• Title/Summary/Keyword: Scattering Analysis

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Nondestructive, Quantitative Synchrotron Grazing Incidence X-ray Scattering Analysis of Cylindrical Nanostructure in Supported Thin Films

  • Yoon, Jin-Hwan;Yang, Seung-Yun;Lee, Byeong-Du;Joo, Won-Chul;Heo, Kyu-Young;Kim, Jin-Kon;Ree, Moon-Hor
    • Proceedings of the Polymer Society of Korea Conference
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    • 2006.10a
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    • pp.300-300
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    • 2006
  • Nondestructive nanostructural analysis is indispensable in the development of nano-materials and nano-fabrication processes for use in nanotechnology applications. In this paper, we demonstrate for the first time a quantitative, nondestructive analysis of nanostructured thin films supported on substrates and their templated nanopores by using grazing incidence X-ray scattering and data analysis with a derived scattering theory. Our analysis disclosed that vertically oriented nanodomain cylinders had formed in 20-100 nm thick films supported on substrates consisting of a mixture of poly(styrene-b-methyl methacrylate) (PS-b-PMMA) and PMMA homopolymer, and that the PMMA nanodomains were selectively etched out by ultraviolet light exposure and a subsequent rinse with acetic acid, resulting in a structure consisting of hexagonally packed cylindrical nanopores.

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Development of an Elastic Analysis Technique Using the Mixed Volume and Boundary Integral Equation Method (혼합 체적-경계 적분방정식법을 이용한 탄성해석 방법 개발)

  • Lee, Jeong-Gi;Heo, Gang-Il;Jin, Won-Jae
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.26 no.4
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    • pp.775-786
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    • 2002
  • A Mixed Volume and Boundary Integral Equation Method is applied for the effective analysis of elastic wave scattering problems and plane elastostatic problems in unbounded solids containing general anisotropic inclusions and voids or isotropic inclusions. It should be noted that this newly developed numerical method does not require the Green's function for anisotropic inclusions to solve this class of problems since only Green's function for the unbounded isotropic matrix is involved in their formulation for the analysis. This new method can also be applied to general two-dimensional elastodynamic and elastostatic problems with arbitrary shapes and number of anisotropic inclusions and voids or isotropic inclusions. In the formulation of this method, the continuity condition at each interface is automatically satisfied, and in contrast to finite element methods, where the full domain needs to be discretized, this method requires discretization of the inclusions only. Finally, this method takes full advantage of the pre- and post-processing capabilities developed in FEM and BIEM. Through the analysis of plane elastostatic problems in unbounded isotropic matrix with orthotropic inclusions and voids or isotropic inclusions, and the analysis of plane wave scattering problems in unbounded isotropic matrix with isotropic inclusions and voids, it will be established that this new method is very accurate and effective for solving plane wave scattering problems and plane elastic problems in unbounded solids containing general anisotropic inclusions and voids/cracks or isotropic inclusions.

Estimation of PM2.5 Correction Factor for Optical Particle Counter in Ambient Air (대기환경에서 광산란 미세먼지 측정기의 PM2.5 보정계수 산정)

  • Kim, Jong Bum;Kim, Danbi;Noh, Sujin;Yoon, Kwan Hoon;Park, Duckshin;Lee, Jeong Joo;Kim, Jeongho
    • Particle and aerosol research
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    • v.16 no.2
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    • pp.49-59
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    • 2020
  • Various devices have been developed to the measurement of particulate matter pollutants, and Optical Particle Counter (OPC) that can be easily and quickly measured is widely used lately. The measured value by OPC is converted to weight concentration using the correction factor (CF). The calculation of CF is very important to improve the reliability and accuracy of OPC. In this study, the CF calculation study of light scattering laser photometer (model 8533, TSI) was carried out to measure in the atmospheric environment using 2 gravimetric devices and 3 light scattering laser photometer devices. Regression analysis and Tukey tests were used to significance the test of measurement devices. Measurements were carried out twice. There was a comparative analysis of measurement data between light scattering laser photometer and gravimetric devices in 1st measurement, and then the Evaluation of PM2.5 concentration corrected by CF performed in 2nd measurement. As a result of the significance analysis between light scattering laser photometer and gravimetric devices, the correlation between the same method was high, but the correlation between different methods was low. CF was calculated as 0.4258 based on the measurement results, and it is a similar level to previous studies at home and abroad. It is expected that these results can be used as basic data in the future study for air quality measurement research using light scattering laser photometer. Also, in order to improve the accuracy of the measurement techniques and the development of technology in the atmospheric environment, CF calculation research should be conducted continuously.

