• Title/Summary/Keyword: Separation technology

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Chromatographic Separation of Hydrogen Isotopes by Deactivated Alumina Stationary Phase (비활성 알루미나 고정상을 이용한 수소동위원소의 크로마토그래피 분리)

  • Kim, Kwang Rag;Lee, Sung Ho;Kang, Hee Suk;Chung, Hongsuk;Sung, Ki Woung
    • Applied Chemistry for Engineering
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    • v.9 no.1
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    • pp.121-128
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    • 1998
  • In fields of operating or handling a hydrogen isotope facility, and of the technology for nuclear fusion source management, gas chromatography has been used as one of the practical techniques lot separation and enrichment of hydrogen isotopic gases including tritium. Chromatographic separation experiments of the hydrogen isotope mixture (hydrogen, deuterium and tritium) were carried out by use of a commercially available gas chromatograph. An aliquot of gas sample was injected by a specially designed vacuum sampler into the stream of inert carrier gas which went through the separation column under liquid nitrogen temperature. The complete separation of hydrogen isotopic molecules was observed with an alumina adsorbent partially deactivated by coating with 10% manganese chlorine. In addition, fairly good separation conditions were obtained without any appearance of nuclear spin isomers with shorter retention time, which would be available for the practical applications of the hydrogen isotope separation and enrichment.

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Separation Performance of a Low-pressure Hydrocyclone for Suspended Solids in a Recirculating Aquaculture System

  • Lee, Jin-Hwan
    • Fisheries and Aquatic Sciences
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    • v.13 no.2
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    • pp.150-156
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    • 2010
  • The separation performance of a low-pressure hydrocyclone (LPH) was evaluated for suspended-solids removal in a recirculating aquaculture system (RAS). The dimensions of the LPH were 335 mm cylinder diameter, 575 mm cylinder height, 60 mm overflow diameter, 50 mm underflow diameter, and $68^{\circ}$ cone angle. The inflow rate varied (400, 600, 800, and 1,000 mL $s^{-1}$) with 25%, 25%, 20%, and 10% of bypass ($R_f$), respectively. The maximum total separation efficiency (Et) and reduced separation efficiency (E't) for suspended solids from the effluent of the second settlement tank (before biofiltration) were 58.9% and 45.2%, respectively, at an inflow rate of 600 mL $s^{-1}$ and 25% of $R_f$. The maximum Et and E't for suspended solids from the water supply channel (after biofiltration) were 24.4% and 16%, respectively, at an inflow rate of 1,000 mL $s^{-1}$ and 10% of $R_f$. The maximum grade efficiency (Ei) was 51.6% for a 300 ${\mu}m$ particle size at an inflow rate of 600 mL $s^{-1}$ with 23% of $R_f$. The maximum reduced grade efficiency (E'i) was 37.6% for a 300 ${\mu}m$ particle size at an inflow rate of 1,000 mL $s^{-1}$ with 11% of $R_f$. The results indicate that the separation performance of the LPH for suspended solids removal was size selective and that maximum removal occurred at particle sizes ranging from 300 to 500 ${\mu}m$.

Methodology to estimate minimum required separation distance between vehicle and bicycle when overtaking (자동차와 자전거 간 추월 최소요구 이격거리 추정 방법론 연구)

  • Jeon, Woo Hoon;Lee, Young-Ihn;Yang, Inchul;Lee, Hyang Mi
    • International Journal of Highway Engineering
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    • v.19 no.6
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    • pp.191-199
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    • 2017
  • PURPOSES : The objective of this study is to develop a methodology to estimate the minimum required separation distance (MRSD) between a vehicle and a bicycle when overtaking. METHODS : Three steps have been conducted to develop a methodology to estimate MSRD. First, a literature review has been conducted on the measurement of MSRD, and how it may be applied in Korea. Second, two assumptions have been made to develop a methodology to estimate the MSRD. The first assumption is that the maximum separation distance between a vehicle and a bicycle can be observed when they are at the same location longitudinally. In addition, it is assumed that the separation distance is invalid when the contra-flow exists. Finally, three cameras were installed at a height of 10 m to record the vehicle-bicycle interaction. Moreover, the vehicle trajectories as well as the separation distance were coded and analyzed. Through the hypothesis test and the interval estimation, the sample mean was tested and the confidence interval was estimated. RESULTS : 141 records of separation distance data were collected, and the hypothesis test demonstrated that the MSRD in Korea is significantly higher than other countries. In addition, the confidence interval of the population mean of MSRD is from 1.51 m to 1.65 m with 95% level of confidence. CONCLUSIONS : It is expected that the proposed methodology to estimate MSRD would be beneficial in studying road safety of vehicles and bicycles. Also, the proposed MSRD is expected to be designated in the act of road and transportation.

