• Title/Summary/Keyword: Sensitive film

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Electrochemical Behavior of Norfloxacin and Its Determination at Poly(methyl red) Film Coated Glassy Carbon Electrode

  • Huang, Ke-Jing;Xu, Chun-Xuan;Xie, Wan-Zhen
    • Bulletin of the Korean Chemical Society
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    • v.29 no.5
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    • pp.988-992
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    • 2008
  • A poly(methyl red) film-modified glassy carbon electrode (PMRE) was fabricated for determination of norfloxacin (NFX). The electrochemical behavior of NFX was investigated and a well-defined oxidation peak with high sensitivity was observed at the film electrode. PMRE greatly enhanced the oxidation peak current of NFX owing to the extraordinary properties of poly(methyl red) film. Based on this, a sensitive and simple voltammetric method was developed for measurement of NFX. A sensitive linear voltammetric response for NFX was obtained in the concentration range of $1\;{\times}\;10^{-6}\;-\;1\;{\times}\;10^{-4}$ mol/L and the detection limit was $1\;{\times}\;10^{-7}$ mol/L using linear sweep voltammetry (LSV). The proposed method possessed advantages such as low detection limit, fast response, low cost and simplicity. The practical application of this new analytical method was demonstrated with NFX pharmaceuticals.

Effect of Anti-Vortex Hole Angle on the Flat Plate Film Cooling Effectiveness (반와류 홀의 각도가 평판의 막냉각 효율에 미치는 영향 연구)

  • Park, Soon Sang;Park, Jung Shin;Lee, Sang Hoon;Moon, Young Gi;Kwak, Jae Su
    • The KSFM Journal of Fluid Machinery
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    • v.17 no.5
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    • pp.5-10
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    • 2014
  • In this paper, the experimental study was carried to investigate the effect of angle of the anti-vortex holes on the film cooling effectiveness on a flat plate. The pressure sensitive paint technique was applied to measure the film cooling effectiveness. Two anti-vortex hole angles of $0^{\circ}$ and $15^{\circ}$ with respect to the primary hole were considered, and the simple cylindrical hole case was also tested. The blowing ratio based on the cylindrical hole was 0.5 and the same flow rate was kept for all anti-vortex hole cases. Results showed that the film cooling effectiveness for the anti-vortex hole cases were much higher than that of the cylindrical case. Among the anti-vortex hole cases, $15^{\circ}$ angle anti-vortex hole case showed higher film cooling effectiveness than that by the $0^{\circ}$ angle anti-vortex hole case.

Improvement of Film Cooling Performance of a Slot on a Flat Plate Using Coanda Effect (코안다 효과를 이용한 평판 슬롯의 막냉각 성능 향상)

  • Kim, Gi Mun;Kim, Ye Jee;Kwak, Jae Su
    • The KSFM Journal of Fluid Machinery
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    • v.20 no.2
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    • pp.5-10
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    • 2017
  • In this study, the Coanda effect inducing bump was applied to improve the film cooling effectiveness on the flat plate with $30^{\circ}$ and $45^{\circ}$ angled rectangular slots. The slot length to width ratio was 6. A cylindrical cap shaped structure, called Coanda bump, was installed at the exit of the slot to generate Coanda effect. The width and height of the bump was 10.5 mm and 1 mm, respectively. The film cooling effectiveness was measured at the fixed blowing ratio, M=2.0, using pressure sensitive paint (PSP) technique. The mainstream velocity was 10 m/s and the turbulence intensity was about 0.5%. Results showed that the film cooling effectiveness for case of $30^{\circ}$ angled slot was higher than that of $45^{\circ}$ angled slot. It was found that there was no positive effect of Coanda effect on the overall averaged film cooling effectiveness for the $30^{\circ}$ angled slot. On the other hand, for the $45^{\circ}$ angled slot, the film cooling effectiveness was improved with the installation of the Coanda bump.

A Study on Synthesis of Acrylic Pressure Sensitive Adhesive for Polarizer Film by Solution Polymerization (용액중합에 의한 편광필름용 아크릴 점착제의 합성에 관한 연구)

  • Lim, Chang-Hyuk;Jung, Young-Jae;Cho, Ur-Ryong
    • Elastomers and Composites
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    • v.44 no.2
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    • pp.175-181
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    • 2009
  • The solution polymerization was conducted to synthesize pressure sensitive adhesive for polarizer film using acrylic monomers. 2-Ethylhexyl acrylate, butyl acrylate, acrylic acid were used as acrylic monomers, benzoyl peroxide as initiator, ethyl acetate as solvent. The ratio of monomers was 2-ethylhexyl acrylate: butyl acrylate: acrylic acid = 25:50:3.6 reflecting $-40^{\circ}C$ of glass transition temperature in the pressure sensitive adhesive. The amount of initiator was determined as 0.09% to monomer considering wetting power and initial tackiness. The ratio of monomer to solvent was determined as 1:1.7 considering wetting power and transmissivity. The transmissivity of pressure sensitive adhesive increased with decreasing both viscosity and molecular weight due to reducing of refractive index by low entanglement between molecules. In the measurement of pot life, it was found that the storage stability was good at 1:1.7 of monomer: solvent without large change of viscosity during 200 min.

