, respectively. Fluidity and shrinkage tests were perform to evaluate the castability of the alloy. Maximum fluidity length and minimum ratio of micro shrinkage were recorded for 0.15wt% Ti addition due to the effect of the finest grain size.

Changes of Quality Characteristics of Radishes Salted with Deep Seawater Salt (해양 심층수염을 이용한 무 절임시 품질특성 변화)

  • 이기동;김숙경;이현아;이명희;김미림
    • Food Science and Preservation
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    • v.10 no.2
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    • pp.182-186
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    • 2003
  • This study was carried out to observe the property changes of radishes salted with different salt (deep sea water and sun-dried salt). Shrinkage rate, salinity and texture were measured. The shrinkage rate values of radishes salted with deep seawater salt solution were higher than those salted with sun-dried salt in 8 hr after salting. The salinity of radishes salted with deep seawater salt solution was also higher than those salted with sun-dried salt. The jelly strength decreased during salting period and 5% salting radish were lower than 3% ones. The softness and hardness of radishes salted with deep seawater salt were higher than those salted with sun-dired salt as well.

A Study on the Vulcanization System and Two-Step Foaming Properties for Natural Rubber Foam (천연고무의 가황시스템 및 성형공정에 따른 2단 발포 특성 연구)

  • Sunhee Lee;Ye-Eun Park;Dikshita Chowdhury
    • Textile Coloration and Finishing
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    • v.35 no.4
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    • pp.246-255
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    • 2023
  • In this study, we investigated for natural rubber foam to replace petrochemical-based neoprene foam. Experiments were conducted on vulcanization system and 2-step foaming process of natural rubber. The vulcanization system were EV(Efficient Vulcanization Cure), Semi-EV(Semi-Efficient Vulcanization Cure) and CV(Conventional Vulcanization Cure). In the 2-step foaming process, first molding temperature was 140℃, times were 15, 20, 25, and 30minutes, and the second molding temperature was 160℃, the times 5, 10, 15, and 20minutes. The cure and viscosity characterization were evaluated by oscillating disc rheometer (ODR) and mooney viscosmeter. Various mechanical characteristics, including hardness, tensile strength, elongation at the point of rupture, and tear strength, were quantified. Subsequently, an assessment of alterations in these mechanical attributes was conducted post-immersion in a NaCl solution. In addition degree of volume change was measured after immersing the NR foam in NaCl solution and the low-temperature permanent compression set was evaluated at 4℃. And expansion ratio and shrinkage ratio of NR foam were evaluated for 28 days. As a result the EV vulcanization system showed the least change in physical properties before and after salt water immersion, and the lowest shrinkage ratio for 28 days. In addition it was confirmed that the 2-step foaming optimum condition differed depending on the appropriate vulcanization condition.

A Study on the Acid Degradation Properties of Cellulose Fabrics for Costume Heritage Restoration (유물 복원을 위한 천연 셀룰로오스 직물의 산에 의한 열화 특성 연구)

  • Jeon Cho-Hyun;Kwon Young-Suk;Lee Sang-Joon;Cho Hyun-Hok
    • Textile Coloration and Finishing
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    • v.17 no.4 s.83
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    • pp.35-40
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    • 2005
  • Researches to preserve and restore the excavated cellulose fabrics as costume heritages have been carried out. In this study, in order to artificially restore an excavated cellulose fabrics, acid-treated cellulose fabrics were prepared. Three kinds of cellulose fabrics were used for an experiment. Three kinds of cellulose fabrics were treated by the acid aqueous solution for the various strength retention ($100\%,\;80\%,\;60\%,\;40\%,\;20\%$). The fine structure and physical properties of acid treated cellulose fabrics were investigated with various techniques such as wide-angle X-ray diffraction, tensile test, weight loss, shrinkage, SEM etc. Tensile strength and strain of cellulose fabrics decreased with increasing acid treatment time. However, weight loss and shrinkage increasing slightly. The crystal diffraction intensity was not changed. SEM results of acid-treated cellulose fabrics show that the surface was damaged.