Mongolia Erden-soum tungsten development (몽골 에르덴솜 텅스텐광 개발을 위한 선별시스템 개발)

  • Kim, Su-Gang;Jeon, Ho-Seok;Baek, Sang-Ho;Kim, Byoung-Gon
    • Mineral and Industry
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    • v.28
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    • pp.1-13
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    • 2015
  • In this study, it was carried out separation process research and development to be able to produce high-grade tungsten concentrate form tungsten taken form Mongolia. In order to reduce treatment cost and increase separation efficiency the jig separation at first was applied for recovering the concentrate. Which reground would make the degree of liberation increase. Which was treated by shaking table to reject the gangue minerals from the first concentrate. Because the heavier product contains not only ferberite but also cassiterite, the product was treated by further dry magnetic separation to obtain the ferberite concentrate. Finally, the high-grade ferberite concentrate of 67.63% $WO_3$ could be obtained with recovery of 86.07% through the separation process developed in this study.

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The Development of Material Separation Technique for Recycling of Waste Car Tail Lamp (폐자동차(廢自動車) Tail Lamp의 재활용(再活用)을 위한 재질분리(材質分離) 기술개발(技術開發))

  • Jeon, Ho-Seok;Park, Chul-Hyun;Baek, Sang-Ho;Park, Jai-Koo
    • Resources Recycling
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    • v.15 no.6 s.74
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    • pp.25-32
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    • 2006
  • In this study, waste car tau lamps that usually gets incinerated or buried has been recovered during the dispose process in order to increase the recycling rate of waste cars and the material separation research was performed by applying triboelectrostatic separation method. After a series of charging characteristic test, PMMA materials was confirmed of being an effective charging material for waste car tail lamp material separation, a cyclone charger using PMMA material for continuous process was developed. In optimum test conditions using triboelectrostatic separator developed in this study, high quality PMMA material with recovery rate of 99.0% and 90.2% was achieved from the waste car tail lamp. Therefore, a material separation technology that can recycle tail lamps of waste cars has been established.

Relations between Radiologists' Job Stress and Intent of Separation (방사선사의 직무스트레스와 이직의도와의 관계)

  • Yeo, Jin-Dong;Kim, Hye-Sook
    • The Korean Journal of Health Service Management
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    • v.5 no.2
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    • pp.35-51
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    • 2011
  • The purpose of this study is to examine relations between the job stress of radiologists, who are serving at secondary medical institutions, and their intent of separation, providing basic information necessary to earlier prevent the separation, improve the quality of radiologists and ensure a more effective personnel management of the professionals. For the purpose, this researcher conducted a structured questionnaire survey of 221 radiologists from Nov 1 to 30, 2010 who were serving at secondary medical institutions located in Busan. Findings of the study can be summarized as follows. 1) The surveyed radiologists were scored 2.82 points in average in terms of job stress. This indicates that they are suffering from job stress higher than moderate. 2) The subjects were significantly different from each other in job stress according to their age, total service period, department where they were serving, satisfaction with their hospital and satisfaction with the foresaid department. 3) The subjects were scored 2.59 points in average in terms of the intent of separation. This indicates that the surveyed radiologists are not so willing to change their job. 4) Those radiologists were significantly different from each other in the intent of separation according to their age, marital status, educational background, average monthly income, total service period, the period of service at a department where they belonged now, position, satisfaction with their hospital and satisfaction with the foresaid department. 5) There were significant correlations between the subjects' job stress and intent of separation.

