• Title/Summary/Keyword: Separation technology

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Preparative Chromatographic Separaction: Simulated Moving Bed and Modified Chromatography Methods

  • Yi Xie;Koo, Yoon-Mo;Nien-Hwa Linda Wang
    • Biotechnology and Bioprocess Engineering:BBE
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    • v.6 no.6
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    • pp.363-375
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    • 2001
  • Chromatography has been method of choice for the separation complex biologi-cal mixtures fro analytical purpose, particularly for the last fifty years. Its use has recently been extended to preparative separation where the productivity relative to the amount of resin and sol-vent used is a matter of concern. To overcome the inherent thermodynamic inefficiency of batch chromatography, as exemplified by the partial temporal usage of the resin and dilution of the product with the solvent, chromatography has been continually modified by separation engineers. Column switching and recycling represnet some of the process modifications that have brought high productivity to chromatography. Recently, the simulated moving bed (SMB) method, which claims a high separation efficiency based on counter-current moving bed chromatography. has be-come the mainstay of preparative separation, especially in chiral separation. Accordingly, this pa-per reviews the current status of SMB along with several chromatographic modification, which may be helpful in routine laboratory and industrial chromatographic practices.

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A Study on the Development of Active Circulating Type Oil Recovery Vessel

  • Lee, Kji-Joo;Shugan, Igor V.;An, Jung-Sun
    • Journal of Ocean Engineering and Technology
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    • v.21 no.6
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    • pp.1-6
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    • 2007
  • A study on the new active circulation type oil-water separation system including buoyancy type guidance system was carried out in this paper. Newly developed oil-water separation system is composed of several oil separation steps. In the beginning of these steps, buoy type separation system would be used. Buoy type oil guiding system was developed based on the difference of density of water and oil.

Employing high-temperature gas flux in a residual salt separation technique for pyroprocessing

  • Kim, Sung-Wook;Heo, Dong Hyeon;Kang, Hyun Woo;Hong, Sun-Seok;Lee, Sang-Kwon;Jeon, Min Ku;Hur, Jin-Mok;Choi, Eun-Young
    • Nuclear Engineering and Technology
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    • v.51 no.7
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    • pp.1866-1870
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    • 2019
  • Residual salt separation is an essential step in pyroprocessing because its reaction products, as prepared by electrochemical unit processes, contain frozen residual electrolyte species, which are generally composed of alkali-metal chloride salts (e.g., LiCl, KCl). In this study, a simple technique that utilizes high-temperature gas flux as a driving force to melt and push out the residual salt in the reaction products was developed. This technique is simple as it only requires the use of a heating gun in combination with a gas injection system. Consequently, $LiNO_3-ZrO_2$ and $LiCl-ZrO_2$ mixtures were successfully separated by the high-temperature gas injection (separation efficiency > 93%), thereby demonstrating the viability of this simple technique for residual salt separation.

Blind Source Separation for OFDM with Filtering Colored Noise and Jamming Signal

  • Sriyananda, M.G.S.;Joutsensalo, Jyrki;Hamalainen, Timo
    • Journal of Communications and Networks
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    • v.14 no.4
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    • pp.410-417
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    • 2012
  • One of the premier mechanisms used in extracting unobserved signals from observed mixtures in signal processing is employing a blind source separation (BSS) algorithm. Orthogonal frequency division multiplexing (OFDM) techniques are playing a prominent role in the sphere of multicarrier communication. A set of remedial solutions taken to mitigate deteriorative effects caused within the air interface of OFDM transmission with aid of BSS schemes is presented. Four energy functions are used in deriving the filter coefficients. Energy criterion functions to be optimized and the performance is justified. These functions together with iterative fixed point rule for receive signal are used in determining the filter coefficients. Time correlation properties of the channel are taken advantage for BSS. It is tried to remove colored noise and jamming components from themixture at the receiver. Themethod is tested in a slow fading channel with a receiver containing equal gain combining to treat the channel state information values. The importance is that, these are quite low computational complexity mechanisms.

The Effect of Additives on the Gasohol (가솔린의 첨가물질이 가소홀에 미치는 영향에 관한 연구)

  • Lee, Jin-Hui;Le, Il-Woo
    • Journal of the Korean Applied Science and Technology
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    • v.28 no.3
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    • pp.374-378
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    • 2011
  • The studied results of the gasohol, which is the mixture of gasoline and ethanol, were investigated for the promotion of applications on commercially by gasoline vehicle referring to octane number, minimum water contents be involved, and separation inhibitors for protecting phase separation etc. especially for the E10 and E20. The results showed that octane number will be revised by higher value as the ethanol is added more, and it's more effect in case of be added as a mixture than individually when inhibition agents is added for the inhibition of separation. and it's reasonable for the water contents of less than 1% by comparing with experimental results and in view of regulations of various countries.

