• Transactions of the Korean Society of Mechanical Engineers A
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• v.37 no.1
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• pp.67-75
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• 2013

The flow stress of zircaloy-4 used in the spacer grid supporting a nuclear fuel rod was determined by the Johnson-Cook model, and model parameters were determined using reverse engineering. Parameters such as A, B, n and $\dot{\varepsilon}_0$ were determined by the tensile test result. To obtain the parameters C and m, a slot milling test and numerical simulation were performed. The objective functions were defined as the difference between the experimental and the simulation results, and then, the parameters were determined by minimizing the objective function. To verify the validity of the determined parameters, cross-verification for each case was conducted through a shearing test and simulation. The results tend to show agreement with the experimental results, such as the features of sheared edges and maximum punch force, with the correlation coefficients exceeding at least 0.97.

• Progress in Superconductivity
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• v.8 no.1
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• pp.108-112
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• 2006

We fabricated Bi-2212/$SrSO_4$ bulk superconductors by the casting process and evaluated the effects of the powder mixing method and annealing temperature on the texture, microstructure, and critical current. In the process, the Bi-2212 powders were mixed with $SrSO_4$ by hand-mixing(HM) and planetary ball milling(PBM) method and then the powder mixtures were melted at $1100^{\circ}C{\sim}1200^{\circ}C$, solidified, and annealed. We observed that the rod made by the PBM had a more homogeneous microstructure and smaller $SrSO_4$ and second phases than that of the rod made by the HM, resulting in increased $I_c$. The $I_c$ of the rod also depended on the annealing temperature and the highest $I_c$ was obtained to be 200 A when prepared by HM at $1200^{\circ}C$ and annealed at $810^{\circ}C$ which is probably due to the moderate density and 2212 texture and the smaller and less second phase compared to that at higher temperature. The possible causes of the variations of $I_c$ with the powder mixing method and annealing temperature were related to the microstructural evolution based on the SEM, EPMA, and DTA analyses.

• Korean Journal of Materials Research
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• v.27 no.10
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• pp.534-543
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• 2017

$Gd_2O_3:Eu^{3+}$ red phosphors were prepared by template method from crystalline cellulose impregnated by metal salt. The crystallite size and photoluminescence(PL) property of $Gd_2O_3:Eu^{3+}$ red phosphors were controlled by varying the calcination temperature and $Eu^{3+}$ mol ratio. The nano dispersion of $Gd_2O_3:Eu^{3+}$ was also conducted with a bead mill wet process. Dependent on the time of bead milling, $Gd_2O_3:Eu^{3+}$ nanosol of around 100 nm (median particle size : $D_{50}$) was produced. As the bead milling process proceeded, the luminescent efficiency decreased due to the low crystallinity of the $Gd_2O_3:Eu^{3+}$ nanoparticles. In spite of the low PL property of $Gd_2O_3:Eu^{3+}$ nanosol, it was observed that the photoluminescent property was recovered after re-calcination. In addition, in the dispersed nanosol treated at $85^{\circ}C$, a self assembly phenomenon between particles appeared, and the particles changed from spherical to rod-shaped. These results indicate that particle growth occurs due to mutual assembly of $Gd(OH)_3$ particles, which is the hydration of $Gd_2O_3$ particles, in aqueous solvent at $85^{\circ}C$.

• Journal of Powder Materials
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• v.15 no.3
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• pp.239-243
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• 2008

Ni-W(1-5 at.%) alloy rods were made by powder metallurgy process including powder mixing, compacting and subsequent sintering. Ni and W powder of appropriate compositions were mixed by a ball milling and isostatically pressed in a rubber mold into a rod. The compacted rods were sintered at $1000^{\circ}C-1150^{\circ}C$ at a reduced atmosphere for densification. The lattice parameters of Ni-W alloys were estimated by a high resolution neutron powder diffractometer. All sintered rods were found to have a face centered cubic structure without any impurity phase, but the diffraction peak locations were linearly shifted with increasing W content. The lattice parameter of a pure Ni rod was $3.5238{\AA}$ which is consistent with the value reported in JCPDS data. The lattice parameter of N-W alloy rods increased by $0.004{\AA}$ for 1 atomic % of W, which indicates the formation of a Ni-W solid solution due to the substitution of nickel atoms by tungsten atoms of larger size.

• Journal of Forest and Environmental Science
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• v.33 no.1
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• pp.33-38
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• 2017

In this study, spray-drying yield and morphological characterization of spray-dried cellulose nanofibril (CNF) and TEMPO-oxidized nanocellulose (TONC) depending on spray-drying condition and surfactant addition was investigated. As spray-drying temperature increased, the yield of spray-dried CNF was increased. The highest spray-drying yields in both nanocelluloses were found at didecyl dimethyl ammonium chloride (DDAC) addition of 2.5 phr at all investigated temperatures. The spray-dried CNF was the sphere-like particle, but the spray-dried TONC showed both rod and sphere-like morphology. The average diameter of spray-dried CNF was decreased with increasing DDAC addition amount, resulting in the increase of specific surface area.

