• Title/Summary/Keyword: Pyrex

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Treatment of Odorous air pollutants by Plasma and Photocatalytic Process. (플라즈마 광촉매 복합 긍정을 이용한 악취물질 중 TEA, MEK의 분해처리)

  • 최금찬;정창훈
    • Journal of Environmental Science International
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    • v.12 no.12
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    • pp.1255-1260
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    • 2003
  • Plasma-photocatalytic oxidation process was applied in the decomposition of Triethylamine(TEA) and Methyl ethyl ketone(MEK). Plasma reactor was made entirely of pyrex glass and consists of 24mm inner diameter, 1,800mm length and discharge electrode of 0.4mm stainless steel. And initial concentrations of TEA and MEK for plasma-photocatalytic oxidation are 100 ppm. Odor gas samples were taken by gas-tight syringe from a glass sampling bulb which was located at reactor inlet and outlet, and TEA and MEK were determined by GC-FID. For plasma process, the decomposition efficiency of TEA and MEK were evaluated by varying different flowrates and decomposition efficiency of TEA and MEK increased considerably with decreasing treatment flowrates. For photocatalytic oxidation process, also the decomposition efficiency of TEA and MEK increased considerably with decreasing treatment flowrates. The decomposition efficiency of MEK was 57.8%, 34.2%, 18.8% respectively and the decomposition efficiency of TEA was reached all 100%. This result is higher than that of plasma process only, From this study, the results indicate that plasma-photocatalytic oxidation process is ideal for treatment of TEA and MEK.

Novel measuring technique for biological adhesion forces using AFM (원자현미경을 이용한 생체물질의 접착력 측정기술 개발)

  • Kim S.J.;Moon W.K.;Jun J.H.
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2005.06a
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    • pp.641-644
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    • 2005
  • The study on the interaction forces of some biological materials is important to understanding biological phenomena and their application to practical purpose. This paper introduces a measuring technique for biological adhesive forces using the AFM(Atomic Force Microscope). Since no standardized thesis on adhesive forces exist, the adhesive forces is defined as adhesive forces against a hardened surface of biological materials. To grant the results are meaningful, which is based on the understanding the surface characteristics of biological materials using the AFM, a nominal value of average adhesive force per unit area should be measured. Therefore the modified AFM probe with small micro glass bead was proposed so that it can guarantee the required contact area for measuring the average adhesive forces. A pyrex glass substrate with circular patterns, which was fabricated by micromachining technique, is introduced in order to controll the contact area. The two types of mussel adhesive proteins, Celltak and recombinant-MGFP5, were tested by the proposed measuring method. The test results show that the adhesive force of the mussel adhesive proteins can be reliably measured by use of this method.

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Study on Reliability of Vapor Cell by Laser Packaging with Au/Au-Sn Heterojunction (Au/Au-Sn 이종접합 적용 레이저 패키징을 통한 Vapor Cell 신뢰성 연구)

  • Kwon, Jin Gu;Jeon, Yong Min;Kim, Ji Young;Lee, Eun Byeol;Lee, Seong Eui
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.33 no.5
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    • pp.367-372
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    • 2020
  • As packaging processes for atomic gyroscope vapor cells, the glass tube tip-off process, anodic bonding, and paste sealing have been widely studied. However, there are stability issues in the alkali metal which are caused by impurity elements and leakage during high-temperature processes. In this study, we investigated the applicability of a vapor cell low-temperature packaging process by depositing Au on a Pyrex cell in addition to forming an Au-Sn thin film on a cap to cover the cell, followed by laser irradiation of the Au/Au-Sn interface. The mechanism of the thin film bonding was evaluated by XRD, while the packaging reliability of an Ne gas-filled vapor cell was characterized by variation of plasma discharge behavior with time. Furthermore, we confirmed that the Rb alkaline metal inside the vapor cell showed no color change, indicating no oxidation occurred during the process.