Preparation of a Water-Selective Ceramic Membrane on a Porous Stainless Steel Support by Sol-Gel Process and Its Application to Dehydration Membrane Reactor

  • Lee, Kew-Ho;Sea, Bongkuk;Youn, Min-Young;Lee, Yoon-Gyu;Lee, Dong-Wook
    • Korean Membrane Journal
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    • v.6 no.1
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    • pp.10-15
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    • 2004
  • We developed a water-selective ceramic composite membrane for use as a dehydration membrane reactor for dimethylether (DME) synthesis from methanol. The membranes were modified on the porous stainless steel support by the sol-gel method accompanied by a suction process. The improved membrane modification process was effective in increasing the vapour permselectivity by removal of defects and pinholes. The optimized alumina/silica composite membrane exhibited a water permeance of 1.14${\times}$10$^{-7}$ mol/$m^2$.sec.Pa and a water/methanol selectivity of 8.4 at permeation temperature of 25$0^{\circ}C$. The catalytic reaction for DME synthesis from methanol using the membrane was performed at 23$0^{\circ}C$, and the reaction conversion was compared with that of the conventional fixed-bed reactor. The reaction conversion of the membrane reactor was much higher than that of the conventional fixed-bed reactor. The reaction conversion of the membrane reactor and the conventional fixed-bed reactor was 82.5 and 68.0%, respectively. This improvement of reaction efficiency can last if the water vapour produced in the reaction zone is removed continuously.

A Study on the Electrolytic Process for Palladium Separation from Recovered Crude Metal of Electronic Waste (전자폐기물에서 회수된 조금속으로부터 팔라듐 분리를 위한 전해공정에 관한 연구)

  • Park, Sung Cheol;Han, Chul Woong;Kim, Yong Hwan;Jung, Yeon Jae;Lee, Man Seung;Son, Seong Ho
    • Resources Recycling
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    • v.30 no.6
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    • pp.76-82
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    • 2021
  • The separation of palladium from crude metal, which is obtained from electronic waste using pyrometallurgy was achieved through electrolysis. This was done to recover high-purity copper. The oxidation potentials of these metals are a fundamental part of the analysis of electrolytic separation of palladium and impurity metals. To achieve this, copper, iron, and nickel were dissolved in the electrolyte, and palladium and aluminum were found to be recoverable from anode slime. During the electrolysis for palladium separation, palladium was present in the anode slime and was obtained with a recovery of 97.46 % indicating almost no loss. 4N-grade copper was recovered from the electrodeposition layer at the cathode.

A Study on Comparision of the Quantity of Phoria as Way to Separation of Binocular Fusion (양안융합의 분리 시간에 따른 사위량 비교에 관한 연구)

  • Kang, Seok Hyon;Hong, Hyungki
    • Journal of Korean Ophthalmic Optics Society
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    • v.19 no.3
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    • pp.331-337
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    • 2014
  • Purpose: This is a comparative experimental study on the amount of phoria by the removal time of binocular fusion. In this study, three tests were used for phoria test like Howell test, Thorington test and developed 3D polarizing test. Methods: In this study, it was considered the removal time of binocular fusion for measuring phoria. The three methods were used for measuring quantity of phoria: Howell test, Thorington test and developed 3D Polarizing test. The measurements progressed quickly to avoid eye-strain. So we designed the test charts for marking 3D display modules and the apparatus inserted lenses, like Maddox lens and prism, which are compatible with three phoria tests. The phoria at the moment separation was measured when the binocular fusion was broken through the apparatus and the that at the stable separation was measured when activity of the separated two images like indicated box and figure on horizontal axis stopped. Results: There were statistically significant difference between quantity of phoria at moment separation and that at stable separation. Amount of phoria at moment separation was relatively larger than amount of that at stable separation. In result in exophoria, the quantity of phoria at moment separation was higher than that at stable separation, and in phoria measured by developed 3D polarizing test, it shows the similar results at two condition. Conclusions: For exophoria, the amount of phoria at moment separation of binocular fusion was relatively larger than that at stable separation. The amount of difference between phoria values at moment separation and that at stable separation was alike among three phoria tests. Usually in working, there is no distinction between moment separation and stable separation. But there were definitely the difference between two ways to separate binocular fusion. Therefore, it is need for writing on prescription test name for measuring phoria and condition of separation of binocular fusion.