• Analytical Science and Technology
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• v.7 no.3
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• pp.421-425
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• 1994

A micro-high performance liquid chromatography(Micro-HPLC) techniquie with solid phase extraction was reported which detected carbendazim and carbaryl at picogram levels. They were separated on microbore packed $C_{18}$ column($1.0mm\;I.\;D{\times}150mm$, $d_f=5{\mu}m$) using a 50% methanol mobile phase and detected at UV 220nm(${\alpha}=2.94$, $R_s=4.71$), while they were not resolved on analtical HPLC system(${\alpha}=1.27$, $R_s=0.76$). The detection thresholds of carbendazim and carbaryl were 0.5ng and 0.1ng on Micro-HPLC, therefore Micro-HPLC system was 20~40 told more sensitive than anayltical HPLC system. Sep-Pak $C_{18}$ catridge was found to be efficient in enriching carbendazim and carbaryl from dilute aqueous solution with 97.0% and 97.8% recoveries of them. The Sep-Pak $C_{18}$ catridge followed by the Micro-HPLC had been applied to the quantitative analysis of carbendazim and carbaryl in spiked juices and a commercial drinking water.

• Journal of Korea Foundry Society
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• v.29 no.1
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• pp.27-32
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• 2009

The microstructure of Al-7Si-0.4Mg-1Fe alloy mainly consists of aluminum dendrites, Al-Si eutectics, and $Al_5FeSi$ needles. When Mn was added to the alloy, the substantial amount of $Al_5FeSi$ phase was changed into Al(Mn,Fe)Si, however the needle-like morphology was almost unchanged. Combined additions of Cr or Sr with Mn to the base alloy resulted in rod-like Al(Mn, Fe,Si)Si phase. The tensile properties of as-cast alloys were enhanced by the Mn addition, especially when it was added with Sr. The tensile properties after T6 heat treatment was a little improved with 0.7%Mn addition, but Cr or Sr additions with Mn didn't show any positive effect on the properties of heat-treated alloys.

• Journal of the Korean Electrochemical Society
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• v.10 no.3
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• pp.179-183
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• 2007

The corrosion behavior of metal covered with mortar under a wet-dry cyclic condition were investigated to apply for the measurement of corrosion rates of reinforcing steel in concrete structure. The carbon steel in mortar having t=3 mm cover thickness was exposed to the alternate condition of 6 h immersion in chloride containing solution and 18 h drying at $25^{\circ}C$ and 50%RH. The electrochemical phenomena of a carbon steel and mortar interface was explained by an equivalent circuit consisting of a solution resistance, a charge transfer resistance and a CPE(Constant Phase Element). The corrosion rates were monitored continuously during exposure using an AC impedance technique. Simultaneously, the current distribution over the working electrode during impedance measurement was analyzed from the phase shift, $\theta$, in an intermediate frequency. The result showed that corrosion rate monitoring using an AC impedance method is suitable under the given exposure conditions even during the drying period when the metal is covered with the wetted mortar.

• Journal of Korea Foundry Society
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• v.31 no.6
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• pp.354-361
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• 2011

The liquid metal shearing device was constructed and assembled with a commercial high-pressure die-caster in order to induce intensive turbulent shearing force on molten aluminum alloys. The effect of the liquid metal shearing on the microstructure and tensile properties of A356 alloys was investigated with the variation of iron content. The experimental results show that dendritic primary ${\alpha}$-Al phase was effectively modified into a equiaxed form by the liquid metal shearing. It was also found that the needle-like ${\beta}$-AlFeSi phase in a Fe containing A356 alloy was changed into a blocky shape resulting in the improved mechanical properties. Based on the mechanical properties, it was suggested that the iron content in A356 alloy could be more widely tolerated by utilizing the liquid metal shearing HPDC process.

• Journal of Electrical Engineering and Technology
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• v.8 no.1
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• pp.137-143
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• 2013

This paper presents development of variable speed generation (VSG) system with energy saving function. The rubber tyred gantry crane (RTGC) requires the power from diesel-engine. Significant fuel savings by reducing the engine speed can be achieved, because all of operation modes except hoisting are required lower power than rated value of engine. When low speed operation output voltage of generator is decrease until acceptable range of motor driver inverters and auxiliary load supplier. According to power demand engine speed is varying from 20 to 60Hz, and voltage is varying between 210Vac and 480Vac. When idle mode or low power operation dc/dc converter operates by constant output voltage control and inverters dc site voltage is compensated by it. This paper proposed 3-phase interleaved boost converter which has the same structure as the commercially available 3-phase inverter and current sharing capability. 400kW interleaved converter is designed and a performance of converter is evaluated through several experiments with a RTGC system. Energy saving VSG system can cut down fuel consumption by 36% and 21.3% at idle and unidirectional load operations.

