• Title/Summary/Keyword: Reflection method

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Sorption Preconcentration and Determination of Nickel in Wastes of Heat Power Industry by Diffuse Reflection Spectroscopy

  • Kalyakina, O.P.;Kononova, O.N.;Kachin, S.V.;Kholmogorov, A.G.
    • Bulletin of the Korean Chemical Society
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    • v.24 no.2
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    • pp.173-177
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    • 2003
  • The present work is focused on the preconcentration of nickel and its determination by means of diffuse reflection spectroscopy. The preconcentration of nickel was carried out by sorption on macroporous aminocarboxylic amphoteric resin ANKB-35. Based on this collector, a method to determine nickel in wastes of heat power industry was worked out using solid-phase spectroscopy. The colored surface compound to be determined was obtained by a preceding nickel sorption on the resin and by subsequent treatment of the concentrate obtained with definite amounts of 1-(2-pyridilazo)-2-naphtol (PAN). The Ni calibration curve is linear in the concentration range of 0.5-20.0 mg/L (sample volume is 200.0 mL) and the detection limit is 0.05 mg/L. The presence of $Cu^{2+},\;Fe^{3+},\;Co^{2+}$ ions as well as macrocomponents of natural water $(Na^+,\;K^+,\;Ca^{2+},\;Mg^{2+})$ do not hinder the solid-phase spectroscopy determination of nickel. The nickel determination by diffuse reflection spectroscopy was carried out in model solutions as well as in solutions obtained after the dissolution of wastes of heat power industry.

Visual Inspection System for Irregularly Formed Timing Belt with Low Reflection Ratio (저반사비를 가진 비균질 타이밍 벨트를 위한 자동시각 검사시스템)

  • Lee, Jae-Woo;Yoon, Joong-Sun
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.13 no.5
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    • pp.1996-2001
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    • 2012
  • Visual inspection systems are widely proposed for the well formed surface materials like electronics parts. But the materials with ill reflection ability have many troubles when visual inspection system is introduced. We have developed a robust visual inspection system that can work well in spite of low reflection ratio and with much noise when truth model is not known in the mixed production line. A workpiece identification technique using k-means has been proposed to identify the type. Based on the identified type, a robust-to-noise segmentation method, called active contour, has been applied to segment the features from the image. Finally, Kalman filter has been applied to adapt the error variation. Experiment shows that performance is about to match the accuracy of manual measurement using projectors.

A Hybrid Boundary Integral Equation Model Applied for the Calculation of Normal Incident Waves (혼합경계적분 요소법을 사용한 직교입사파랑의 반사률계산 모델)

  • 서승남;김상익
    • Journal of Korean Society of Coastal and Ocean Engineers
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    • v.3 no.3
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    • pp.170-175
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    • 1991
  • In order to calculate reflection coefficients of surface waves due to underwater obstacles, the hybrid boundary integral equation method is used. Numerical results based on the linear element are verified to the exact solutions for a flat bottom. Reflection coefficient and transmission coefficients for a step are compared to Young's results and the results by EFEM (Kirby et al., 1987), in which reflection coefficients decrease to zero as the periods of incident waves decrease. Reflection coefficients for a sinusiodal hump located on a constant depth increase due to the interaction between humps.

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Soft Mold Imprinting Fabrication of Anti-reflection Film using Self-Organized Nanostructure Polymer Surfaces Irradiated by Ion Beams (이온빔 처리된 폴리머 표면의 자가나노구조화를 이용한 반사방지 필름 제조용 소프트 몰드 임프린팅 연구)

  • Lee, Seunghun;Byeon, Eun-Yeon;Choi, Juyeon;Jung, Sunghoon;Yu, Byeong-Gil;Kim, Do-Geun
    • Journal of the Korean institute of surface engineering
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    • v.50 no.6
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    • pp.480-485
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    • 2017
  • Soft mold imprinting method that uses nanostructured polymer mold was investigated for anti-reflection film fabrication. The nanostructured soft mold was polyethylene terephthalate(PET) irradiated by oxygen ion beams. The collisional energy transfer between oxygen ion and the polymer surface induced cross-linking and scission reactions, resulting in self-organized nanostructures with regular patterns of the wavenumber of $5{\mu}m^{-1}$. Post processes including ultra-violet curable resin coating and delamination fabricated anti-reflection films. The imprinted resin surface also showed the consistent wavenumber, $5{\mu}m^{-1}$. Pristine PET, oxygen ion beam treated PET, and imprinted replica sample showed total transmittance of 91.04, 93.25, and 93.57-93.88%, respectively.

Study of Phase Transition of Copper(II)-phthalocyanine using a Near Field Scanning Microwave Microscope (근접장 마이크로파 현미경을 이용한 Copper(II)-phthalocyanine의 Phase Transition 연구)

  • Park, Mie-Hwa;Yoo, Hyun-Jun;Yun, Soon-Il;Lim, Eun-Ju;Lee, Kie-Jin;Cha, Deok-Joon;Lee, Young-San
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.17 no.6
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    • pp.641-646
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    • 2004
  • We report the changes of the microwave reflection coefficients S$_{11}$ of copper(II)-phthalocyanine (CuPc) thin films by using a near-field microwave microscope(NSMM) in order to understand the phase transition of CuPc. For a NSMM system, a high-quality microstrip resonator coupled with a dielectric resonator was used. CuPc thin films were prepared on the pre-heated glass substrates using a thermal evaporation method. The reflection coefficients S$_{11}$ of CuPc thin films were changed by the dependence on the substrate pre-heating temperatures. By comparing reflection coefficient S$_{11}$ and crystal structures, we found the phase transition of CuPc thin films from $\alpha$-phase to $\beta$-phase at the substrate heating temperature 200 $^{\circ}C$./TEX>.