Microfilter Chip Fabrication for Bead-Based Immunoassay (비드를 이용한 면역분석용 마이크로필터 칩의 제작)

  • Lee, Seung-Woo;Ahn, Yoo-Min;Chai, Young-Gyu
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.28 no.9
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    • pp.1429-1434
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    • 2004
  • Immunoassay is one of the important analytical methods for clinical diagnoses and biochemical studies, but needs a long time, troublesome procedures and expensive reagents. In this study, therefore, we propose the micro filter chip with microbeads for immunoassay, which has pillar structures. The advantage of the proposed micro filter chip is to use simple fabrication process and cheap materials. The mold was made by the photolithography technique with Si wafer and negative photoresist SU-8. The replica was made of PDMS, bonded on the pyrex glass. The micro filter chip consists of inlet channel, filter chamber and outlet channel. HBV (Hepatitius B virus) monoclonal antibody (Ag1) labeled with biotin were immobilized onto streptavidin coated beads of 30∼50 $\mu$m size. Fluorescein isothiocyanate (FITC)-labeled HBV monoclonal antibody (Ag8) was used to detect HBsAg (Hebatitis B virus surface Antigen), and fluorescence intensity was monitored by epi-fluorescence microscope. In this study, the immune response of less than 30 min was obtained with with the use of 100 $m\ell$ of sample.

A Comparative Study on the Characteristics of Thermoacoustic Laser for Applying Solar Energy (태양열 적용을 위한 열음향 레이저의 특성 비교 연구)

  • Park, Sung-Seek;An, Eoung-Jin;Oh, Seung-Jin;Chun, Won-Gee;Kim, Nam-Jin
    • Journal of the Korean Solar Energy Society
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    • v.32 no.2
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    • pp.105-112
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    • 2012
  • The conversion of solar energy into acoustic waves is experimentally studied. Measurements were made on the Sound Pressure Level (SPL), frequency, onset time and the temperature gradient across the stack. A pyrex resonance tube is used with a honey-comb structure ceramic stack along with Ni-Cr and Cu wires. An AL1 acoustical analyzer was used to measure the SPL and frequency of acoustic waves whereas K-type thermocouples were hired to estimate temperature gradients. For a resonance tube of 100 mm, no acoustic waves were generated with a power input of 25W. By increasing its length to 200 mm, however, maximum SPLs of 96.4 dB, 106.3 dB and 112.8 dB were detected for the tubes of 10mm,20mm and 30mm in IDs and their respective stack positions of 70mm, 60mm and 50mm from the closed end.

Development for UV/TiO2 Photocatalytic Oxidation Indoor Air Compound Process (광촉매/광산화를 이용한 VOCs 처리장치 개발)

  • Jeon, Bo-Kyung;Choi, Kum-Chan;Suh, Jeong-Min
    • Journal of Environmental Science International
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    • v.15 no.9
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    • pp.855-864
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    • 2006
  • This study introduces a method to eliminate formaldehyde and benzene, toluene from indoor air by means of a photocatalytic oxidation reaction. In the method introduced, for the good performance of the reaction, the effect and interactions of the $TiO_2$ catalyst and ultraviolet in photocatalytic degradation on the reaction area, dosages of catalysts, humidity and light should be precisely examined and controled. Experiments has been carried out under various intensities of UV light and initial concentrations of formaldehyde, benzene and toluene to investigate the removal efficiency of the pollutants. Reactors in the experiments consist of an annular type Pyrex glass flow reactor and an 11W germicidal lamp. Results of the experiments showed reduction of formaldehyde, benzene and toluene in ultraviolet $/TiO_2/$ activated carbon processes (photooxidation-photocatalytic oxidation-adsorption processes), from 98% to 90%, from 98% to 93% and from 99% to 97% respectively. Form the results we can get a conclusion that a ultraviolet/Tio2/activated carbon system used in the method introduced is a powerful one for th treatment of formaldehyde, benzene and toluene of indoor spaces.

A Comparative Study on the Characteristics of Thermoacoustic Laser for Using Solar Energy (태양에너지 이용을 위한 열음향 레이저의 특성 비교 연구)

  • Park, Sung-Seek;An, Eoung-Jin;Oh, Seung-Jin;Chun, Won-Gee;Kim, Nam-Jin
    • 한국태양에너지학회:학술대회논문집
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    • 2012.03a
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    • pp.516-521
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    • 2012
  • The conversion of solar energy into acoustic waves is experimentally studied. Measurements were made on the Sound Pressure Level (SPL), frequency, onset time and the temperature gradient across the stack. A pyrex resonance tube is used with a honey-comb structure ceramic stack along with Ni-Cr and Cu wires. An AL1 acoustical analyzer was used to measure the SPL and frequency of acoustic waves whereas K-type thermocouples were hired to estimate temperature gradients. For a resonance tube of 100mm, no acoustic waves were generated with a power input of 25W. By increasing its length to 200mm, however, maximum SPLs of 96.4 dB, 106.3 dB and 112.8 dB were detected for the tubes of 10mm, 20mm and 30mm in IDs and their respective stack positions of 70mm, 60mm and 50mm from the closed end.