Finite Element Analysis of Ultrasonic Wave Propagation and Scattering (초음파 전파 및 산란 문제의 유한요소 해석)

  • Jeong, Hyun-Jo;Park, Moon-Cheol;Park, Yun-Won
    • Journal of the Korean Society for Nondestructive Testing
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    • v.22 no.4
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    • pp.411-421
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    • 2002
  • The accurate analysis of ultrasonic wave propagation and scattering plays an important role in many aspects of nondestructive evaluation. A numerical analysis makes it possible to perform parametric studies, and in this way the probability of detection and reliability of test results can be improved. In this study, a finite element method was developed for the analysis of ultrasonic fields, the accuracy of results was checked by solving several representative problems. The size of element and the integral time step, which are the critical components for the convergence of numerical results, were determined in a commercial finite element code. Several propagation and scattering problems in 2-D isotropic and anisotropic materials were solved and their results were compared with known analytical or experimental results.

The Intensity Scale of Multiple Scattering of X-rays in Non-Crystalline Solids (비정질 고체에 대한 X선의 다중 산란 강도)

  • 박성수;장윤식;류봉기;박희찬
    • Journal of the Korean Ceramic Society
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    • v.34 no.1
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    • pp.109-113
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    • 1997
  • When the intensity of X-rays scattered from amorphous materials (very weakly absorbing materials) is measured using standard diffractometric technique, the intensity caused by multiple scattering is obtained in the measured X-ray intensity. Computer programs have been developed to estimate the intensity of the mul-tiple scattering obtained in vitreous SiO2 and B2O3 with various X-rays. Using the above computer program, the intensity ratios of multiple scattering to single scattering in vitreous SiO2 were 0.10~0.16% at CuK$\alpha$, 0.98~5.87% at MoK$\alpha$, and 1.88~17.86% at AgK$\alpha$ in the range of 2$\theta$=0~180$^{\circ}$. Therefore, pri-or to the structural analysis of vitreous SiO2 and B2O3 performed experimentally using X-ray diffractometric technique, the intensity data measured in MoK$\alpha$ and AgK$\alpha$ radiations must be corrected for multiple scattering effect.

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Distribution of the Deep Scattering Layer around Uljin Coastal Area (울진 연안의 음향 산란층 분포)

  • HWANG Doo Jin;KIM Dong Eon;JEONG Sun Beom;SON Yong Uk;CHAE Jin Ho;CHO Ki Ryang
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.38 no.3
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    • pp.205-213
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    • 2005
  • A hydroacoustic and a close-open-close zooplankton net survey were conducted to understand the distribution characteristics of the deep scattering layer (DSL) and to estimate the density of zooplankton in the DSL, in the Uljin coastal area. The survey was carried out during March 13-14 and June 4-5, 2003 at each station for zooplankton. The vertical migration mechanisms of zooplankton are very variable to the taxa. In this study, after we grasp the vertical migration of zooplankton through the results of an echo-sounder survey, we verified the mechanisms of their vertical migration in the Uljin coastal area. Also, to estimate effectively the biomass of zooplankton, we researched the acoustic scattering strength according to the species. On the basis of these results, we devised a method for estimating zooplankton biomass through comparing net and echo-soundings. We obtained the results as a follows; 1) According to the examination of collections from the net sampling, in March, 2003, Euphausia pacifica comprised $38\%$ of zooplanktons inhabiting the sound scattering layer, while copepods, chaetognaths, and amphipods accounted for $29\%,\;23\%\;and\;10\%$, respectively. And in June, 2003, the ratio of E. pacifica was $51\%$, copepods $43\%$, and the others comprised $6\%$. In both March and June E. pacifica showed dominance among the species of zooplankton. 2) The analysis of vertical distribution through acoustic data in the scattering layer was more apparent in June (spring/summer) of 2003, than in March (winter/spring) of that year. The vertical migration of zooplankton peaked around sunrise and sunset in both March and June. 3) As for the sound scattering layer, it distributed in the open sea in March, and in the inland sea in June. Therefore it is suggested that some zooplankton species such as E. pacifica performed ontogenic horizontal migration througth the spring and early summer.

