• Title/Summary/Keyword: SEM-EDX 분석

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Analysis of Charred-Woods Excavated from the Daewoongjeon Hall of Youngguksa Temple (영국사 대웅전 출토 탄화목의 재질 분석)

  • Son, Byung Hwa;Park, Won-Kyu
    • Journal of the Korean Wood Science and Technology
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    • v.35 no.1
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    • pp.36-43
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    • 2007
  • Elemental analysis, SEM-EDX, X-ray diffraction (XRD) and IR analysis were adopted to examine the quality of charred woods excavated from the underground of the Daewoongjeon Hall of Youngguksa Temple, Youngdong-gun, Chungbuk, Korea. A large amount of calcium was detected in SEM-EDX analysis. The analyses of chemical elements suggested that completely charred wood was carbonized at about $500^{\circ}C$. The XRD results indicated the destruction of cellulose crystalline region. The IR analysis exhibited that thermal degradation of wood component was different depending upon the carbonization temperature. It can be suggested from the results that PEG with different molecular weights should be used for the conservation of excavated charred woods.

SEM/EDX Analysis on the Composition and Surface Defect in a Pin Bushing Bearing for an Automotive Engine (자동차 엔진용 핀부싱 베어링의 SEM/EDX 이용 성분.결함분석에 관한 연구)

  • Kim, Chung-Kyun
    • Tribology and Lubricants
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    • v.23 no.5
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    • pp.195-200
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    • 2007
  • This paper presents the friction induced scuffing and wear defects analysis of a pin bushing bearing based on the chemical composition using a scanning microscopy (SEM) and an energy dispersive X-ray analyzer (EDX). The SEM/EDX system, which may provide good information on the surface thermal defects and chemical compositions, provides impurities such as an aluminum, a silicon, a ferrous component and an oxygen, especially. The EDX measured results show that the oxygen may reduce the strength and a hardness of a pin busing, which may lead to a scuffing and a seizure on the rubbing contact surface. The current technology fabricated by a sintering for a pin bushing bearing should be modified or changed to reduce the oxygen composition and the impurities in pin bushing materials.

A Study on individual Diesel Particles by SEM/EDX (SEM/EDX를 이용한 디젤 분진의 입자별 분석)

  • 김혜진;이종태;김동술
    • Journal of Korean Society for Atmospheric Environment
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    • v.15 no.2
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    • pp.175-182
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    • 1999
  • Scanning electron microscopy (SEM) has played an important role in receptor modeling area because it is a powerful tool for characterizing individual particles. The purpose of the study was to classify individual diesel particles base on statistical analysis and image analysis by SEM/EDX (energy dispersive x-ray analyser). The diesel particles were sampled by both a modified CVS 75 mode and a high speed mode with a chassis dynamometer. The SEM/EDX system provides various physical parameters including particle's particle diameter and chemical information. Thus density and mass of the diesel particle were estimated cased on its chemical composition and further fractal dimensions of the diesel particle were obtained by the Hurst exponent method. The fractal dimension in the sample of modified CVS 75 mode was higher than the high speed mode. Finally, mass fractions for a diesel vehicle as a source profile were estimated cased on a particle class concept.

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On the Surface Defect Analysis of an Aluminum Tube for an OPC Drum using n SEM and EDX (SEM/EDX를 이용한 OPC 드럼용 Al 튜브의 표면결함 분석에 관한 연구)

  • Kim, Chung-Kyun
    • Tribology and Lubricants
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    • v.23 no.4
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    • pp.143-148
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    • 2007
  • The surface defects of an aluminum tube for an OPC drum have been analyzed using a scanning microscopy(SEM) and an energy dispersive X-ray analyze.(EDX). The SEM/EDX system, which may provide good information on the surface defects and their distributions, provides an optical diameter of an impurity and a chemical composition. These are strongly related on the coated film thickness and quality of an OPC drum, which is a key element of a toner cartridge for a laser printer. The experimental results show that the local deformations, scratch wear, and flaws are produce the non-uniform coating layers, which may be removed by a manufacturing process of an aluminum tube. The major parameters on the coating quality of an OPC drum are the impurities of an aluminum tube such as silicon, oxygen, calcium, carbon, sulphur, chlorine, and others. These impurities may be removed by an ingot molding, extrusion and drawing, quality control, and packing processes with a strict manufacturing technology.