A Rapid Preparation of Carrier-Free Fluorine-38 for Medical Use

  • Kim, You-Sun;Kim, Jaerok
    • Nuclear Engineering and Technology
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    • v.8 no.1
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    • pp.1-8
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    • 1976
  • For tile rapid production of fluorine-18 for medical use, the up-to-date methods of separation such as the recoil separation, the alumina column chromatography, and the distillation are reviewed. The amount of the residue, the gamma emitting impurity, and the tritium content in the product obtained by each separation method are determined. The product obtained by the nuclear recoil separation or by the alumina column chromatography is inferior to that obtained by the distillation in the purity point of view. Thus, the separation by the distillation is tile most effective especially in the case of using a natural lithium carbonate target. Carrier free fluorine-18 of about 2 mCi can routinely be produced by irradiating 7g of the natural lithium carbonate under the neutron flux of about 1$\times$10$^{13}$ n/$\textrm{cm}^2$/sec for 3 hrs, and subsequent separation by the distillation. The over-all processing time is 35-40n1in.

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The enhancement of protein separation by duplex SDS-PAGE (Duplex SDS-PAGE를 이용한 단백질 분리향상)

  • Pyo, Jae Sung;Roh, Si Hun;Song, Jin-Su;Lee, Kyung Hyeon;Kim, Hie-Joon;Park, Jeong Hill;Kwon, Sung Won
    • Analytical Science and Technology
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    • v.19 no.6
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    • pp.529-534
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    • 2006
  • The protein separation with molecular weight using SDS-PAGE(sodium dodecyl sulfate-polyacrylamide gel electrophoresis) is the one of the most conventional and simple techniques. In, this study, two dimensional SDS-PAGE using same separation principle consecutively was investigated and compared with one dimensional SDS-PAGE. The enhanced separation from duplex SDS-PAGE was observed and separated proteins in the gel were identified by MALDI TOF MS. Identified proteins from different gel spots were found to have different gi numbers. Therefore, duplex SDS-PAGE separation method will be used for economic separation method in the future because only tiny amount of inexpensive reagents are used to perform duplex SDS-PAGE.

Recovery Processes of Organic Acids from Fermentation Broths in the Biomass-Based Industry

  • Li, Qian-Zhu;Jiang, Xing-Lin;Feng, Xin-Jun;Wang, Ji-Ming;Sun, Chao;Zhang, Hai-Bo;Xian, Mo;Liu, Hui-Zhou
    • Journal of Microbiology and Biotechnology
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    • v.26 no.1
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    • pp.1-8
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    • 2016
  • The new movement towards green chemistry and renewable feedstocks makes microbial production of chemicals more competitive. Among the numerous chemicals, organic acids are more attractive targets for process development efforts in the renewable-based biorefinery industry. However, most of the production costs in microbial processes are higher than that in chemical processes, among which over 60% are generated by separation processes. Therefore, the research of separation and purification processes is important for a promising biorefinery industry. This review highlights the progress of recovery processes in the separation and purification of organic acids, including their advantages and disadvantages, current situation, and future prospects in terms of recovery yields and industrial application.

Gas Permeation Properties of Sulfonated 6FDA-based Polyimide Membranes (설폰화된 6FDA계 폴리이미드 막을 이용한 기체투과특성)

  • Rhim, Ji-Won;Yoon, Seok-Won;Lee, Byung-Seong;Lee, Bo-Sung;Cheong, Seong-Ihl
    • Membrane Journal
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    • v.19 no.3
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    • pp.237-243
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    • 2009
  • Polyimides synthesized by using 2,2'-bis(3,4-carboxylphenyl) hexafluoropropane dianhydride (6FDA) and 4,4'-diaminodiphenylmethane (DAM) were sulfonated according to reaction times, 5 min to 20 min. And the resulting polyimide membranes were investigated in terms of permeability and separation factor for $N_2$, $O_2$, and $CO_2$ gases. The introduction of bulky group, $-{SO_3}H$, leads to the decreases of both diffusivities and solubilities for all the range of reaction times. At 20 min of sulfonation, the diffusivity and solubility of $N_2$ decrease up to 21% and 26%, respectively. Overall separation efficiencies for $O_2/N_2$ and $CO_2/N_2$ increase as the reaction time increases to 20 min.