Manufacturing of Wood Charcoal Cup by Using Carbonization Method and Its Water Repellency (목재를 이용한 무할렬 숯잔 제조 및 발수특성)

  • Park, Sang Bum;Lee, Min
    • Journal of the Korea Furniture Society
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    • v.25 no.3
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    • pp.207-212
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    • 2014
  • With increased interests in environmental issues, people are looking for new materials that serve special and bio-activated functions. One of interesting materials is charcoal which has excellent adsorption ability for harmful volatile organic compounds, fireproof performance, far-infrared ray emission, and electromagnetic shielding. Since non-crack carbonized board was developed from wood-based composite materials, carbonization method might be applied to woodcraft products such as wood cup and bamboo. In this study, manufacture of wood charcoal bowl was conducted with carbonization method developed in 2009 in order to activate wood products market. Ash tree(Fraxinus rhynchophylla) cup was carbonized at $600^{\circ}C$ with two pretreatments which were phenol resin and wood tar solution treatment. After carbonization of ash tree cup, non-crack charcoal cup were successfully manufactured. Phenol resin treatment affected on charcoal cup manufacturing both positively and negatively. For a positive way, it prevented shrinkage. For a negative way, it decreased water repellency. On the contrary, wood tar treatment accelerated shrinkage a bit and increased water repellency. Based on the results, wood tar can be used as pre-treatment solution for reducing post-treatment costs. We confirmed woodcraft products can be carbonized without deformation, so carbonization may provide a high value-added products from wood.

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ABRASION RESISTANCE OF DENTURE BASE RESIN INCLUDING VINYLOLIGOSILSESQUIOXANE (Vinyloligosilsesquioxane 함유 의치상용 아크릴릭 레진의 마모 저항성)

  • Park Ran;Shim June-Sung;Han Dong-Hoo
    • The Journal of Korean Academy of Prosthodontics
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    • v.41 no.5
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    • pp.626-639
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    • 2003
  • Statement of problem : Recently, in attempts to reinforce the acrylic resin and to reduce the polymerization shrinkage, it has been reported that adding vinyloligo-silsesquioxane (vinyl-POSS) to PMMA significantly compensates for polymerization shrinkage and somewhat increases the fracture resistance. Purpose : There haven't been any studies on abrasion that can affect the adaptation of the denture in long-term use. In this study abrasion resistance was compared between acrylic resin with vinyl-POSS and commercialized acrylic resin for denture base. In addition, the difference in abrasion resistance according to molding methods was compared. Material and method : Using PaladentR 20 including vinyl-POSS. PaladentR 20, Lucitone 199R, SR IvocapR, denture bases were fabricated using compression molding technique and continuous-pressure injection technique. Surface hardness and abrasion were measured for each group, and the worn surfaces were observed under a scanning electron microscope. Results : 1. When surface hardness was measured for each material and molding technique, there was no statistically significant difference among the materials. (p<0.05) 2. When same denture base material and molding technique were used, the abrasion due to toothpaste solution was 5 times as severe as the abrasion due to soap solution. 3, When toothpaste solution was used, the abrasion decreased in the order of PaladentR20, PaladentR 20 including vinyl-POSS, SR IvocapR, and Lucitone 199R. However statistically significant difference was seen only among PaladentR 20, SR IvocapR, and Lucitone 199R. (p<0.05). 4. When soap solution was used, the abrasion was more severe in PaladentR 20 and including vinyl-POSS PaladentR 20 groups than in SR IvocapR and Lucitone 199R groups. (p<0.05). Conclusion : Addition of vinyl-POSS doesn't improve the abrasion resistance, and the abrasion resistance was similar to those of existing materials. Additional studies under different conditions are needed. For clinical application of vinyl-POSS, further investigations with different requirements and conditions are necessary.