• Journal of Powder Materials
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• v.2 no.2
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• pp.135-141
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• 1995

As the first step of study on fabrication of ceramic powders from phytoliths in rice, especially in rice husks, pulverization method of rice husks and the properties of milled rice husks were investigated. Impact methods, such as ball milling, were not meaningful for pulverizing elastic and thin fabric structure of rice husks. The most effective one was cutting method. In the present work, a rotating knife cutting method was applied to pulverizing rice husks. A 40-mesh screen was inserted under the rotating knives. The most portion of the milled powder was found in -50/+100 mesh section. Morphology of the milled rice husks revealed that the husks larger than 70 mesh were flake-like shape, at -70/+100 mesh section relatively equi-axed shape, at -170/+325 mesh section rod-like shape, and below 325 mesh section dust-like shape. Tap density of raw rice husks was about 0.1 $g/cm^3$, while those of milled rice husks were over $0.4 g/cm^3$. This meant that, for a given volume of reactor, raw material charge can be increased more that 4 times when using milled rice husks than unmilled one. True densities of unmilled and milled rice husks were higher than $1.4 g/cm^3$, and increased with decreasing milled sizes.

• Proceedings of the KSME Conference
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• 2001.11a
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• pp.753-759
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• 2001

The purpose of this study is to suggest the machining technique of the constant control of cutting speed in order to improve precision machining and tool life in high speed machining using ball end mill. Cutting speed is changed in machining free form surface like free form surface. So, we don't have supreme surface form and toll life on machining. The way to solving this problem is that we should be settled to optimal cutting speed in free form surface machining. And, to improve precision machining is executed high speed machining method to output optimum NC data with developed constant control of cutting speed program after modeling of CAD/CAM. In this paper, a comparison was made of the cutting precision and tool life in conventional cutting and those in free form surface machining applying the program developed.

• Journal of the Korean Society for Precision Engineering
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• v.21 no.12
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• pp.174-181
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• 2004

Ultra precision positioning mechanism has widely been used on semiconductor manufacturing equipments, optical spectrum analyzer and cell manipulations. Ultra precision positioning mechanism is consisted of several actuators, sensors, guides and control systems. Its efficiency depends on each performance of components. The object of this study is to design, analysis and manufacture all of the inchworm linear motor system, which is one of the equipments embodied in ultra precision positioning mechanism. Inchworm linear motor system is consisted of a controller system and an inchworm linear motor, and its driving form is similar to a motion of spanworm. A design and manufacture of inchworm linear motor, which is consisted of three PZT actuators, a rod, two columns and a guide plate, are performed. Minimizing the von-Mises stress of the hinge using Taguchi method and simulation by FEM software optimizes the structural design in a column of flexure hinge. The designed columns and guide plates are manufactured by a W-EDM and NC-milling. A controller system, which is an apparatus to drive inchworm linear motor, can easily adjust driving conditions by varying resonance frequency and input-output voltage of actuators and amplifiers. The performance of manufactured inchworm linear motor system is verified and valuated. In the future, inchworm linear motor system will be used to make a more precision positioning by reinforcing a sensor and feedback system.

• The Journal of Advanced Prosthodontics
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• v.6 no.5
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• pp.346-350
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• 2014

PURPOSE. Impact forces in implant supported FDP (fixed dental prosthesis) are higher than that of tooth supported FDPs and the compositions used in frameworks also has a paramount role for biomechanical reasons. The aim of this study was to evaluate the flexural strength of two different zirconia frameworks. MATERIALS AND METHODS. Two implant abutments with 3.8 mm and 4.5 mm platform were used as premolar and molar. They were mounted vertically in an acrylic resin block. A model with steel retainers and removable abutments was fabricated by milling machine; and 10 FDP frameworks were fabricated for each Biodenta and Cercon systems. All samples were thermo-cycled for 2000 times in $5-55^{\circ}C$ temperature and embedded in $37^{\circ}C$ artificial saliva for one week. The flexural test was done by a rod with 2 mm ending diameter which was applied to the multi-electromechanical machine. The force was inserted until observing fracture. The collected data were analyzed with SPSS software ver.15, using Weibull modulus and independent t-test with the level of significance at ${\alpha}=.05$. RESULTS. The mean load bearing capacity values were higher in Biodenta but with no significant differences (P>.05). The Biodenta frameworks showed higher load bearing capacity ($F_0=1700$) than Cercon frameworks ($F_0=1520$) but the reliability (m) was higher in Cercon (m=7.5). CONCLUSION. There was no significant difference between flexural strengths of both zirconia based framework systems; and both Biodenta and Cercon systems are capable to withstand biting force (even parafunctions) in posterior implant-supported bridges with no significant differences.

• Korean Journal of Food Science and Technology
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• v.48 no.4
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• pp.361-365
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• 2016

This study was conducted to isolate and identify a microorganism that increases tricin-O-(threo-${\beta}$-guaiacylglyceryl) ether (TTGE) content in the hulls of rice (Oryza sativa L.). Bacteria from germinated rice were isolated by enrichment cultivation using yeast mold, luria bertani, potato dextrose and mannitol egg york polymyxin broths. The highest increase in TTGE content ($339.30{\mu}g/g$) was achieved by a microorganism isolated by PDA enrichment cultivation. On the basis of 16S RNA sequence homology and phylogenetic analysis, the isolated bacterium was identified to have 100% similarity with Burkholderia vietnamiensis. The isolated bacteria were short rods, negative for the Gram stain, and positive for the catalase test. The highest TTGE level was $435.86{\mu}g/g$ in 72-h fermented samples, representing a 2.5x increase compared with the control ($175.65{\mu}g/g$). In conclusion, the bacterium isolated from germinated rice extract was Burkholderia vietnamiensis, and the optimum fermentation period to maximize TTGE levels was 72 h. These findings might help in developing functional materials using rice hulls, a waste product of rice milling.