Dissolution Resistance Property of Modified Asphalt Waterproofing Sheet Coated with Polyamide Film by SEM-EDX Analysis (폴리아마이드 필름이 코팅된 개량 아스팔트 방수시트의 SEM-EDX 분석을 통한 유기용제 저항성 확인)

  • An, Ki-Won;Yoo, Jae-Yong;Oh, Sang-Keun
    • Journal of the Korea Institute of Building Construction
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    • v.17 no.5
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    • pp.437-444
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    • 2017
  • In the composite waterproofing method in which a polyurethane coating waterproofing material is applied on the modified asphalt waterproofing sheet, the organic solvent is diluted in the coating waterproofing material in order to improve the workability. However, since the organic solvent is not volatilized before the curing of the polyurethane coating waterproofing material, the organic solvent causes dissolution of asphalt layer, thereby causing oil leakage. As a result, a polyamide film having a high dissolution resistance property was laminated on modified asphalt sheet, and through testing the dissolution resistance was visually confirmed and quantitative analysis of the polyamide film by SEM-EDX analysis was also used to confirmed the dissolution resistance of the polyamide film.

Analysis of Deposited Dust Particles using SEM/EDX (SEM/EDX 분석법을 이용한 침착먼지에 대한 분석사례)

  • Ha, Eun-Ji;Park, Jeong-Ho
    • Journal of Environmental Science International
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    • v.30 no.3
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    • pp.279-287
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    • 2021
  • In this study, the composition and morphology of deposited dust particles with size ranging from a few to tens ㎛ were investigated using SEM/EDX (scanning electron microscopy with energy dispersive x-ray spectrometer). Then deposited dust particles were classified into 8 groups: quartz, aluminosilicates, ca-rich, Fe/Ti oxide, carbon-rich, industrial particle, Fe-rich, and biogenic particle. The sources of deposited dust were high in the order of aluminosilicates 41% > biogenic 18% > Fe-rich 11% > quartz and C-rich 8% > industrial 7% > Fe/Ti oxide 5% > Ca-rich 1%. In particular, the ratio of biogenic particles was relatively high due to influence of pollen. The ratio of carbon-rich was 11% at YM site, 10% at MD site, and 4% at MO site, and the site close to the large emission source was high.

Analysis of rifle and pistol primer gunshot residue using SEM-EDX (SEM-EDX에 의한 소총과 권총의 뇌관화약잔사 분석)

  • Jeon, Chung-Hyun;Park, Sung-Woo
    • Analytical Science and Technology
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    • v.23 no.3
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    • pp.322-329
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    • 2010
  • Primer gunsot residues (GSR) obtained from K1A and K2 rifles, and K5 pistol were analysed with scanning electron microscopy/energy dispersive X-ray spectrometry (SEM-EDX) as basic data in firearm accidents. Ammunition of 5.56 mm is employed for K1A and K2 rifles and 9.0 mm for a K5 pistol. The analyses of morphology, size, particle number, elemental ratio were performed for primer GSR prepared after shooting 3 times. The detected content was Ba>Pb>Sb in most GSR particles but Sb>Pb>Ba or Pb>Sb>Ba in some particles. In the statistical result of composition ratio of elements, the particles with more Sb than Ba were detected in most primer GSR from a K5 pistol, 3~8 times more than K1A and K2 rifles. This results can be employed to discriminate gun type between rifles and pistols. Furthermore, the size and the number of particles can be applied to access the type of guns.