• Journal of the Korean Institute of Illuminating and Electrical Installation Engineers
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• v.20 no.3
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• pp.62-68
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• 2006

In this paper, an adaptive input-output linearization and zero dynamics control of three phase AC/DC converter are proposed. For achieving output do voltage regulation with unity power factor, the q-axis current of the rotating d-q frame is regulated to zero and the output do voltage is controlled to track a given reference voltage $V_r$. The proposed scheme is robust to the parametric uncertainty md load current of the converter due to the adaptation process. The simulation results are presented to illustrate the performance and feasibility of the proposed control scheme.

• Proceedings of the KIEE Conference
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• 2000.07c
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• pp.1859-1861
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• 2000

The high temperature thermal plasma technology applied to waste treatment has undoubtedly gained high importance owing to its outstanding properties such as flexibility, compact reactor. and clean treatment as the environmental problem goes to a main issue in public talks, because the thermal plasma with temperature of around 10,000K or little less is particularly suitable for waste treatment. Since the thermal plasma is, in general, governed by a number of parameters, some complicated and elaborate controls might be mandatory. The high maintenance cost caused by big input power has been a main obstacle to the growth of the waste treatment plant based on thermal plasma technology, but the recent R&D on the waste-to-energy shows that the problem could be solved soon. In this paper, the authors introduce the current R&D activity related to three-phase ac plasma torch in KERI.

• Transactions of the Korean Society of Mechanical Engineers B
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• v.28 no.11
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• pp.1432-1439
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• 2004

By using unique experimental techniques and careful construction of the experimental apparatus, the characteristics of the local heat transfer were investigated using the condensing R134a two-phase flow, in horizontal single mini-channels. The circular channels (D$_{h}$=0.493, 0.691, and 1.067 mm) and rectangular channels (Aspect Ratio=1.0, D$_{h}$=0.494, 0.658, and 0.972 mm) were tested and compared. Tests were performed for a mass flux of 100, 200, 400, and 600 kg/$m^2$s, a heat flux of 5 to 20 ㎾/$m^2$, and a saturation temperature of 4$0^{\circ}C$. In this study, effect of heat flux, mass flux, vapor qualities, hydraulic diameter, and channel geometry on flow condensation are investigated and the experimental local condensation heat transfer coefficients are shown. The experimental data of condensation Nusselt number are compared with existing correlations.ons.

• Archives of Pharmacal Research
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• v.26 no.9
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• pp.763-767
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• 2003

The differences in pharmacokinetic behavior and tissue distribution of verapamil and its enantiomers were investigated in rats. In high-performance liquid chromatographic method, an achiral ODS column (150 mm $\times$ 4.6 mm i.d.) with the mobile phase consisting of methanol-water (73:30, v/v) was used for the determination of the concentration for racemic verapamil, and a Chiralcel OJ column (250 mm$\times$4.6 mm i.d.) with the mixture of n-haxane-ethanol-triethylamine (85:15:0.2, v/v/v) as mobile phase was used to determine the concentrations of verapamil enantiomers. A fluorescence detector in the analytical system was set at excitation and emission wavelengths of 275 nm and 315 nm. The differences between enantiomers were apparent in the pharmacokinetics in rats. The area under the concentration-time curve (AUC) of S-(-) verapamil was higher than that of R-(+) verapamil. The half-distribution time ($T_{1/2(\alpha)}$) of S-(-) verapamil which distributing to tissue from blood was shorter than that of R-(+) verapamil, but the elimination half-time ($T_{1/2(\beta)}$) was longer in rat following oral administration of racemic verapamil. At 1.3 h after oral administration of racemic verapamil, however, there were no significant differences between enantiomers for the distributions in major tissues such as heart, cerebrum, cerebellum, liver, spleen and kidney.

• Journal of the Korean Society of Visualization
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• v.19 no.1
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• pp.28-35
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• 2021

In this study, an image processing method for the measurement of two-phase bubbly flow is developed. Shadowgraphy images obtained by high-speed camera are used for analysis. Some bubbles are generated as single unit and others are overlapped or clustered. Single bubbles can be easily analyzed using parameters such as bubble shape, centroid, and area. But overlapped bubbles are difficult to transform clustered bubbles into segmented bubbles. Several approaches were proposed for the bubble segmentation such as Hough transform, connection point method and watershed. These methods are not enough for bubble segmentation. In order to obtain the size distribution of bubbles, we present a method of splitting overlapping bubbles using watershed and approximating them to ellipse. There is only 5% error difference between manual and automatic analysis. Furthermore, the error can be reduced down to 1.2% when a correction factor is used. The ellipse fitting algorithm developed in this study can be used to measure bubble parameters accurately by reflecting the shape of the bubbles.