Emotional Analysis on the Building Background of Chinese History Film 'Hero' (중국역사영화 '영웅'의 건물배경에 대한 감성분석)

  • Yu, Shen;Song, Seung-keun
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2018.05a
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    • pp.291-292
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    • 2018
  • The purpose of this study is to examine the sensitivity of the audience to the background of the building where Chinese historical film 'Hero' is used. In this study, the sensitive vocabulary suitable for the building background was derived through previous research related to sensitivity, and the sensitive analysis was analyzed by questionnaire form. Research result shows that the building background of the movie can have an sensitive impact on the audience and will help to understand Chinese traditional style and culture.

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Synthesis and Characterization of HPMC Derivatives as Novel Duodenum-Specific Coating Agents

  • Huang Yuan;Zheng ling Ii;Liu Jun;Zhang Zhi rong
    • Archives of Pharmacal Research
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    • v.28 no.3
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    • pp.364-369
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    • 2005
  • HPMC (Hydroxypropyl methylcellulose) was chemically modified, using maleic anhydrides, to obtain pH-sensitive HPMCAM (Hydroxypropyl methylcellulose acetate maleate) polymers for use as novel duodenum-specific coating agents. The pharmaceutical properties of HPMCAM, such as film forming, acid values, pH-sensitive values, water vapor permeability, tensile strength and Tg, were investigated, and found to show good film forming properties. The pH­sensitive values were 3.0 to 3.7. In vitro results demonstrate that HPMCAM could completely suppress drug release within 2h in a simulated gastric fluid (pH 1.2) and rapidly release the drug in a simulated pathological duodenal fluid (pH 3.4). These results indicate that HPMCAM might be a useful material for a duodenum-specific drug delivery system.

Sensitivity Improvement and Operating Characteristics Analysis of the Pressure Sensitive Field Effect Transistor(PSFET) Using Highly-Oriented ZnO Piezoelectric Thin Film

  • Lee, Jeong-Chul;Cho, Byung-Woog;Kim, Chang-Soo;Nam, Ki-Hong;Kwon, Dae-Hyuk;Sohn, Byung-Ki
    • Journal of Sensor Science and Technology
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    • v.6 no.3
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    • pp.180-187
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    • 1997
  • We demonstrate the improvement of sensitivity and analysis of operating characteristics of the piezoelectric pressure sensor using ZnO piezoelectric thin film and FET(field effect transistor) for sensing applied pressure and transforming the pressure into electrical signals, respectively. The sensitivity of the PSFET(pressure sensitive field effect transistor) was improved by using highly-oriented ZnO film perpendicular to the substrate surface and the operating characteristics was investigated by monitoring output voltage with time in various static pressure levels.

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Strain sensing skin-like film using zinc oxide nanostructures grown on PDMS and reduced graphene oxide

  • Satish, Tejus;Balakrishnan, Kaushik;Gullapalli, Hemtej;Nagarajaiah, Satish;Vajtai, Robert;Ajayan, Pulickel M.
    • Structural Monitoring and Maintenance
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    • v.4 no.2
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    • pp.107-113
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    • 2017
  • In this paper, we present a strain-sensitive composite skin-like film made up of piezoresistive zinc oxide (ZnO) nanorods embedded in a flexible poly(dimethylsiloxane) substrate, with added reduced graphene oxide (rGO) to facilitate connections between the nanorod clusters and increase strain sensitivity. Preparation of the composite is described in detail. Cyclic strain sensing tests are conducted. Experiments indicate that the resulting ZnO-PDMS/rGO composite film is strain-sensitive and thus capable of sensing cycling strain accurately. As such, it has the potential to be molded on to a structure (civil, mechanical, aerospace, or biological) in order to provide a strain sensing skin.

A Highly Sensitive Humidity Sensor Using a Modified Polyimide Film

  • Kim, Yong-Ho;Lee, Joon-Young;Kim, Yong-Jun;Kim, Jung-Hyun
    • JSTS:Journal of Semiconductor Technology and Science
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    • v.4 no.2
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    • pp.128-132
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    • 2004
  • This paper presents the design, fabrication sequence and measurement results of a highly sensitive capacitive-type humidity sensor using a polyimide film without hydrophobic elements. The structure of the humidity sensor is MIM (metalinsulator-metal). For a high sensitivity, a modified aromatic polyimides as a moisture absorbing layer has been synthesized instead of using general polyimides containing hydrophobic elements. The polyimide film was obtained by synthesizing and thermally polymerizing polyamic acid composed of m-pyromellitic dianhydride, phenelenediamine and dimethylacetamide. Characteristics of fabricated sensors which include sensitivity, hysteresis and stability have been measured. The measurement result shows the percent normalized capacitance change of 0.37/%RH over a range from 10 to 90%RH, hysteresis of 0.77% over the same %RH range and maximum drift of 0.25% at 50%RH. The result shows that the developed humidity sensor can be applied to evaluate a hermeticity of various sensors and actuator systems as well as micro packages.