NUMERICAL ANALYSIS OF WAVE CHARACTERISTICS AROUND PERMEABLE SUBMERGED BREAKWATER ON THE POROUS SEABED (침투 해저면 위의 투과잠제주변 파랑특성의 수치해석)

  • Kim, N.H.;Woo, S.M.
    • Journal of computational fluids engineering
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    • v.19 no.3
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    • pp.8-13
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    • 2014
  • In this study, wave characteristics coming with oblique incident angle to permeable trapezoidal submerged breakwater on the porous seabed are calculated by using boundary element method. This numerical analysis, based on the wave pressure function, is analyzing the continuity in the analytical region including fluid and structure. From the comparison of the reflection coefficients and damping coefficient, the results of this study are in good agreement with the existing results. The peak values of reflection coefficient obtained by permeable trapezoidal submerged breakwater on the porous seabed are smaller than those of permeable trapezoidal submerged breakwater on the non-porous seabed. The velocity vector in front of permeable trapezoidal submerged breakwater on the porous seabed is smaller than that in front of permeable trapezoidal submerged breakwater on the non-porous seabed with out the energy loss.

Investigation of Layered Structure of Fiber Cell Wall in Korean Red Pine by Confocal Reflection Microscopy

  • Kwon, Ohkyung
    • Applied Microscopy
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    • v.44 no.2
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    • pp.61-67
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    • 2014
  • Layered structures of fiber cell wall of Korean red pine (Pinus densiflora) were investigated by confocal reflection microscopy (CRM). CRM micrographs revealed detailed structures of the fiber cell wall such as S1, S2, and S3 layers as well as transition layers (S12 and S23 layers), which are present between the S1, S2, and S3 layers. Microfibril angle (MFA) measurement was possible for the S2 and S3 layer in the cell wall. The experimental results suggest that CRM is a versatile microscopic method for investigation of layered structures and MFA measurement in individual sub layer of the tracheid cell wall.

Effects of Fluid Resistance Coefficient on Wave Characteristics around Permeable Submerged Breakwater

  • Kim, Namhyeong;Woo, Sumin;Ko, Yongsu
    • Proceedings of the Korean Institute of Navigation and Port Research Conference
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    • 2014.06a
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    • pp.244-245
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    • 2014
  • Recently, the studies on submerged breakwater are increased due to needs considering the quality of water and the scenic view. In this paper, waves coming to permeable submerged breakwater coming with oblique angle are computed numerically by using wave pressure function. The wave pressure function throughout the analytical region including the fluid and submerged breakwaters is used. An unknown quantity expressed by the wave pressure function is simulated by boundary element method. The maximum reflection coefficient shows the tendency of decrease with the increase of oblique angle and The reflection coefficient shows the tendency of increase with the increase of the values of the linear dissipation coefficient and the added mass coefficient. It is means that the reflection coefficients are strongly dependent on the oblique angle and resistance coefficients.

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Wave Transmission Approach of Coupled Plate Structures through Non-conservative Joints for Power Flow Analysis (파워흐름해석을 위한 비보존 조인트로 편성된 평판 구조물의 파워투과반사계수 해석)

  • Song, J.H.;Hong, S.Y.;Park, Y.H.;Park, D.H.;Kil, H.G.
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2002.11b
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    • pp.505-510
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    • 2002
  • The attenuation of waves transmitted through non-conservative joints that are shown in many paractical structures, is affected by the impedance and the orientation of the joint. In this paper, the joints between plate structures are assumed to be modeled as linear spring-dashpot systems and the transmission and reflection of vibration energy in the medium to high frequency ranges are investigated. The calculated power transmission and reflection coefficients are applied to the PFA method for the prediction of energy density and intensity in structures.

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Measurement of Milling Ratio using the Visible and the Near-Infrared Rays Spectrum (가시광선 및 근적외선 스펙트럼을 이용한 도정비율 측정)

  • 이용국;이재현
    • Journal of Biosystems Engineering
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    • v.24 no.3
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    • pp.259-266
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    • 1999
  • This research was carried out to investigate the possibility of real time rice milling ratio measurement using the spectral reflection characteristics. In this study, various methods were compared such as \circled1 using the whiteness meter, \circled2 using the colorimeter, \circled3 using the Visible and the NIR reflection spectrum. The samples were milled in the domain of 84~96% by 0.5% interval classified by milling ratio. The NMG treatment method required about 20 minutes to determine the milled ratio and r2 was 0.0028 to 0.7959 that was very low. In case of whiteness meter, r2 was high but speed of measurement was 5 minutes that was very low. Measurement with the colorimeter required about 5 minutes and r2 was 0.60 to 0.85 that was low. The reflection spectrum were measured in the range of 400~2,500nm with 2nm interval and the MLR model with six-wavelength obtained from first derivative of spectra gave the best results(r2 = 0.967, SEP = 0.729%)

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