Mid Frequency Band Reverberation Model Development Using Ray Theory and Comparison with Experimental Data (음선 기반 중주파수 대역 잔향음 모델 개발 및 실측 데이터 비교)

  • Chu, Young-Min;Seong, Woo-Jae;Yang, In-Sik;Oh, Won-Tchon
    • The Journal of the Acoustical Society of Korea
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    • v.28 no.8
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    • pp.740-754
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    • 2009
  • Sound in the ocean is scattered by inhomogeneities of many different kinds, such as the sea surface, the sea bottom, or the randomly distributed bubble layer and school of fish. The total sum of the scattered signals from these scatterers is called reverberation. In order to simulate the reverberation signal precisely, combination of a propagation model with proper scattering models, corresponding to each scattering mechanism, is required. In this article, we develop a reverberation model based on the ray theory easily combined with the existing scattering models. Developed reverberation model uses (1) Chapman-Harris empirical formula and APL-UW model/SSA model for the sea surface scattering. For the sea bottom scattering, it uses (2) Lambert's law and APL-UW model/SSA model. To verify our developed reverberation model, we compare our results with those in Ellis' article and 2006 reverberation workshop. This verified reverberation model SNURM is used to simulate reverberation signal for the neighboring seas of South Korea at mid frequency and the results from model are compared with experimental data in time domain. Through comparison between experiment data and model results, the features of reverberation signal dependent on environment of each sea is investigated and this analysis leads us to select an appropriate scattering function for each area of interest.

A Study on the Measurement of Fine Scratches by Scattering of Laser Light (레이저 산란광을 이용한 미소표면 결합의 측정평가법에 관한 연구)

  • Gang, Yeong-Jun
    • Journal of the Korean Society for Precision Engineering
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    • v.9 no.2
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    • pp.22-28
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    • 1992
  • This paper is studied about the method to measure the fine scratches on the mirror surfaces, such as the silicon wafer and magnetic memory disk by the optical measuring method. The theoretical background of this analysis is based upon the light scattering theory developed by Beckmann. In this analysis, the roughness in fine scratches is not considered because the aberage roughness is very small compared with the size of fine scratches. Empasis is on quantilaive method of fine scratches by non-contact method. Experiments are followed by the image processing system attached to the CCD Camera. As a results, I propose the new method to measure the size of the fine scratches from the parameters obtained by the computer simulation and experiments.

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A novel method for the synthesis of nano-magnetite particles

  • Syahmazgi, Maryam Ghodrati;Falamaki, Cavus;Lotfi, Abbas Sahebghadam
    • Advances in nano research
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    • v.2 no.2
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    • pp.89-98
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    • 2014
  • A novel and simple method for the synthesis of nano-magnetite particles is disclosed. In the novel procedure, $Fe^{2+}$ is the only source of metal cation. Carboxymethylcellulose (CMC) is used as the structure directing agent. The phase analysis of the nano-particles was performed using XRD and electron diffraction techniques. Size and morphology analysis was performed using light scattering and TEM techniques. The effect of $NH_4OH$ solution (32 wt. %) at different CMC concentrations on the size distribution of the final magnetite powders is studied. An optimal base concentration exists for each CMC concentration leading to minimal agglomeration. There exists a minimum CMC concentration (0.0016 wt. %), lower than that no magnetite forms. It is shown that using the new method, it is possible to immobilize a lipase enzyme (Candida Rugosa) with immobilization efficiency larger than 98 % with a loading more than 3 times the reported value in the literature. The latter phenomenon is explained based on the agglomerate state of the nano-particles in the liquid phase.