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A Study on Thermal Conductivity Measurement and Optical Characteristics of Thin Films (박막의 열물성 측정 및 광학특성 연구)

  • Gwon, Hyuk-Rok;Lee, Seong-Hyuk
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.56 no.12
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    • pp.2202-2207
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    • 2007
  • The present article investigates experimentally and theoretically thermal and optical characteristics of thin film structures through measurement of thermal conductivity of Pyrex 7740 and reflectance in silicon thin film. The $3{\omega}$ method is used to measure thermal conductivity of very thin film with high accuracy and the optical characteristics in thin films are studied to examine the influence of incidence angle of light on reflectance by using the CTM(Characteristics Transmission Method) and the 633 nm He-Ne laser reflectance measurement system. It is found that the estimated reflectance of silicon show good agreement with experimental data. In particular, the present study solves the EPRT(Equation of Phonon Radiative Transport) which is based on Boltzmann transport equation for predicting thermal conductivity of nanoscale film structures. From the results, the measured thermal conductivity is in good agreement with the previous published data. Moreover, thermal conductivities are estimated for different film thickness. It indicates that as film thickness decreases, thermal conductivity decreases substantially due to internal scattering.

Heat transfer enhancement of nanofluids in a pulsating heat pipe for heat dissipation of LED lighting

  • Kim, Hyoung-Tak;Bang, Kwang-Hyun
    • Journal of Advanced Marine Engineering and Technology
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    • v.38 no.10
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    • pp.1200-1205
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    • 2014
  • The effect of nanofluids on the heat transfer performance of a pulsating heat pipe has been experimentally investigated. Water-based diamond nanofluid and aluminium oxide ($Al_2O_3$) nanofluid were tested in the concentration range of 0.5-5%. The pulsating heat pipe was constructed using clear Pyrex tubes of 1.85 mm in inner diameter in order to visualize the pulsating action. The total number of turns was eight each for heated and cooled parts. The supply temperatures of heating water and cooling water were fixed at $80^{\circ}C$ and $25^{\circ}C$ respectively. The liquid charging ratio of the nanofluid was 50-70%. The test results showed that the case of 5% concentration of diamond nanofluid showed 18% increase in heat transfer rate compared to pure water. The case of 0.5% concentration of $Al_2O_3$ nanofluid showed 24% increase in heat transfer rate compared to pure water. But the increase of $Al_2O_3$ nanofluid concentration up to 3% did not show further enhancement in heat transfer. It is also observed that the deposited nanoparticles on the tube wall played a major role in enhanced evaporation of working fluid and this could be the reason for the enhancement of heat transfer by a nanofluid, not the enhanced thermal conductivity of the nanofluid.

Microflow Photochemistry - Acetone sensitized Addition of Isopropanol to (5R)-5-Menthyloxy-2-(5H)-furanone

  • Aida, Shin;Nishiyama, Yasuhiro;Kakiuchi, Kiyomi;Hoffmann, Norbert;Fon, Adeline;Oelgemoller, Michael
    • Rapid Communication in Photoscience
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    • v.2 no.3
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    • pp.68-71
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    • 2013
  • Acetone sensitized photoadditions of isopropanol to (5R)-5-menthyloxy-2-(5H)-furanone were investigated in two different microflow reactor systems. Setup A employed a commercially available glass reactor under a UVB-panel. Setup B utilized a FEP microcapillary wrapped tightly around a Pyrex cylinder with a single UVB fluorescent tube at its center. The reactions under flow conditions were subsequently compared to analogue reactions conducted in a batch chamber reactor. Overall, the microflow systems gave faster conversions and higher isolated yields. The flexible microcapillary setup, however, showed the best performance and promise in terms of future scale-up and reactor optimization.