• Title/Summary/Keyword: Research synthesize

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Preparation of Silver Nanocolloids Using Silver Alkylcarbamate Complex in Organic Medium with PVP Stabilizer

  • Park, Hyung-Seok;Park, Heon-Su;Gong, Myoung-Seon
    • Bulletin of the Korean Chemical Society
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    • v.31 no.9
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    • pp.2575-2580
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    • 2010
  • We present a method for chemically reducing silver alkylcarbamate complex with hydrazine to synthesize silver nanocolloids in an organic solvent using polyvinylpyrrolidone (PVP) as the stabilizer. To determine the optimal conditions for preparing stable silver colloids of controlled size and shape, the silver 2-ethylhexylcarbamate (Ag-EHCB) complex, PVP, hydrazine, and 2-propanol solvent concentrations in the reaction mixture were varied. The initial colloid has a mean particle diameter of 5-80 nm, and it exhibits an absorption band with various shapes in the UV region with a maximum near 420 nm. UV-vis spectroscopy, TEM, and X-ray diffraction techniques were used to investigate the formation and growth process of the metallic silver nanocolloids.

Effect of Gluconic Acid on the Production of Cellulose in Acetobacter xylinum BRC5

  • PARK, SANG TAE;TAEKSUN SONG;YOUNG MIN KIM
    • Journal of Microbiology and Biotechnology
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    • v.9 no.5
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    • pp.683-686
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    • 1999
  • Four mutants of Acetobacter xylinum BRC5 defective in gluconic acid production were isolated from UV-irradiated cells. The gluconic acid-negative mutants did not show glucose oxidase activity. The mutants were also defective in cellulose production. A randomly selected mutant grown in the Hestrin-Schramm medium (pH 6.0) supplemented with gluconic acid, however, was found to synthesize cellulose. The mutant grown in Hestrin-Schramm medium whose pH was adjusted to 5.0 with HC1 and contained no gluconic acid also produced cellulose. Wild-type cells grown under the same condition synthesized cellulose more rapidly than those grown in the pH 6.0 medium.

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A Synthesis on Essential Issues in the Field of Mathematics Education (수학교육분야에서 중요한 이슈들에 대한 통합)

  • Kim, Dong-Joong;Cho, Jeong-Il
    • Journal of the Korean School Mathematics Society
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    • v.14 no.3
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    • pp.377-388
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    • 2011
  • Acknowledging mathematics education as a research field and its relation to different domains such as mathematics, educational sciences, psychology, sociology, and history, two paradigmatic issues of theoretical research and classroom practice are focused on to synthesize the different domains in mathematics education. Six sub-categories in the field of mathematics education are proposed to have a better understanding of their role and interdependence.

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Synthesis of Aluminum Nitride Nanopowders by Carbothermal Reduction of Aluminum Oxide and Subsequent In-situ Nitridization (산화알루미늄 분말의 탄소열환원 및 직접 질화반응을 통한 질화알루미늄 나노분말의 합성)

  • Seo, Kyung-Won;Lee, Seong-Yong;Park, Jong-Ku;Kim, Sung-Hyun
    • Journal of Powder Materials
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    • v.13 no.6 s.59
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    • pp.432-438
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    • 2006
  • Aluminum nitride (AlN) nanopowders with low degree of agglomeration and uniform particle size were synthesized by carbothermal reduction of alumina and subsequent direct nitridization. Boehmite powder was homogeneously admixed with carbon black nanopowders by ball milling. The powder mixture was treated under ammonia atmosphere to synthesize AlN powder at lour temperature. The effect of process variables such as boehmite/carbon black powder ratio, reaction temperature and reaction time on the synthesis of AlN nanopowder was investigated.

Effect of Mineralizer Concentration and Starting Materials on the Characteristics of PZT Powders by Hydrothermal Process (수열합성법으로 제조된 PZT 분말의 특성에 미치는 광화제 농도와 출발물질의 영향)

  • Yang, Beom-Seok;Yun, Ki-Seok;Park, Young-Chul;Won, Chang-Whan
    • Journal of the Korean Ceramic Society
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    • v.42 no.11 s.282
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    • pp.743-748
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    • 2005
  • The effect of reaction parameters in the characteristic of $Pb(Zr_{0.52} Ti_{0.48})O_3$ powders by hydrothermal process was investigated in this study. In the preparation of PZT, the types of starting material and concentration of mineralizer on phase fraction and morphology was investigated respectively. Regardless the types of Pb precursor, PZT was able to synthesize ranging from 7 to 20 on KOH concentration and from 13.01 to 13.55 on pH of solution. The particle size of the PZT powders can be controlled by the mineralizer concentration and various types of precursor.

Preparation and Characterization of Coating Solution Based on Waterborne Polyurethane Dispersion containing Fluorine for Primer on Electro Galvanized Steel Sheet

  • Jin, Chung Keun;Lim, Sung Hyung
    • Corrosion Science and Technology
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    • v.14 no.5
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    • pp.207-212
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    • 2015
  • The purpose of this research was to synthesize fluorine modified waterborne polyurethane dispersion (F-WPU) by soap-free (internal emulsifier) emulsion polymerization techniques, to prepare coating solution based on fluorine modified waterborne polyurethane dispersion (F-WPU) and to compare the chemical and thermo-mechanical properties on the electrogalvanized steel sheet. Environmentally friendly F-WPU was prepared with a fluorinated polyol containing 60 wt% of fluorine. There are various ways of combining a wide variety of fluorinated polyols and diisocyanate to exhibit novel properties of waterborne polyurethane dispersion. Components of coating solution were largely divided into 4 kinds i.e., F-WPU, acrylic emulsion, silane coupling agent, and colloidal silicate. F-WPU coating solution on the electro-galvanized steel sheet showed excellent properties of corrosion resistance, alkali resistance and heat resistance, as compared to other coating solutions using a general waterborne resin. The F-WPU coating solution's reliable effects are possibly due to the fluorine atoms incorporated even in a small amount of F-WPU.

Preparation of Iron Catalytic Layer onto Functionalized Silicon Substrate for Synthesis of Carbon Nanotubes

  • Adhikari, Prashanta Dhoj;Cho, Jumi;Park, Chong-Yun
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.02a
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    • pp.611-611
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    • 2013
  • In this study, iron oxide nanoclusters layer (Nc) was prepared onto functionalized silicon substrate by wet method. The amine-terminated SAM fabricated on silicon substrate (APTMS/Si) was carried out by UV-treatment and immersed into the FeCl3/HCl aqueous solution. Then, Nc were immobilized onto oxidized SAM silicon substrate (SAMs/Si) through electrostatic interaction between cationic Nc and anionic SAMs/Si. This catalytic layer (Nc/SAMs/Si) was used to grow carbon nanotubes (CNTs). The characterization results clearly show that the well-graphitized CNTs were synthesized by using functionalized silicon substrate as a template having appropriate density of catalyst. These consequences show that SAM containing template is important to achieve the effective layer of catalyst to synthesize CNTs.

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Biosynthesis of Indole-3-acetic Acid in Ginseng Growth-promoting Pseudomonas fluorescens KGPP 207

  • Leonid, N.Ten;Lee, Mee-Kyoung;Lee, Mi Ja;Park, Hoon
    • Journal of Applied Biological Chemistry
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    • v.43 no.4
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    • pp.269-272
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    • 2000
  • The ginseng growth-promoting bacterium Pseudomonas fluorescens KGPP 207 synthesized indole-3- acetic acid (IAA) from L-tryptophan, indole-3-pyruvic acid (IPyA), and indole-3-acetaldehyde (IAAld), but not from indole-3-acetamide (lAM) and other intermediates of various IAA biosynthetic pathways in the experiment with indole compound supplemented cell suspensions. TLC, HPLC, and GC-MS analyses revealed the presence of IPyA, indole-3-ethanol, indole-3-lactic acid and its methyl ester, IAA and its methyl, and ethyl esters in the culture supernatant of the bacterium. IAAld was detected in the supernatant using sodium bisulfite and TLC. The results indicate that unlike gall-forming bacteria which can synthesize IAA by lAM, the indole-3-pyruvic acid pathway is the route for IAA biosynthesis in this beneficial strain of P. fluorescens.

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General Coupling Matrix Synthesis Method for Microwave Resonator Filters of Arbitrary Topology

  • Uhm, Man-Seok;Lee, Ju-Seop;Yom, In-Bok;Kim, Jeong-Phill
    • ETRI Journal
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    • v.28 no.2
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    • pp.223-226
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    • 2006
  • This letter presents a new approach to synthesize the resonator filters of an arbitrary topology. This method employs an optimization method based on the relation between the polynomial coefficients of the transfer function and those of the $S_{21}$ from the coupling matrix. Therefore, this new method can also be applied to self-equalized filters that were not considered in the conventional optimization methods. Two microwave filters, a symmetric 4-pole filter with four transmission zeros (TZs) and an asymmetric 8-pole filter with seven TZs, are synthesized using the present method for validation. Excellent agreement between the response of the transfer function and that of the synthesized $S_{21}$ from the coupling matrix is shown.

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Study on Current State of the Art of Serviscape in Healthcare Sector (의료분야의 서비스케이프 연구동향에 관한 연구)

  • Lee, Chang Won;Kim, Hee Soo
    • Korea Journal of Hospital Management
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    • no.spc
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    • pp.14-24
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    • 2016
  • This study is to present current research state of the art in serviscape and performance in healthcare system. Previous studies related to serviscape in healthcare sector are explored with limitations. This study conducts a content analysis with literature reviews in order to synthesize previous studies into three branch constitution dimension of the serviscape presenting the service environment. This study provides a current research state of the art and a future direction in serviscape in healthcare sector. Study results provide serviscape, customer response, satisfaction, and behavior intention in terms of healthcare settings. The patients and hospital customers as well as hospital employees should share the service experiences of the good quality in a proper service environment so that the patients and customer can satisfy and revisit the hospital.